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1.
Polymers (Basel) ; 14(15)2022 Jul 28.
Article in English | MEDLINE | ID: mdl-35956575

ABSTRACT

In this paper, we present an extensive experimental study on the dynamic mechanical properties of composites with polymer matrices, as well as a quantification of the parameters that influence these properties. Polymer-composite matrices make it possible to form any reinforcement arrangement of fibres, particles, and layers, which makes it possible to form composite materials with certain dominant mechanical properties according to the internal arrangement for the application. In this study, we focused on the dynamic properties (i.e., damping parameters, such as the loss factor (tan d), logarithmic decrement (λ), storage modulus (E'), and loss modulus (E″)) of composites with polymer matrices, including parameters such as the fibre material, fabric weaving, fibre orientation, temperature, frequency, particle size, volume of short fibres, and epoxy resin type. If other articles focus on one type of composite and 1-2 parameters, then the benefit of this article lies in our analysis of 8 mentioned parameters in the experimental analysis of 27 different types of composites with polymer matrices. The tested fibre materials were glass, aramid, and carbon; the tested woven fabrics were twill, plain, unidirectional, and satin; the temperature range was from -50 to +230 °C; the frequency was 1 Hz and 10 Hz; the particle size was 0.1-16 mm; the volume percentages of the short fibres were 3, 6, and 12 vol.% of the hybrid polymer composites and the type of polymer matrix. We used the free-damped-vibration method with vibration dynamic signal analysis and the forced-damped vibration of dynamic mechanical thermal analysis for testing. We ranked the parameters that influence the dynamic vibration properties according to the effects. Among sets of results provided in the paper, considering the storage modulus, loss modulus, and loss factor, the best results of the fibre composites were for aramid-fibre-reinforced polymers, regardless of the weave type, with an advantage for unidirectional fabric. The best results of the particle composites were for those with fine filler sizes that incorporated the short fibres.

2.
Materials (Basel) ; 15(11)2022 May 24.
Article in English | MEDLINE | ID: mdl-35683041

ABSTRACT

In recent years, on the basis of FSP/FSW technologies, a number of new solutions, methods and variants have been developed, constituting not only proof of the continuous evolution of FSP/FSW technologies, but also of the huge scientific and application potential hidden in these methods [...].

3.
Materials (Basel) ; 14(11)2021 Jun 05.
Article in English | MEDLINE | ID: mdl-34198918

ABSTRACT

This study focuses on the properties and process parameters dictating behavioural aspects of friction stir welded Aluminium Alloy AA6061 metal matrix composites reinforced with varying percentages of SiC and B4C. The joint properties in terms of mechanical strength, microstructural integrity and quality were examined. The weld reveals grain refinement and uniform distribution of reinforced particles in the joint region leading to improved strength compared to other joints of varying base material compositions. The tensile properties of the friction stir welded Al-MMCs improved after reinforcement with SiC and B4C. The maximum ultimate tensile stress was around 172.8 ± 1.9 MPa for composite with 10% SiC and 3% B4C reinforcement. The percentage elongation decreased as the percentage of SiC decreases and B4C increases. The hardness of the Al-MMCs improved considerably by adding reinforcement and subsequent thermal action during the FSW process, indicating an optimal increase as it eliminates brittleness. It was seen that higher SiC content contributes to higher strength, improved wear properties and hardness. The wear rate was as high as 12 ± 0.9 g/s for 10% SiC reinforcement and 30 N load. The wear rate reduced for lower values of load and increased with B4C reinforcement. The microstructural examination at the joints reveals the flow of plasticized metal from advancing to the retreating side. The formation of onion rings in the weld zone was due to the cylindrical FSW rotating tool material impression during the stirring action. Alterations in chemical properties are negligible, thereby retaining the original characteristics of the materials post welding. No major cracks or pores were observed during the non-destructive testing process that established good quality of the weld. The results are indicated improvement in mechanical and microstructural properties of the weld.

4.
Polymers (Basel) ; 13(9)2021 Apr 22.
Article in English | MEDLINE | ID: mdl-33922169

ABSTRACT

In recent times, demand for light weight and high strength materials fabricated from natural fibres has increased tremendously. The use of natural fibres has rapidly increased due to their high availability, low density, and renewable capability over synthetic fibre. Natural leaf fibres are easy to extract from the plant (retting process is easy), which offers high stiffness, less energy consumption, less health risk, environment friendly, and better insulation property than the synthetic fibre-based composite. Natural leaf fibre composites have low machining wear with low cost and excellent performance in engineering applications, and hence established as superior reinforcing materials compared to other plant fibres. In this review, the physical and mechanical properties of different natural leaf fibre-based composites are addressed. The influences of fibre loading and fibre length on mechanical properties are discussed for different matrices-based composite materials. The surface modifications of natural fibre also play a crucial role in improving physical and mechanical properties regarding composite materials due to improved fibre/matrix adhesion. Additionally, the present review also deals with the effect of silane-treated leaf fibre-reinforced thermoset composite, which play an important role in enhancing the mechanical and physical properties of the composites.

5.
Materials (Basel) ; 14(9)2021 Apr 23.
Article in English | MEDLINE | ID: mdl-33922471

ABSTRACT

In this work, aluminium alloy ADC12 reinforced with various amounts of ZrB2 (0 wt.%, 3 wt.%, 6 wt.%, 9 wt.%) were synthesized by an in-situ reaction of molten aluminium with inorganic salts K2ZrF6 & KBF4. XRD, EDAX, and SEM techniques are used for the characterization of the fabricated composite. XRD analysis revealed the successful in situ formation of ZrB2 in the composite. From the SEM images, it was concluded that the distribution of reinforcement was homogeneous in the composites. A study of mechanical and tribological properties under the dry sliding condition of ZrB2-reinforced ADC12 alloy has also been carried out. It is seen that there is an increase in tensile strength by 18.8%, hardness by 64.2%, and an increase in wear resistance of the material after reinforcement. The ductility of the material decreased considerably with an increase in the amount of reinforcement. The composite's impact strength decreased by 27.7% because of the addition of hard ZrB2 particulates.

6.
Materials (Basel) ; 14(4)2021 Feb 19.
Article in English | MEDLINE | ID: mdl-33669892

ABSTRACT

In this investigation, the extensive wear behaviour of materials was studied using SiC reinforced magnesium alloy composites fabricated through the stir casting process. The wear properties of AZ91 alloy composites with a small variation (i.e., 3%, 6%, 9% and 12%) of SiC particulates were evaluated by varying the normal load with sliding velocity and sliding distance. The worn surfaces were examined by scanning electron microscope to predict the different wear mechanisms on the pin while sliding on the hard disk in the dry sliding wear test condition. The microhardness of the SiC reinforced AZ91 composites was found to be more than the un-reinforced AZ91 alloy. Pins tested at load 19.62 N, and 2.6 m/s exhibited a series of short cracks nearly perpendicular to the sliding direction. At higher speed and load, the oxidation and delamination were observed to be fully converted into adhesion wear. Abrasion, oxidation, and delamination wear mechanisms were generally dominant in lower sliding velocity and lower load region, while adhesion and thermal softening/melting were dominant in higher sliding velocity and loads. The wear rate and coefficient of friction of the SiC reinforced composites were lower than that of the unreinforced alloy. This is due to the fact of higher hardness exhibited by the composites. The wear behaviour at the velocity of 1.39 m/s was dominated by oxidation and delamination wear, whereas at the velocity of 2.6 m/s the wear behaviour was dominated by abrasion and adhesion wear. It was also found that the plastic deformation and smearing occurred at higher load and sliding velocity.

7.
Materials (Basel) ; 13(23)2020 Nov 27.
Article in English | MEDLINE | ID: mdl-33260868

ABSTRACT

In this study, experiments are performed to study the physical and mechanical behaviour of chemically-treated sugarcane bagasse fibre-reinforced epoxy composite. The effect of alkali treatment, fibre varieties, and fibre lengths on physical and mechanical properties of the composites is studied. To study the morphology of the fractured composites, scanning electron microscopy is performed over fractured composite surfaces. The study found that the variety and lengths of fibres significantly influence the physical and mechanical properties of the sugarcane bagasse-reinforced composites. From the wear study, it is found that the composite fabricated from smaller fibre lengths show low wear. The chemically-treated bagasse-reinforced composites fabricated in this study show good physical and mechanical properties and are, therefore, proposed for use in applications in place of conventional natural fibres.

8.
Materials (Basel) ; 13(24)2020 Dec 11.
Article in English | MEDLINE | ID: mdl-33322502

ABSTRACT

In this paper, the experimental investigation results of the bead sequence input on geometry, structure, and hardness of surfaced layers after multi-pass weld surfacing are analyzed. Three S355 steel plates surfaced by GMAW (Gas Metal Arc Welding) were tested with three different combinations of six beads. The geometric, structural, and hardness analysis was carried out in the cross-section of the plates in the middle of the welded layers. The dimensions of padded layers, fusion and heat-affected zone, as well as the individual padded weld were evaluated. On the basis of metallographic samples, qualitative and quantitative structure analysis was performed. Hardness measurements in surfacing welds and heat-affected zones in the tested cross-sections of the surfacing layers were carried out. A comparative analysis of structure and hardness, taking into account the thermal implications of the bead sequence, allowed for the formulation of conclusions. Comparative studies have shown differences in properties between heat-affected zones (HAZ) for individual surfacing sequences. These differences were mainly in the dimensions of the surfacing layers, the share of structural components, as well as the uniformity of hardness distributions. Finally, the most favorable sequence in terms of structure and hardness distribution, maximum hardness, and range of hardness has been indicated.

9.
Materials (Basel) ; 13(21)2020 Oct 31.
Article in English | MEDLINE | ID: mdl-33142936

ABSTRACT

In this study, the processing of SiC particulate-strengthened magnesium alloy metal matrix composites via vacuum supported inert atmosphere stir casting process is presented. The effects of small variations in the SiC particulate (average size 20 µm) reinforcement in magnesium alloy AZ91 were examined. It was found that with the addition of SiC particulate reinforcement, the hardness improved considerably, while the ultimate tensile and yield strength improved slightly. The density and porosity of the magnesium alloy-based composites increased with the increase in the wt.% of SiC particulates. The tensile and compressive fracture study of the fabricated composites was also performed. The tensile fractures were shown to be mixed-mode fractures (i.e., ductile and cleavage). The fractured surface also disclosed tiny dimples, micro-crack, and cleavage fractures which increases with increasing reinforcement. For the compression fracture, the surface microstructural studies of AZ91 displayed major shear failure and demonstrated the greater shear bands when compared to AZ91/SiC composites, which instead revealed rough fracture surfaces with mixed-mode brittle and shear features.

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