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J Vis Exp ; (81)2013 Nov 27.
Article in English | MEDLINE | ID: mdl-24327099

ABSTRACT

Procedures utilizing millifluidic devices for chemical synthesis and time-resolved mechanistic studies are described by taking three examples. In the first, synthesis of ultra-small copper nanoclusters is described. The second example provides their utility for investigating time resolved kinetics of chemical reactions by analyzing gold nanoparticle formation using in situ X-ray absorption spectroscopy. The final example demonstrates continuous flow catalysis of reactions inside millifluidic channel coated with nanostructured catalyst.


Subject(s)
Copper/chemistry , Gold/chemistry , Metal Nanoparticles/chemistry , Microfluidic Analytical Techniques/instrumentation , Microfluidic Analytical Techniques/methods , Kinetics , Lab-On-A-Chip Devices , Nanotechnology/instrumentation , Nanotechnology/methods
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