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1.
Acta Crystallogr Sect E Struct Rep Online ; 68(Pt 9): o2750, 2012 Sep 01.
Article in English | MEDLINE | ID: mdl-22969633

ABSTRACT

In the title compound, C(16)H(11)F(3)O, the dihedral angle between the two rings is 48.8 (2)°. The crystal packing exhibits no classical inter-molecular inter-actions between the mol-ecules.

2.
Acta Crystallogr Sect E Struct Rep Online ; 68(Pt 6): m847-8, 2012 Jun 01.
Article in English | MEDLINE | ID: mdl-22719384

ABSTRACT

In the dinuclear title compound, [Na(2)(C(13)H(15)ClN(5)O(5)S)(2)(H(2)O)(6)](n), two Na(+) cations, disposed about a centre of inversion, are linked by two bridging water mol-ecules. The coordination geometry is based on an O(5) donor set defined by four water mol-ecules and a 4-amino-benzene-sulfonate O atom in a distorted trigonal-bipyramidal geometry. In the crystal, significant O-H⋯O, O-H⋯N and N-H⋯O hydrogen bonds lead to the formation of a three-dimensional architecture.

3.
Acta Crystallogr Sect E Struct Rep Online ; 68(Pt 6): o1742, 2012 Jun 01.
Article in English | MEDLINE | ID: mdl-22719527

ABSTRACT

In the title compound, C(15)H(13)NO(3), the dihedral angle between the two aromatic rings is 79.25 (16)°.

4.
Acta Crystallogr Sect E Struct Rep Online ; 68(Pt 2): o388, 2012 Feb 01.
Article in English | MEDLINE | ID: mdl-22347010

ABSTRACT

The asymmetric unit of the title compound, C(14)H(11)NS, contains two mol-ecules in which the dihedral angles between the phenyl rings are 77.23 (7) and 86.30 (7)°. No aromatic π-π stacking inter-actions are observed.

5.
Acta Crystallogr Sect E Struct Rep Online ; 67(Pt 12): o3505, 2011 Dec 01.
Article in English | MEDLINE | ID: mdl-22199975

ABSTRACT

In the title compound, C(8)H(6)BrNO(2), the dihedral angle between the planes of the benzene ring and the nitro group is 22.99 (12)°. In the crystal, inversion dimers associated by pairs of short Br⋯O contacts [3.2319 (17) Å] occur.

6.
Acta Crystallogr Sect E Struct Rep Online ; 67(Pt 11): o2861, 2011 Nov.
Article in English | MEDLINE | ID: mdl-22219901

ABSTRACT

The complete mol-ecule of the title compound, C(12)H(10)ClO(2)PS, is generated by crystallographic mirror symmetry, with the P, S and Cl atoms lying on the mirror plane. The resulting PO(2)SCl tetra-hedron is significantly distorted [O-P-O = 96.79 (9)°]. The crystal packing exhibits no directional inter-actions.

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