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[Determination of scopolamine in the poisoning case by GC/MS].
Chu, Jian-Xin; Xie, Yu; Zhuo, Xiao-Cong.
Fa Yi Xue Za Zhi ; 22(4): 285-7, 2006 Aug 15.
Article in Chinese | MEDLINE | ID: mdl-17080669

ABSTRACT

OBJECTIVE: To separate and determine scopolamine from the food in a poisoning case by GC/MS. METHODS: The scopolamine was determined by GC/MS/El used CP5860(CP-sil8CB) column (30 mx 0.25 mmx 0.33 microm) with liquid- liquid extraction. RESULTS: The deny scopolamine was found in the case sample, and the chromatographic separation of the peaks is fine. CONCLUSION: The method is accurate and reliable.


Subject(s)
Foodborne Diseases/etiology , Forensic Medicine/methods , Gas Chromatography-Mass Spectrometry/methods , Scopolamine/analysis , Scopolamine/poisoning , Hallucinations/chemically induced , Hallucinations/diagnosis , Humans , Male , Psychoses, Substance-Induced/diagnosis , Psychoses, Substance-Induced/etiology , Scopolamine/chemistry , Sensitivity and Specificity , Solanaceae/chemistry , Solvents/chemistry
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