Fracture resistance of pressed ZLS crowns versus pressed LD crowns under thermo-mechanical cycling

Resumo Este estudo teve como objetivo avaliar a resistência à fractura do silicato de lítio reforçado com zircônio todo o material cerâmico "Celtra Press" em comparação com um "IPS e-max Press" em condições orais simuladas. Quatorze coroas cerâmicas foram fabricadas em moldes epóxi que foram duplicados a partir de moldes principais de aço inoxidável e divididos em dois grupos iguais (n=7) de acordo com o material de construção; Grupo A: Coroas fabricadas com material IPS e-max Press e Grupo B: Coroas fabricadas com material Celtra Press. As coroas foram então cimentadas nos seus moldes correspondentes com um cimento de resina auto-adesivo e submetidas a ciclos térmicos e cargas cíclicas. Em seguida, foram carregadas para fraturar numa máquina universal de ensaios. Os resultados foram tabulados e analisados estatisticamente utilizando os testes Kolmogorov-Smirnov e Shapiro-Wilk. O teste t de Student usado para comparar os valores médios. O nível de significância foi fixado em P ≤ 0,05 e intervalo de confiança de 95%. A análise estatística foi realizada utilizando o software Graph Pad Instat (Graph Pad, Inc.) para Windows. Os valores médios ± SD da resistência à fractura foram registados para o grupo Disilicate de lítio (1706,01 ±154,32 N) enquanto que os valores médios ± SD registados com o grupo celtra foram (1550,67±196,71 N). As coroas cerâmicas de silicato de lítio reforçado com zircónio produziram valores de resistência à fractura comparáveis aos das coroas cerâmicas de dissilicato de lítio e ambos os materiais testados estão dentro dos valores clinicamente aceitáveis na área posterior.

Abstract The aim of this study was conducted to assess the fracture resistance of zirconia reinforced lithium silicate all ceramic material "Celtra Press" compared to lithium disilicate one "IPS e-max Press" under simulated oral conditions. Fourteen ceramic crowns were fabricated on epoxy dies which were duplicated from stainless steel master die and divided into two equal groups (n=7) according to the material of construction; Group A: Crowns fabricated with IPS e-max Press material and Group B: Crowns fabricated with Celtra Press material. The crowns were then cemented onto their corresponding dies with a self-adhesive resin cement and subjected to thermocycling and cyclic loading. Then they were loaded to fractur in a universal testing machine. The results were tabulated and statistically analyzed using Kolmogorov-Smirnov and Shapiro-Wilk tests. Student t-test used to compare mean values. The significance level was set at P ≤ 0.05 and 95% Confidence interval. Statistical analysis was performed using Graph Pad Instat (Graph Pad, Inc.) software for windows. The mean ± SD values of fracture resistance were recorded for lithium Disilicate group (1706.01 ±154.32 N) meanwhile the mean ± SD value recorded with celtra group were (1550.67±196.71 N). Zirconia reinforced lithium silicate ceramic crowns produced comparable fracture resistance values to lithium disilicate ceramic crowns and both tested materials are within the clinically acceptable values in the posterior area.

Biomechanical Cadaveric Evaluation of the Role of Medial Column Instability in Hallux Valgus Deformity.

BACKGROUND: Medial column instability is a frequent finding in patients with flatfeet and hallux valgus, within others. The etiology of hallux valgus is multifactorial, and medial ray axial rotation has been mentioned as having an individual role. Our objective was to design a novel cadaveric foot model where we could re-create through progressive medial column ligament damage some components of a hallux valgus deformity. METHODS: Ten fresh-frozen lower leg specimens were used, and fluorescent markers were attached in a multisegment foot model. Constant axial load and cyclic tibial rotation (to simulate foot pronation) were applied, including pull on the flexor hallucis longus tendon (FHL). We first damaged the intercuneiform (C1-C2) ligaments, second the naviculocuneiform (NC) ligaments, and third the first tarsometatarsal ligaments, leaving the plantar ligaments unharmed. Bony axial and coronal alignment was measured after each ligament damage. Statistical analysis was performed. RESULTS: A significant increase in pronation of multiple segments was observed after sectioning the NC ligaments. Damaging the tarsometatarsal ligament generated small supination and varus changes mainly in the medial ray. No significant change was observed in axial or frontal plane alignment after damaging the C1-C2 ligaments. The FHL pull exerted a small valgus change in segments of the first ray. DISCUSSION: In this biomechanical cadaveric model, the naviculocuneiform joint was the most important one responsible for pronation of the medial column. Bone pronation occurs along the whole medial column, not isolated to a certain joint. Flexor hallucis longus pull appears to play some role in frontal plane alignment, but not in bone rotation. This model will be of great help to further study medial column instability as one of the factors influencing medial column pronation and its relevance in pathologies like hallux valgus. CLINICAL RELEVANCE: This cadaveric model suggests a possible influence of medial column instability in first metatarsal pronation. With a thorough understanding of a condition's origin, better treatment strategies can be developed.

Comparing Torque Loss in Standard Implants and Short Implants with Increased Vertical Cantilever Abutments: an In Vitro Study / Comparação da perda de torque em implantes padrão e implantes curtos com pilares cantilever verticais aumentados (in vitro)

Objectives: With regard to the prevalence of abutment screw loosening (SL) and bone height reduction, particularly in the posterior regions of the jaws, as well as the contradictory issue of applying short implants instead of surgeries, along with all preparations associated with longer implants, the present study aimed to compare the amount of torque loss in short implants with increased vertical cantilever abutments and standard ones. Material and Methods: In this experimental study, a total number of 20 implants (MegaGen Implant Co., Ltd, South Korea) with 4.5 mm diameter including 10 short implants (7 mm) and 10 standard ones (10 mm) were utilized. Using a surveyor, fixtures were perpendicularly mounted in 13×34 mm resin for short implants and 19×34 mm resin for standard ones. The abutments of the same height but different cuff heights (2.5 mm for the standard implants and 5.5 mm for the short ones) were then tightened with 30 N.cm, via a digital torque meter. To compensate the settling effect, the abutment screw was re-tightened with 30 N.cm after 10 min. Upon applying 500,000 cycles at 75 N.cm and 1 Hz along the longitudinal axis on each sample, blind reverse torque value (RTV) was measured with a digital torque meter. The data were finally analyzed using Student's t-test. Results:Both groups experienced torque loss, but there was no statistically significant difference between the case and control groups in terms of abutment SL (p = 0451). Conclusion: Short implants seem to be a good mechanical alternative in emergencies with respect to torque loss and abutment SL. (AU)

Objetivos: Considerando a prevalência de afrouxamento de parafuso dos pilares, redução da altura óssea especialmente nas regiões posteriores, a questão contraditória da aplicação de implantes curtos em vez de cirurgias e todos os preparos associados a implantes mais longos, este estudo buscou comparar implantes curtos com pilares cantilever verticais aumentados e implantes padrão na quantidade de perda de torque. Material e métodos: Neste estudo experimental, foram utilizados 20 implantes (Megagen, Coreia do Sul) com diâmetro de 4,5 mm, incluindo 10 implantes curtos (7 mm) e 10 implantes padrão (10 mm). A fixação foi realizada perpendicularmente em uma resina 13 × 34 mm para implantes curtos e uma resina 19 × 34 mm para implantes padrão, usando um topógrafo. Os pilares da mesma altura, mas com diferentes comprimentos de manguito (2,5 mm para os implantes padrão e 5,5 mm para os implantes curtos) foram apertados com 30 N, utilizando um torquímetro digital. Para compensar o efeito de sedimentação, o parafuso do pilar foi reapertado com 30 N após 10 min. Depois de aplicar 500.000 ciclos a 75 N e 1 Hz ao longo do eixo longitudinal em cada amostra, o valor de torque reverso cego foi medido com um medidor de torque digital. Os dados foram analisados pelo teste t de Student. Resultados: Todos os grupos tiveram perda de torque, mas não houve diferença estatisticamente significativa entre os grupos caso e controle em termos de afrouxamento do parafuso do pilar (p = 0451). Conclusão: Os implantes curtos parecem ser uma boa alternativa mecânica em emergências em termos de perda de torque e afrouxamento do parafuso do pilar. (AU)

Shaking Table Test of U-Shaped Walls Made of Fiber-Reinforced Foamed Concrete.

Fiber-reinforced foamed concrete (FRFC) is a lightweight material that has the potential to perform well in seismic applications due to its low density and improved mechanical properties. However, studies focused on the seismic assessment of this material are limited. In this work, U-shaped wall specimens, made of FRFC reinforced with henequen fibers and plain foamed concrete (PFC) with a density of 900 kg/m3, were subjected to shaking table tests. PFC and FRFC were characterized using compression and tension tests. FRFC exhibited enhanced mechanical properties, which were attributed to the fibers. The dynamic tests showed that U-shaped walls made of FRFC performed better than those made of PFC. The time period prior to the collapse of the FRFC U-shaped walls was longer than that of the PFC specimens, which was attributed to the enhanced specimen integrity by the fibers. Finite element simulations of the shaking table test allowed for the prediction of the stress concentration and plastic strain that may lead to the failure of the U-shaped wall. These results showed that U-shaped walls made of FRFC have the potential to perform well in seismic applications, however, these results are preliminary and further studies are needed to support the findings of this work.

Influence of CAD/CAM Material and Preparation Design on the Long-term Fracture Resistance of Endocrowns Restoring Maxillary Premolars / Influência do material de CAD / CAM e tipo de preparo na resistência à fratura a longo prazo de coroas endodônticas adesivas na restauração de pré-molares superiores

Objective: To evaluate the effect of different occlusal preparation designs and CAD/CAM materials on the fracture resistance of maxillary premolars end crowns. Materials and Methods: sixty-four endodontically treated upper first premolars were randomly divided into four groups according to ceramic materials (Vita Enamic and IPS emax CAD) and occlusal preparation designs (Anatomical and horizontal butt joint). After teeth preparation, the restorations were all made by CAD/CAM system (Cerec MCXL). Half of each group had undergone cyclic fatigue testing of 105 cycles with 50N loading force at a frequency of 0.5Hz in a mechatronic chewing simulator machine, and then all samples were loaded to fracture using a universal testing machine with a cross head speed of 0.5 mm/min recording the fracture resistance values in N . The specimens were measured and statistically analyzed using using three-way analyses of variance (ANOVA), followed by serial two-way and one-way ANOVAs at each level of the study. P-values were adjusted for multiple comparisons using BENFORRONI correction and the significance level was set at P ≤ 0.05 for all tests. Results: Vita Enamic endocrowns showed higher fracture resistance values than IPS e max specimens. Conclusions: Vita Enamic endocrowns with anatomical preparations were found to be more favourable restoring endodontically treated maxillary premolars (AU)

Objetivo: Avaliar o efeito de diferentes tipos de preparo oclusal e materiais CAD/CAM na resistência à fratura de coroas endodônticas adesivas em pré-molares. Materiais e Métodos: Sessenta e quatro primeiros pré-molares superiores tratados endodonticamente foram divididos randomicamente em quatro grupos de acordo com os materiais cerâmicos (Vita Enamic e IPS emax CAD) e tipos de preparo oclusal (Recobrimento Incisal Anatômico e Horizontal). Após o preparo dental, as restaurações foram confeccionadas pelo sistema CAD/CAM (Cerec MCXL). Metade de cada grupo foi submetido a testes de fadiga cíclica de 105 ciclos com força de carga de 50N a uma frequência de 0,5Hz em uma máquina simuladora de mastigação mecatrônica, e então todas as amostras foram submetidas a fratura por uma máquina de teste universal com uma velocidade de 0,5 mm / min registrando os valores de resistência à fratura em N. As amostras foram medidas e analisadas estatisticamente usando análises de variância de três fatores (ANOVA), seguidas por ANOVAs de dois fatores e de um fator em cada nível do estudo. Os valores de p foram ajustados para comparações múltiplas usando a correção BENFORRONI e o nível de significância estabelecido foi de P ≤ 0,05 para todos os testes. Resultados: Coroas endodônticas adesivas da Vita Enamic mostraram maiores valores de resistência à fratura do que as amostras de IPS emax. Conclusões: Verificou-se que as coroas endodônticas adesivas da Vita Enamic com preparos com recobrimento incisal anatômico foram mais favoráveis para restaurar os pré-molares superiores tratados endodonticamente (AU)

Fracture load of nano-ceramic composite material for anterior endocrown restorations / Carga de fratura de material compósito nano-cerâmico para restaurações endocrown anteriores

Objective: to evaluate ability of Nano Ceramic Composite endocrown to withstand occlusal forces when used in the anterior region. Material and Methods: eighty endodontically treated maxillary central incisors teeth were randomly divided into two main groups according to the restoration type. Forty of these teeth were post, core and crown restorations and 40 were endocrown restorations. Then they were divided by halves into two subgroups according to the material used 20 were made with Lava Ultimate and the other 20 with IPS e.max. Each subgroup was then further subdivided into two divisions according to the remaining tooth structure above the CEJ (n = 10): 2 mm and 0.5 mm above the CEJ. After teeth preparation, the restorations were all made by CAD/CAM system (Cerec MCXL). All samples had undergone cyclic fatigue testing, and then loaded to fracture using a universal testing machine. The specimens were measured and statistically analyzed using Mann-Whitney test for comparing the mean changes between the groups. Results: Lava Ultimate showed higher mean fracture load values than IPS e.max specimens. Conclusions: endocrowns were found to be more favorable when used on endodontically treated teeth than the conventional post, core and crown restorations.(AU)

Objetivo: Avaliar a capacidade do compósito nanocerâmico endocrown para suportar forças oclusais quando usado na região anterior. Material e Métodos: Oitenta incisivos centrais superiores tratados endodonticamente foram divididos aleatoriamente em dois grupos principais, de acordo com o tipo de restauração. Quarenta desses dentes receberam restaurações com retentor intrarradicular, núcleo e coroa e 40 receberam restaurações endocrown. Em seguida, foram divididos pela metade em dois subgrupos, de acordo com o material utilizado, sendo 20 confeccionados com Lava Ultimate e os demais 20 com IPS e.max. Cada subgrupo foi posteriormente subdividido em dois, de acordo com a estrutura dentária remanescente acima da JEC (n = 10): 2 mm e 0,5 mm acima do JEC. Após o preparo dos dentes, todas as restaurações foram realizadas pelo sistema CAD/ CAM (Cerec MCXL). Todas as amostras foram submetidas a testes de fadiga cíclica e submetidas ao esforço até a fratura em uma máquina universal de testes. As amostras foram medidas e analisadas estatisticamente pelo teste de MannWhitney para comparação das alterações médias entre os grupos. Resultados: lava Ultimate apresentaram valores médios mais altos de carga até a fratura do que as amostras IPS e.max. Conclusões: as endocrowns mostraram-se mais favoráveis quando utilizadas em dentes tratados endodonticamente do que as restaurações convencionais com retentor intrarradicular, núcleo e coroa.(AU)

Proximal and Distal Failure Site Analysis in Percutaneous Achilles Tendon Rupture Repair.

BACKGROUND: Different techniques have been described for percutaneous Achilles tendon rupture repair, but no biomechanical evaluation has been performed separately for proximal and distal suturing techniques. The purpose of this study was to biomechanically analyze proximal versus distal percutaneous Achilles suture configurations during cyclic loading and load to failure. METHODS: A simulated, midsubstance rupture was created 6 cm proximal to the calcaneal insertion in fresh-frozen cadaveric Achilles tendons. Fifteen proximal specimens were divided into 3 groups: (A1) triple locking technique, (A2) Bunnell-type technique, and (A3) double Bunnell-type technique. Twelve distal specimens were divided into 2 groups: (B1) triple nonlocking technique and (B2) oblique technique. Repairs were subjected to cyclic testing and load to failure. Load to failure, cause of failure, and tendon elongation were evaluated. RESULTS: None of the proximal specimens and 7/12 of the distal ones failed in cyclic testing. The proximal fixation groups demonstrated significantly more strength than the distal groups (P = .001), achieving up to 710 N of failure load in Group A3. Groups B1and B2 failed on average at 380 N with no difference between them (P > .05). The majority of all repairs failed in the suture-tendon interface. Distal groups had more elongation during cyclic testing (13.7 mm) than proximal groups (9.4 mm) (P = .02). CONCLUSION: The distal fixation site in this Achilles tendon repair was significantly weaker than the proximal fixation site. A proximal modified suture configuration increased resistance to cyclic loading and load to failure significantly. CLINICAL RELEVANCE: A modification can be suggested to improve strength of the Achilles repair.

Influence of aging on bond strength of artificial teeth to denture base acrylic resins

Aim: The aim of this study was to evaluate the bond strength of artificial teeth to different types of denture base resins when submitted to thermomechanical cycling (TMC). Methods: Sixty artificial mandibular first molars (Trilux, Vipi) were randomly divided into 3 groups according to denture base acrylic resins (Vipi Wave, Vipi Cril, and Vipi Cril Plus, Vipi). The teeth were fixed onto self-polymerizing acrylic resin bars (0.5 cm2 cross-section x 2 cm height), and the set was included in a metal flask using dental stone/silicone. After the dental stone was set, the bar was removed, and the denture base resin was packed and processed according to the group studied (Vipi Wave: 180 W/20 minutes + 540W/5 minutes; Vipi Cril and Vipi Cril Plus: Water bath at 74ºC for 9h). After polymerization, the samples were divided into 2 groups (n=10), according to the TMC treatment received (simulation of 5 years of mastication or not). The samples were submitted to tensile bond strength test (1 mm/min), and the data (MPa) were statistically analyzed (2-way ANOVA, Bonferroni, α=0.05). The fracture interfaces were evaluated using a stereomicroscope (50x). Results: The bond strength results showed no statistically significant difference (p>0.05) between the resins studied. TMC was significant (p<0.05), demonstrating lower values for the bond strength of artificial teeth to Vipi Cril Plus. The predominant fracture type was cohesive in resin. Conclusions: It was concluded that there is no difference in bond strength between artificial teeth and the resins used for denture base. However, TMC decreases the bond strength values of artificial teeth and crosslink thermo-polymerizable acrylic resin

Abutments with reduced diameter for both cement and screw retentions: analysis of failure modes and misfit of abutment-crown-connections after cyclic loading.

OBJECTIVE: The aim of this study was to analyze failure modes and misfit of abutments with reduced diameter for both cement and screw retentions after cyclic loading. MATERIAL AND METHODS: Forty morse-taper abutment/implant sets of titanium were divided into four groups (N = 10): G4.8S-4.8 abutment with screw-retained crown; G4.8C-4.8 abutment with cemented crown; G3.8S-3.8 abutment with screw-retained crown; and G3.8C-3.8 abutment with cemented crown. Copings were waxed on castable cylinders and cast by oxygen gas flame and injected by centrifugation. After, esthetic veneering ceramic was pressed on these copings for obtaining metalloceramic crowns of upper canine. Cemented crowns were cemented on abutments with provisional cement (Temp Bond NE), and screw-retained crowns were tightened to their abutments with torque recommended by manufacturer (10 N cm). The misfit was measured using a stereomicroscope in a 10× magnification before and after cyclic loading (300,000 cycles). Tests were visually monitored, and failures (decementation, screw loosening and fractures) were registered. Misfit was analyzed by mixed linear model while failure modes by chi-square test (α = 0.05). RESULTS: Cyclic loading affected misfit of 3.8C (P ≤ 0.0001), 3.8S (P = 0.0055) and 4.8C (P = 0.0318), but not of 4.8S (P = 0.1243). No differences were noted between 3.8S with 4.8S before (P = 0.1550) and after (P = 0.9861) cyclic loading, but 3.8C was different from 4.8C only after (P = 0.0015) loading. Comparing different types of retentions at the same diameter abutment, significant difference was noted before and after cyclic loading for 3.8 and 4.8 abutments. Analyzing failure modes, retrievable failures were present at 3.8S and 3.8C groups, while irretrievable were only present at 3.8S. CONCLUSIONS: The cyclic loading decreased misfit of cemented and screw-retained crowns on reduced diameter abutments, and misfit of cemented crowns is greater than screw-retained ones. Abutments of reduced diameter failed more than conventional.

Influence of Cyclic Fatigue in Water on Screw Torque Loss of Long-Span One-Piece Implant-Supported Zirconia Frameworks.

PURPOSE: It is still unclear whether four, six, or more implants should be used when restoring fully edentulous maxillae. This research evaluated the in vitro screw torque loss of zirconia frameworks supported by six implants and cantilevered zirconia frameworks supported by four implants. MATERIALS AND METHODS: Computer aided design/computer-assisted machining was used to fabricate 10 one-piece frameworks. Standardized pressable porcelain crowns were fabricated and luted to the frameworks. Specimens were divided into two groups (n = 5): AO4, cantilevered 12-unit full-arch fixed dental prosthesis supported by four implants; AO6, 14-unit supported by six implants. An opposing mandibular dental arch was fabricated with bis-acrylic composite resin. Specimens were submitted to 200 N underwater cyclic load at 2-Hz frequency for 1 × 106 cycles in a controlled 37°C temperature. A digital torque gauge assessed the initial and postload screw removal torque. Linear mixed-effects model was used for statistical analysis (α = 0.05). RESULTS: Significant screw torque loss was found for AO6 after cyclic loading (before: 36.20%/after: 52.82%; p < 0.05). Group AO6 (36.20%) presented lower preload loss before the cyclic loadings compared with AO4 (60.10%) (p < 0.05). CONCLUSIONS: Cyclic loading and lower implant-to-replaced-units ratio do not seem to compromise screw stability compared with higher implant-to-replaced-units ratio; however, a steep drop in preload was found before cyclic loading for both groups.

Influence of Liquid Lubrication on the Screw-Joint Stability of Y-TZP Implant Abutment Systems.

PURPOSE: To evaluate the effectiveness of abutment screws coated with liquid Vaseline on the screw-joint stability of yttria-stabilized tetragonal zirconia (Y-TZP) abutment systems. MATERIALS AND METHODS: Forty Y-TZP prefabricated abutments, 20 Neodent and 20 Bionnovation, were tightened to 20 Ncm on their respective external hexagon implants, and divided into four groups (n = 10) according to the screws: coated with Vaseline or uncoated. The removal torque (RT) value of the abutment screw was measured before and after loading. A cyclic loading (0.5 × 106 cycles; 15 Hz) between 11 and 211 N was applied. Means were compared using a repeated-measures ANOVA (α = 0.05). RESULTS: There was no significant difference between coated and uncoated screws (p = 0.822). Significant differences were found between the abutment systems (p < 0.001). There was a significant effect of cyclic loading (p < 0.001). CONCLUSIONS: Coated and uncoated screws presented similar effectiveness in maintaining preload. CLINICAL RELEVANCE: The liquid lubricant used in this study does not influence the stability of Y-TZP single-implant restorations.

Experimental primers containing synthetic and natural compounds reduce enzymatic activity at the dentin-adhesive interface under cyclic loading.

OBJECTIVE: To evaluate the effect of experimental primers (chlorhexidine, enriched mixture of proanthocyanidins, and doxycycline) on the adhesive properties and gelatinolytic activity at dentin-resin interfaces of occlusal Class I restorations. METHODS: The inactivation of enzymes by the experimental primers was assessed by fluorescence assay and gelatin zymography. To assess the adhesive properties, occlusal Class I cavities were prepared in sound human molars, etched with phosphoric acid and restored with one of the primers and an etch-and-rinse adhesive system (Adper Single Bond Plus-3M ESPE). After the restorative procedures, specimens were divided into two subgroups (n=6) consisting of storage in incubation buffer or axial cyclic loading at 50N and 1,000,000 cycles. Then, the specimens were sectioned and slices were assigned to in situ zymography assay and microtensile bond strength (TBS) test. RESULTS: Fluorescence assay and gelatin zymography revealed that the experimental primers inactivated rMMPs. In situ zymography (2-way ANOVA, Tukey, p<0.05) showed that cyclic loading increased the gelatinolytic activity at the resin-dentin interface and the experimental primers decreased the gelatinolytic activity at the adhesive interface. The experimental primers had no significant effects on dentin-adhesive bond strengths with or without cyclic loading (2-way ANOVA, p>0.05). SIGNIFICANCE: The use of experimental primers impaired the enzymatic activity at the dentin-adhesive interface after cyclic loading and the activity of rMMPs. Cyclic loading did not have a significant effect on the bond strength.

The effect of casting and masticatory simulation on strain and misfit of implant-supported metal frameworks.

The influence of casting and masticatory simulation on marginal misfit and strain in multiple implant-supported prostheses was evaluated. Three-unit screw retained fixed dental prosthesis (FDP) and screw retained full-arch fixed dental prosthesis (FAFDP) frameworks were made using calcinable or overcasted cylinders on conical dental implant abutment. Four groups were obtained according to the cylinder and prosthesis type (n=10). Frameworks were casted in CoCr alloy and subjected to strain gauge analyses and marginal misfit measurements before and after 10(6) mechanical cycles (2 Hz/280 N). Results were submitted to ANOVA, Tukey's HSD and Pearson correlation test (α=0.05). No difference was found on misfit among all groups and times (p>0.05). Overcasted frameworks showed higher strain than the calcinable ones (FDP - Initial p=0.0047; Final p=0.0004; FAFDP - Initial p=0.0476; Final p=0.0115). The masticatory simulation did not influence strain (p>0.05). No correlation was observed between strain and misfit (r=0.24; p>0.05). In conclusion, the marginal misfit value in the overcasted full-arch frameworks was higher than clinical acceptable data. It proved that overcasted method is not an ideal method for full-arch prosthesis. Overcasted frameworks generate higher strain upon the system. The masticatory simulation had no influence on misfit and strain of multiple prostheses.

Self-Sensing of Damage Progression in Unidirectional Multiscale Hierarchical Composites Subjected to Cyclic Tensile Loading.

The electrical sensitivity of glass fiber/multiwall carbon nanotube/vinyl ester hierarchical composites containing a tailored electrically-percolated network to self-sense accumulation of structural damage when subjected to cyclic tensile loading-unloading is investigated. The hierarchical composites were designed to contain two architectures differentiated by the location of the multiwall carbon nanotubes (MWCNTs), viz. MWCNTs deposited on the fibers and MWCNTs dispersed within the matrix. The changes in electrical resistance of the hierarchical composites are associated to their structural damage and correlated to acoustic emissions. The results show that such tailored hierarchical composites are able to self-sense damage onset and accumulation upon tensile loading-unloading cycles by means of their electrical response, and that the electrical response depends on the MWCNT location.

Influence of Cement Type and Relining Procedure on Push-Out Bond Strength of Fiber Posts after Cyclic Loading.

PURPOSE: The aim of this study was to evaluate the influence of cement type and relining procedure on push-out bond strength of fiber posts (FPs) after cyclic loading. MATERIALS AND METHODS: Forty bovine incisor roots were divided into four groups: group 1, FP luting with RelyX Unicem; group 2, FP relined with resin composite (FPC) luting with RelyX Unicem; group 3, FP luting with RelyX ARC; group 4, FPC luting with RelyX ARC. Afterwards, half the specimens were exposed to 250,000 cycles in a controlled chewing simulator. With the other half of the specimens in each group, the push-out test was performed 24 hours after FP luting (immediate groups). All roots were sectioned transversely, producing 1-mm-thick slices, and the push-out test was performed. Statistical analysis was performed using ANOVA and the Tukey test for post hoc comparisons (α = 0.05). RESULTS: FPC had higher bond strengths than FP (p < 0.05). RelyX Unicem showed higher bond strength than RelyX ARC (p < 0.05). Cyclic loading did not significantly affect the bond strength value (p > 0.05). CONCLUSION: The relining procedure and the cement type are important factors for the bond strength of FPs to root dentin.

Fit and Stability of Screw-Retained Implant-Supported Frameworks Under Masticatory Simulation: Influence of Cylinder Type.

PURPOSE: The aim of the study was to evaluate the effect of a prosthetic cylinder and casting on the misfit and loosening torque of screw-retained multiple-unit implant-supported dental prostheses under masticatory simulation. MATERIALS AND METHODS: Screw-retained, three-unit fixed dental prostheses (FDP) and screw-retained full-arch FDP frameworks were waxed using calcinable (plastic cylinders) or overcasted (premachined cast-on cylinders) on the dental implant abutments. The cylinders were cast in Co-Cr alloy to obtain four groups according to cylinder type and prosthesis type (n = 10). The screws were tightened with 20 N/cm (abutment) and 10 N/cm (prosthetic) torque according to the manufacturer's recommendation. After 24 hours, the initial loosening torque was analyzed. The initial misfit measurements were performed according to the Schiffleger test. The screws were retightened, and the specimens were submitted to 10(6) mechanical cycles (2 Hz/280 N). Loosening torque and misfit were reevaluated (final measurements), and data were submitted to ANOVA, Tukey's HSD, and Pearson's correlation tests (α = 0.05). RESULTS: The calcinable three-unit FDP demonstrated greater misfit (initial: 107.53 ± 40.36 µm; final: 99.00 ± 40.85 µm) than did the overcasted three-unit FDP frameworks (initial: 51.50 ± 22.98 µm; final: 44.33 ± 14.14 µm) (initial: p = 0.0005; final: p = 0.0007). No difference was noted between the calcinable and overcasted full-arch FDP frameworks (p > 0.05). Masticatory simulation did not affect the misfit (p > 0.05). The overcasted full-arch FDP presented a lower abutment screw loosening torque (12.05 ± 1.80 N/cm) than did the calcinable ones (14.75 ± 1.72 N/cm) in the final measurement (p = 0.0024). The calcinable groups presented a lower prosthetic screw loosening torque than did the overcasted groups in the final evaluation (p < 0.05). After masticatory simulation, the prosthetic screw loosening torque of the calcinable three-unit FDP decreased (initial: 5.49 ± 1.07 N/cm; final: 3.73 ± 1.15 N/cm; p = 0.0044). Correlation between misfit and loosening was observed only for the prosthetic screws (p < 0.05). CONCLUSIONS: The overcasted components provided a better fit in three-unit FDPs but did not influence the fit of full-arch FDPs. Prosthetic screws of overcasted frameworks presented higher stability, whereas masticatory simulation did not influence misfit but did reduce the prosthetic screw loosening torque of calcinable three-unit FDP frameworks.

Influência da deformação cíclica em torção na resistência à fadiga flexura dos instrumentos rotatórios de NiTi Hyflex CM, Typhoon CM e Vortex Blue / The influence of cyclic torcional straining on the flexural fatigue resistance of Hyflex CM, Typhoon CM and Vortex Blue rotary NiTi instruments

Os instrumentos rotatórios de NiTi são submetidos simultaneamente a tensões cíclicas flexurais e torcionais durante preparo de canais radiculares. As propriedades mecânicas destes instrumentos são afetadas por fatores como geometria, microestrutura, composição química da liga e tratamentos termomecânicos. Neste estudo avaliou-se a influência da deformação cíclica por torção na resistência à fadiga flexural de instrumentos Hyflex CM (HF; Coltene/ Whaladent Inc.), Typhoon CM, (TYP; Clinician´sChoice Dental Products,) e Vortex Blue (VB; Dentsply Tulsa Dental), calibre e taper 30/.06. Dez instrumentos novos de cada sistema foram ensaiados em um dispositivo de bancada para a determinação do número médio de ciclos até a fratura por fadiga (Nf), e outro grupo (n=10) foi submetido a um carregamento cíclico torcional de 20 ciclos contínuos de 0° a 180°. Após o carregamento, os instrumentos foram ensaiados até a ruptura por fadiga flexural nas mesmas condições que o controle. As superfícies longitudinais, bem como as superfícies de fratura por fadiga foram examinadas em microscópio eletrônico de varredura. Os resultados foram analisados pelo teste ANOVA (¿ = .05). Os instrumentos HF novos mostraram-se mais resistentes à fratura por fadiga (P < .05) seguidos por VB e TYP. Durante a ciclagem em torção, os instrumentos apresentaram redução no torque após o primeiro ciclo, com tendência à estabilização nos ciclos subsequentes. A maior queda nos valores médios de torque foi observada nos instrumentos TYP. Após o carregamento em torção, houve redução de 20%, 39% e 45% nos valores médios de Nf dos instrumentos HF, VB e TYP, respectivamente. Trincas longitudinais, decorrentes da ciclagem torcional não foram visualizadas em instrumentos CM (HF e TYP), apenas em VB. A superfície de fratura dos instrumentos HF mostrou maiores áreas de nucleação e crescimento lento de trincas. Os instrumentos avaliados, que envolvem tratamentos térmicos em sua fabricação, apresentaram comportamentos e possivelmente microestruturas distintas. Houve uma redução da resistência à fadiga após a deformação cíclica em todos os instrumentos avaliados

The NiTi rotary instruments undergo simultaneous flexural and torcional stresses during the root canal shaping. The mechanical properties of these instruments are influenced by many factors such as geometry, microstructure, chemical composition of the alloy and thermomechanical treatments. In this study, the influence of cyclic torsional straining on the fatigue resistance of different thermal treated instruments was assessed. Hyflex CM (HF; Coltene/ Whaladent Inc.), Typhoon CM, (TYP;Clinician´sChoice Dental Products,) e Vortex Blue (VB; Dentsply Tulsa Dental), size and taper 30/.06 were the instruments chosen, based on their geometry and specific characteristics of their manufacturing process. Ten new instruments for each system were tested in a bench test device to determine the mean value of the number of cycles to failure (Nf) of new instruments (GC, Control Group); another group (of 10instruments was submitted to 20 cycles of torsional straining between 0° and 180°. After the cyclic straining, the instruments (EG, Experimental Group) were submitted to fatigue until rupture under the same conditions of the control group. The longitudinal area and the fatigue fracture surfaces were examined by scanning electron microscopy (SEM). The results were analyzed by one-way analysis of variance ANOVA ( = .05). The new HF instruments displayed a higher resistance to fatigue (P < .05), followed by VB and TYP. During the torsional preloads, theinstruments exhibited a decrease in the torque values after the first cycle, with a tendency of stabilization in the following cycles. The lowest mean torque value was observed for the TYP instruments. After the torsional preloads, there was reduction of 20%, 39% and 45% of the mean Nf values for the instruments HF, VB and TYP, respectively. Longitudinal cracks, generated during the torsional preload were not observed in the CM instruments (HF and TYP), but were present in VB files. The instruments evaluated that involve a thermal treatment during its manufacturing, presented different mechanical behavior and possible distinct microstructure. There was a reduction in fatigue resistance after cyclic deformation in all instruments evaluated.Key words: Mechanical Torsion, Fatigue, Alloy, Instrumentation, CM instruments, Thermomechanical Treatment, Cyclic Loading

The influence of simulated clinical use on the flexibility of rotary ProTaper Universal, K3 and EndoSequence nickel-titanium instruments.

AIM: To investigate the influence of cyclic flexural and torsional loading on the flexibility of ProTaper Universal, K3 and EndoSequence nickel-titanium instruments, in view of the hypothesis that these types of loading would decrease the flexibility of the selected NiTi rotary files. METHODOLOGY: The instruments evaluated were S2 and F1 ProTaper Universal, sizes 20 and 25, .06 taper K3, and sizes 20 and 25, .06 taper EndoSequence. Flexibility was determined by 45° bending tests according to ISO 3630-1 specification. Values of the bending moment (MB ) obtained with new instruments were considered as the control group (CG). Bending tests were then conducted in instruments previously fatigued to one-fourth and three-fourths of their average fatigue life (fatigue groups, FG» and FG¾), as well as after cyclic torsional loading (torsional group, TG). Fatigue tests were carried out in a bench device that allowed the files to rotate freely inside an artificial canal with an angle of curvature of 45° and a radius of 5 mm. Cyclic torsional loading tests were performed that entailed rotating the instrument from zero angular deflection to 180° and then returning to zero applied torque in 20 cycles. Data were analysed using one-way analysis of variance at a significance level of 5%. RESULTS: Simulated clinical use by means of flexural fatigue tests did not affect the flexibility of the instruments, except for a significant increase in flexibility observed in a few instruments (P < 0.05). In addition, comparative statistical analyses between the values of MB measured in new instruments and after cyclic torsional loading showed no significant differences between them (P > 0.05). CONCLUSIONS: The flexibility of rotary ProTaper Universal, K3 and EndoSequence NiTi instruments, measured in bending tests, was not adversely affected by simulated clinical use in curved root canals.

Efeito da altura do pilar, de diferentes cimentos e das ciclagens térmica e mecânica sobre a resistência máxima à tração de infraestruturas metálicas cimentadas / Effect of abutment height, different cements, thermocycling and cyclic loading on the ultimate tensile strength of cement-retained/implant-supported cast restorations

Este estudo avaliou (1) o efeito da altura do pilar, dos diferentes cimentos e da termociclagem e (2) o efeito dos diferentes cimentos e da ciclagem mecânica sobre a resistência máxima à tração (RMT) de restaurações implantossuportadas cimentadas. Pilares de titânio (UCLA), com alturas de 4,0 e 6,0 mm (1), ou 4,0 mm (2), foram torqueados com 32 N.cm a análogos de implantes HI. Infraestruturas em Co-Cr, jateadas com óxido de alumínio 50 µm foram cimentadas com: Fosfato de Zinco- FZ; RelyX Luting 2- RXL2; C & B Cement- C&B; RelyX U100- RXU100 e RelyX Temp NE- RXTNE. Os conjuntos foram submetidos aos ensaios de tração (0,5 mm/min) após: 1- armazenagem em saliva artificial a 37 ºC durante 24 h (controle), 2- termociclagem (10.000 ciclos, 5,0 e 55 °C, 30 s de imersão), ou 3-ciclagem mecânica (106 ciclos, 140 N, 15 Hz). Os dados foram analisados por (1) 3-way ANOVA e Dunnett, e (2) 2-way ANOVA e Tukey HSD (α=0,05). Independentemente da altura do pilar, não houve diferença nos resultados dos grupos sem termociclagem (p≥0,05). Após termociclagem, houve aumento (p<0,05) na RMT nos pilares de 6,0 mm. Após ciclagem mecânica, houve diminuição (p<0,05) nos resultados de RMT produzidos por RXL2. A altura do pilar influenciou os resultados do RXL2, que produziu RMT mais elevada com os pilares de 6,0 mm. Com exceção do RXL2, a ciclagem mecânica não comprometeu a RMT das infraestruturas cimentadas. Em determinadas condições, o RXTNE produziu RMT semelhante à alguns cimentos finais

This study evaluate (1) the effect of abutment height, different cements and thermocycling, and (2) the effect of different cements and cyclic loading on the ultimate tensile strength (UTS) of cement-retained/implant-supported cast restorations. UCLA-type abutments with 4.0 and 6.0-mm height (1), or 4.0-mm height (2) were torqued to with 32 N.cm to internal hexagon dental implant replicas. Copings casted in Co-Cr, sandblasted with 50-µm aluminum oxide particles were cemented with: Zinc Phosphate- ZP; RelyX Luting 2- RXL2; C & B Cement- C&B; RelyX U100-RXU100 and RelyX Temp NE- RXTNE. The assemblies were submitted to the tensile test (0.5 mm/min) after: 1- storage in artificial saliva at 37 °C for 24 h (control), 2-thermocycling (10,000 cycles, 5.0 and 55 ºC, 30-s dwell time), or 3- cyclic loading (106 cycles, 140 N, 15 Hz). Data were analyzed by (1) 3-way ANOVA and Dunnett tests, and (2) 2-way ANOVA and Tukey HSD tests (α=0.05). Regardless of the abutments' heights, no significant differences were found among the UTS of the nonthermocycled groups (p≥0.05). After thermocycling, an increasing in the UTS was observed for the 6.0-mm abutments (p<0.05). After cyclic loading, the UTS values produced by RXL2 were decreased (p<0.05). The abutment's heights used affected the RXL2 results, which produced higher results with the 6.0-mm abutments. With the exception of RXL2, cyclic loading did not detrimentally affect the UTS of the cemented castings. In some conditions, the provisional cement RXTNE produced similar UTS to some definitive cements

Effect of cement type on microleakage of cast post-and-core systems under cyclic loading / Efeito do tipo de cimento na microinfiltração de núcleos metálicos fundidos submetidos à fadiga cíclica

Objective: The purpose of this study was to compare the microleakage of four cements in cast post-andcoresystems under cyclic loading. Materials and methods: Sixty-four human premolars were sectionedat the cement-enamel junction, endodontically treated, and divided into four groups (n = 16). Cast postsand cores were fabricated for root segments and were cemented with zinc phosphate cement (Harvard),resin-modified glass ionomer (Fuji PLUS), dual-cured phosphate methacrylate resin cement (Panavia F),or a dual-cured resin cement (Variolink II). All specimens underwent thermal cycling for 1.500 cycleswith 5 °C and 55 °C, with a dwelling time of 12 seconds. Half of the specimens of each group were subjectedto cycling loading with 50 N at 1.2 Hz for 750,000 cycles. Specimens were then immersed in 5%basic fuchsin solution for 24 hours. Specimens were sectioned, visualized by stereomicroscope under40x magnification and scored for dye penetration. The ratio between the length of the interface and thelength of dye penetration was also determined. Microleakage differences between the four cements were analyzed by Kruskal-Wallis test, and the effect of fatigue was analyzed with Mann-Whitney nonparametrictest (α =.05). Results: No failures occurred during fatigue testing. The zinc phosphate cement showedsignificantly higher microleakage values compared to other cements under both unloaded and loadedconditions (p = .007 and p = .006). Fatigue significantly increased the microleakage in all groups (p < .05).Conclusions: The microleakage values for the resin cements and the resin-modified glass ionomer weresimilar and significantly less than those of zinc phosphate, irrespective of loading. Fatigue loading increasedthe microleakage values for all the cements.

Objetivo: O objetivo deste estudo foi comparar a microinfiltração de pinos e núcleos de preenchimento metálicoscimentados com quatro diferentes materiais. Materiais e Métodos: 64 pré-molares humanos foram seccionadosna junção cemento-esmalte, tratados endodonticamente e divididos em quatro grupos (n = 16). Pinos enúcleos metálicos fundidos foram fabricados e cimentados com cimento de fosfato de zinco (Harvard), cimentode ionômero de vidro modificado (Fuji Plus), cimento resinoso dual de metacrilato fosfato (Panavia F) e cimentoresinoso dual (Variolink II). Todos os espécimes foram submetidos à ciclagem térmica (1.500 ciclos a 5-55 °C, 12segundos de banho). Metade dos espécimes de cada grupo foi submetida a uma carga cíclica de 50 N a 1,2 Hz emum total de 750.000 ciclos. Após a ciclagem, os espécimes foram imersos em solução de fucsina básica 5% por24 horas, seccionados, visualizados sob aumento de 40x e ranqueados quanto à penetração do corante. A proporçãoentre o comprimento da interface e o comprimento da penetração do corante foi também determinada.As diferenças de infiltração entre os quatro cimentos foram analisadas por teste de Kruskal-Wallis e o efeito dafadiga foi analisado por teste não paramétrico de Mann-Whitney (α = 0,05). Resultados: Não ocorreram falhasdurante o teste de fadiga. O cimento de fosfato de zinco mostrou valores de infiltração significativamente maiorescomparados aos demais cimentos na ausência ou presença da fadiga (p = 0,007 e p = 0,006). A fadiga elevousignificativamente a microinfiltração em todos os grupos (p < 0,05). Conclusões: Os valores de microinfiltraçãopara os cimentos resinosos e para o cimento de ionômero de vidro modificado foram similares e inferiores àquelesdo cimento de fosfato de zinco, independente da aplicação do teste de fadiga. A fadiga elevou os valores de microinfiltraçãopara todos os cimentos.