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Chem Commun (Camb) ; 48(45): 5560-2, 2012 Jun 07.
Article in English | MEDLINE | ID: mdl-22540123

ABSTRACT

An efficient chemo-enzymatic process for construction of the α-linked disaccharide unit (GlcNAcα1-4Gal) found in gastric mucin has been developed. The process consists of a one-step preparation of a novel triazine type glycosyl donor in water and the subsequent transglycosylation to a galactose derivative catalysed by α-N-acetylglucosaminidase.


Subject(s)
Disaccharides/chemistry , Galactose/analogs & derivatives , Gastric Mucins/chemistry , Acetylglucosaminidase/metabolism , Bacteroides/enzymology , Disaccharides/chemical synthesis , Disaccharides/metabolism , Galactose/chemical synthesis , Galactose/metabolism , Gastric Mucins/chemical synthesis , Gastric Mucins/metabolism , Triazines/chemistry , Triazines/metabolism
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