Ribbons of superparamagnetic colloids in magnetic field.

While the aggregation process of superparamagnetic colloids in strong magnetic field is well known on short time since a few decades, recent theoretical works predicted an equilibrium state reached after a long time. In the present paper, we present experimental observations of this equilibrium state with a two-dimensional system and we compare our data with the predictions of a pre-existing model. Above a critical aggregation size, a deviation between the model and the experimental data is observed. This deviation is explained by the formation of ribbon-shaped aggregates. The ribbons are formed due to lateral aggregation of chains. An estimation of the magnetic energy for chains and ribbons shows that ribbons are stable structures when the number of magnetic grains is higher than N = 30 .

Bernal random loose packing through freeze-thaw cycling.

We study the effect of freeze-thaw cycling on the packing fraction of equal spheres immersed in water. The water located between the grains experiences a dilatation during freezing and a contraction during melting. After several cycles, the packing fraction converges to a particular value η(∞)=0.595 independently of its initial value η(0). This behavior is well reproduced by numerical simulations. Moreover, the numerical results allow one to analyze the packing structural configuration. With a Voronoï partition analysis, we show that the piles are fully random during the whole process and are characterized by two parameters: the average Voronoï volume µ(v) (related to the packing fraction η) and the standard deviation σ(v) of Voronoï volumes. The freeze-thaw driving modify the volume standard deviation σ(v) to converge to a particular disordered state with a packing fraction corresponding to the random loose packing fraction η(BRLP) obtained by Bernal during his pioneering experimental work. Therefore, freeze-thaw cycling is found to be a soft and spatially homogeneous driving method for disordered granular materials.

Sliding friction on wet and dry sand.

We show experimentally that the sliding friction on sand is greatly reduced by the addition of some-but not too much-water. The formation of capillary water bridges increases the shear modulus of the sand, which facilitates the sliding. Too much water, on the other hand, makes the capillary bridges coalesce, resulting in a decrease of the modulus; in this case, we observe that the friction coefficient increases again. Our results, therefore, show that the friction coefficient is directly related to the shear modulus; this has important repercussions for the transport of granular materials. In addition, the polydispersity of the sand is shown to also have a large effect on the friction coefficient.

Dissipation in quasistatically sheared wet and dry sand under confinement.

We investigated the stress-strain behavior of sand with and without small amounts of liquid under steady and oscillatory shear. Since dry sand has a lower shear modulus, one would expect it to deform more easily. Using a new technique to quasistatically push the sand through a tube with an enforced parabolic (Poiseuille-like) profile, we minimize the effect of avalanches and shear localization. We observe that the resistance against deformation of the wet (partially saturated) sand is much smaller than that of the dry sand, and that the latter dissipates more energy under flow. This is also observed in large-amplitude oscillatory shear measurements using a rotational rheometer, showing that the effect is robust and holds for different types of flow.