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2.
J AOAC Int ; 79(4): 976-80, 1996.
Artículo en Inglés | MEDLINE | ID: mdl-8757457

RESUMEN

The homogeneity of comminuted composites of 20 lb samples of apples, cabbage, and green beans containing field-incurred residues of p, p'-methoxychlor was studied to determine whether a 5 min comminution in a 40 qt vertical cutter mixer produces a homogeneous composite and whether the size of test portions used accurately represents the composite. Duplicate test portions of 100, 50, 25, 10, 5, and 2 g taken from each of 6 separate sections of the mixer were analyzed by standard pesticide residue methodology for p, p'-methoxychlor. Results of this study confirmed that comminution of fresh produce in a 40 qt vertical cutter mixer, according to instructions described in the U.S. Food and Drug Administration's Pesticide Analytical Manual, Volume I, Section 203B, produces a homogeneous composite. No significant differences were found in the data for the 3 crops taken from the 6 sections of the mixer. Test portion weights of 100, 50, and 25 g produced equivalent results for all 3 crops. Statistically significant differences were observed for cabbage at 2, 5, and 10 g and for green beans at 2 g.


Asunto(s)
Manipulación de Alimentos , Frutas/química , Insecticidas/análisis , Metoxicloro/análisis , Residuos de Plaguicidas/análisis , Verduras/química , Análisis de Varianza , Guías como Asunto , Insecticidas/metabolismo , Metoxicloro/metabolismo , Residuos de Plaguicidas/metabolismo , Control de Calidad , Estados Unidos , United States Food and Drug Administration
3.
J AOAC Int ; 79(1): 163-70, 1996.
Artículo en Inglés | MEDLINE | ID: mdl-8620105

RESUMEN

The Total Diet Studies conducted by the U.S. Food and Drug Administration (FDA) provide yearly information on levels of pesticide residues, contaminants, and nutrients in the food supply and diets of specific age-sex groups. They also identify trends and changes in the levels of these substances in the food supply and in diets over time. Results are useful in making policy decisions regarding the safety of the food supply, food additives, pesticide use, nutrient fortification, and food labeling. This paper provides information on studies performed by FDA from 1987 to 1993.


Asunto(s)
Dieta , Análisis de los Alimentos , United States Food and Drug Administration , Adolescente , Adulto , Anciano , Niño , Preescolar , Femenino , Ácido Fólico/análisis , Contaminación de Alimentos , Humanos , Lactante , Masculino , Persona de Mediana Edad , Residuos de Plaguicidas/análisis , Piridoxina/análisis , Radioisótopos/análisis , Estados Unidos
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