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1.
Materials (Basel) ; 12(9)2019 May 07.
Artículo en Inglés | MEDLINE | ID: mdl-31067683

RESUMEN

Using an electron beam melting (EBM) printing machine (Arcam A2X, Sweden), a matrix of 225 samples (15 rows and 15 columns) of Ti-6Al-4V was produced. The density of the specimens across the tray in the as-built condition was approximately 99.9% of the theoretical density of the alloy, ρT. Tensile strength, tensile elongation, and fatigue life were studied for the as-built samples. Location dependency of the mechanical properties along the build area was observed. Hot isostatic pressing (HIP) slightly increased the density to 99.99% of ρT but drastically improved the fatigue endurance and tensile elongation, probably due to the reduction in the size and the distribution of flaws. The microstructure of the as-built samples contained various defects (e.g., lack of fusion, porosity) that were not observed in the HIP-ed samples. HIP also reduced some of the location related variation in the mechanical properties values, observed in the as-printed condition.

2.
Nanotechnology ; 21(36): 365705, 2010 Sep 10.
Artículo en Inglés | MEDLINE | ID: mdl-20702934

RESUMEN

Inorganic layered materials can form hollow multilayered polyhedral nanoparticles. The size of these multi-wall quasi-spherical structures varies from 4 to 300 nm. These materials exhibit excellent tribological and wear-resisting properties. Measuring and evaluating the stiffness of individual nanoparticle is a non-trivial problem. The current paper presents an in situ technique for stiffness measurements of individual WS(2) nanoparticles which are 80 nm or larger using a high resolution scanning electron microscope (HRSEM). Conducting the experiments in the HRSEM allows elucidation of the compression failure strength and the elastic behavior of such nanoparticles under uniaxial compression.

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