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1.
Materials (Basel) ; 16(2)2023 Jan 08.
Artigo em Inglês | MEDLINE | ID: mdl-36676337

RESUMO

The aim of the article is to examine the workability of sintered powder material of aluminum alloy (Alumix 321) through severe plastic deformations under the conditions of the equal channel angular rolling (ECAR) process. Accordingly, the stress-strain analysis of the ECAR was carried out through a computer simulation using the finite element method (FEM) by Deform 3D software. Additionally, the formability of the ALUMIX 321 was investigated using the diametrical compression (DC) test, which was measured and analyzed by digital image correlation and finite element simulation. The relationship between failure mode and stress state in the ECAR process and the DC test was quantified using stress triaxiality and Lode angle parameter. It is concluded that the sintered powder material during the ECAR processing failure by a shearing fracture because in the fracture location the stress conditions were close to the pure shear (η and θ¯ ≈ 0). Moreover, the DC test revealed the potential role as the method of calibration of the fracture locus for stress conditions between the pure shear and the axial symmetry compression.

2.
Materials (Basel) ; 15(2)2022 Jan 06.
Artigo em Inglês | MEDLINE | ID: mdl-35057129

RESUMO

In this work, AA1070 aluminium alloy sheets are joined using TIG and MIG welding after three different edge preparations. Shearing, water jet and plasma-cut processes were used to cut sheets, subsequently welded using ER5356 and ER4043 filler metals for TIG and MIG, respectively. Mechanical properties of the obtained sheets were assessed through tensile tests obtaining a relation between sheet preparation and welding tightness. Micro-hardness measures were performed to evaluate the effects of both welding and cutting processes on the micro-hardness of the alloy, highlighting that TIG welding gives rise to inhomogeneous micro-hardness behaviour. After tensile tests, surface fractures were observed employing scanning electron microscopy to highlight the relation between tensile properties and edge preparations. Fractures show severe oxidation in the water jet cut specimens, ductile fractures and gas porosities.

3.
Materials (Basel) ; 14(22)2021 Nov 12.
Artigo em Inglês | MEDLINE | ID: mdl-34832247

RESUMO

During the past 50 years, the aim to reduce the eddy current losses in magnetic cores to a minimum led to the formulation of new materials starting from electrically insulated iron powders, today called Soft Magnetic Composites (SMC). Nowadays, this promising branch of materials is still held back by the mandatory tradeoff between energetic, electrical, magnetic, and mechanical performances. In most cases, the research activity focuses on the deposition of an insulating/binding layer, being one of the critical points in optimizing the final composite. This insulation usually is achieved by either inorganic or organic layer constituents. The main difference is the temperature limit since most inorganic materials typically withstand higher treatment temperatures. As a result, the literature shows many materials and process approaches, each one designed to meet a specific application. The present work summarizes the recent advances in state of the art, analyzing the relationship among material compositions and magnetic and mechanical properties. Each coating shows its own processing sets, which vary from simple mechanical mixing to advanced chemical methods to metallurgical treatments. From state of the art, Aluminum coatings are characterized by higher current losses and low mechanical properties. In contrast, higher mechanical properties are obtained by adopting Silicon coatings. The phosphates coatings show the best-balanced overall properties. Each coating type was thoroughly investigated and then compared with the literature background highlighting. The present paper thus represents a critical overview of the topic that could serve as a starting point for the design and development of new and high-performing coating solutions for SMCs. However, global research activity continuously refines the recipes, introducing new layer materials. The following steps and advances will determine whetherthese materials breakthrough in the market.

4.
Materials (Basel) ; 13(15)2020 Jul 27.
Artigo em Inglês | MEDLINE | ID: mdl-32726905

RESUMO

Additive manufacturing is a key enabling technology in the manufacture of highly complex shapes, having very few geometric limitations compared to traditional manufacturing processes. The present paper aims at investigating mechanical properties at cryogenic temperatures for a 316L austenitic stainless steel, due to the wide possible cryogenic applications such as liquid gas confinement or superconductors. The starting powders have been processed by laser powder bed fusion (LPBF) and tested in the as-built conditions and after stress relieving treatments. Mechanical properties at 298, 77 and 4.2 K from tensile testing are presented together with fracture surfaces investigated by field emission scanning electron microscopy. The results show that high tensile strength at cryogenic temperature is characteristic for all samples, with ultimate tensile strength as high as 1246 MPa at 4.2 K and 55% maximum total elongation at 77 K. This study can constitute a solid basis for investigating 316L components by LPBF for specific applications in cryogenic conditions.

5.
Materials (Basel) ; 13(10)2020 May 18.
Artigo em Inglês | MEDLINE | ID: mdl-32443609

RESUMO

This paper reports the results of the designing, manufacturing and characterization of a jewel obtained by means of coupling the dogmas of industrial design to the analytical engineering approach. The key role in the design of the jewel was played by an in-house synthesized Neodymium (Nd)-doped phosphate glass, selected due to its easy handling and capability to change color according to the incident light wavelength. The glass core was covered by a metal alloy to mitigate its relatively high fragility and sensitivity to thermal shock and, at the same time, to highlight and preserve its beauty. The selection of the proper metal alloy, having thermo-mechanical properties compatible with those exhibited by the glass, was carried out by means of Ashby's maps, a powerful tool commonly adopted in the field of industrial design.

6.
Materials (Basel) ; 12(22)2019 Nov 11.
Artigo em Inglês | MEDLINE | ID: mdl-31718051

RESUMO

In powder metallurgy (PM), severe plastic deformation (SPD) is a well-known technological solution to achieve interesting properties. However, the occurrence of pores in the final product may limit these properties. Also, for a given type of microstructure, the stereometric parameters of the pore structures, such as shape (represented by Aspect and Dcircle) and distribution (fshape, and fcircle), decisively affect the final properties. The influence of different processing routes (pressing, sintering and equal channel angular pressing (ECAP)) on pore structures in an aluminum PM alloy is discussed. The nature of porosity, porosity evolution and its behavior is explored. The correlation between pore size and morphology is also considered. The final pore structure parameters (Aspect, Dcircle, fshape, and fcircle) of studied aluminum alloys produced by different processing routes depends on the different formation routes.

7.
Materials (Basel) ; 12(21)2019 Oct 24.
Artigo em Inglês | MEDLINE | ID: mdl-31652888

RESUMO

Aluminum alloys are widely used to produce automotive components, thanks to their great mechanical properties-to-density ratio. Engine components such as pistons are conventionally produced by casting of Al-Si eutectic alloys (Silumin alloys) such as EN AC 48000. Due to the harsh working conditions and the lower ductility if compared to aluminum-silicon alloys with lower silicon content, pistons made of this alloy are prone to fatigue failures in the skirt region. In order to overcome such limits, the use of a Functionally Graded Material (FGM) in the production of a piston is proposed. The adoption of a functionally graded architecture can maximize the properties of the component in specific areas. A higher level of thermal resistance in the crown of the piston can be achieved with EN AC 48000 (AlSi12CuNiMg), while higher elongation at rupture in the skirt region would be conferred by an EN AC 42100 (AlSi9Mg0.3). The FGM properties are strictly related to the metallurgical bonding between the alloys as well as to the presence of intermetallic phases in the alloys junction. In the present article, the characterization of gravity casted FGM samples based on Al-Si alloys with respect to microstructure and mechanical testing is presented, with a specific focus on the characterization by impact testing of the joint between the two alloys.

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