Crack propagation and toughening mechanism of bilayered short-fiber reinforced resin composite structure -Evaluation up to six months storage in water.

Clinically relevant parameters, such as stress intensity factor of bilayered resin composite structure with short fiber base and its stability over time, has yet to be investigated. This study investigated the stress intensity factor of pre-cracked bilayered specimens composed of short fiber resin composite base (SFC) and particulate filler resin composite (PFC) as veneering layer, with a crack located in the PFC layer, 0.5 mm away from the PFC-SFC interface. Monolayered specimens served as controls. All specimens were stored in water at 37°C either for 1 week, 1 month or 6 months before testing. Two-way ANOVA (p=0.05) was used to determine the differences among the groups. Results indicated that SFC base improve the brittleness of the PFC. The type of short fibers affected the crack propagation; fiber bridging in millimeter-scale SFC was the main crack arresting mechanism, whereas fiber pulling observed in micrometer-scale SFC mainly deviated the crack path.

The influence of FRC base and bonded CAD/CAM resin composite endocrowns on fatigue behavior of cracked endodontically-treated molars.

Cracked endodontically treated molars (ETMs) are commonly treated with full crowns. Less invasive techniques could include fiber-reinforced composite (FRC) base and adhesively bonded endocrowns. The purpose of this study was to assess the fatigue resistance of ETMs restored with CAD/CAM resin composite endocrowns and reinforced with different FRC bases. Cracks were simulated in fifty mandibular molars by cutting the teeth longitudinally and reassembling the two parts. After performing endodontic treatments and preparing cavities, teeth were restored in one of the following methods (n = 10). In Group 1, cavity floors were lined with 0.5 mm of flowable composite (Universal Injectable; GUI, shade A2). In Groups 2 and 3, the cavity floors were covered with one and three layers of FRC-net (ES Net) respectively, whereas in Groups 4 and 5 with 1 mm and 2 mm of flowable FRC-resin (EverX Flow Dentin; EXFD) respectively. Endocrowns (Cerasmart 270; CE, A2 HT) with 5 mm thickness were adhesively luted with preheated composite and all specimens were subjected to cyclic loading in water at 5 Hz, starting with a load of 600 N (5000 cycles), followed by stages of 1000, 1300, 1600, 1900, 2200 and 2500 at a maximum of 20 000 cycles each. Results were analyzed using Kaplan-Meier survival analysis and the Log-Rank test (p = 0.05). The fatigue failure load of ES Net applied in three layers (1617 N ± 371) or in one layer (1499 N ± 306), as well as EXFD applied in 2 mm (1496 N ± 264) or in 1 mm (1434 N ± 372) did not differ significantly (p > 0.05). Control teeth fractured at 1255 N ± 350 (p > 0.05). In the fiber-reinforced groups, restorable fractures were observed in 50%-80%, with only 30% deemed restorable in the control group. The fractures originated mainly at the occlusal contact points and the main crack propagated in the corono-apical direction. No crack origin (primary or secondary) starting from the artificial pre-existing crack was observed in fractured specimens. FRC bases did not improve the fatigue resistance of cracked ETMs, but favorably influenced the failure mode.

Temporary Implant-Supported Single Crowns Using Titanium Base Abutments: An In Vitro Study on Bonding Stability and Pull-out Forces.

PURPOSE: To evaluate the effect of cementation protocols on the bonding interface stability and pull-out forces of temporary implant-supported crowns bonded on a titanium base abutment (TiB) or on a temporary titanium abutment (TiA). MATERIALS AND METHODS: A total of 60 implants were restored with PMMA-based CAD/CAM crowns. Five groups (n = 12) were created: Group 1 = TiB/SRc: crown conditioned with MMA-based liquid (SR Connect, Ivoclar Vivadent); Group 2 = TiB/50Al-MB: crown airborne particle-abraded with 50-µm Al2O3 and silanized (Monobond Plus, Ivoclar Vivadent); Group 3 = TiB/30SiOAl-SRc: crown airborne particle-abraded with 30-µm silica-coated Al2O3 (CoJet, 3M ESPE) and conditioned with MMA-based liquid (SR Connect); Group 4 = TiB/30SiOAl-MB: crown airborne particle-abraded with 30- µm silica-coated Al2O3 (CoJet) and silanized (Monobond Plus); and Group 5 = TiA/TA-PMMA: crown manually enlarged, activated, and rebased with PMMA resin (Telio Lab, Ivoclar Vivadent). Specimens in the TiB groups were cemented using a resin cement (Multilink Hybrid Abutment, Ivoclar Vivadent). After aging (120,000 cycles, 49 N, 1.67 Hz, 5°C to 55°C, 120 seconds), bonding interface failure was analyzed (50x). Pull-out forces (N) (0.5 mm/minute) and modes of failure were registered. Chi-square and Kruskal-Wallis tests were used to analyze the data (α = .05). RESULTS: Bonding failure after aging varied from 0% (Group 5) to 100% (Groups 1, 2, and 4) (P < .001). Mean pull-out force ranged between 53.1 N (Group 1) and 1,146.5 N (Group 5). The pull-off forces were significantly greater for Group 5 (P < .05), followed by Group 3 (P < .05), whereas the differences among the remaining groups were not significant (P > .05). CONCLUSION: The cementation protocol had an effect on the bonding interface stability and pull-out forces of PMMA-based crowns bonded on a titanium base. Airborne particle abrasion of the crown internal surface and conditioning it with an MMA-based liquid may be recommended to improve retention of titanium base temporary restorations. Yet, for optimal outcomes, conventional temporary abutments might be preferred.

Direct bilayered biomimetic composite restoration: The effect of a cusp-supporting short fiber-reinforced base design on the chewing fracture resistance and failure mode of molars with or without endodontic treatment.

The aim of this study was to assess the chewing fracture resistance of compromised molars restored with direct composite resin (CR) restorations, with and without a short-fiber reinforcing (short-FRC) base. Wide extension of MOD cavities with removed palatal cusps preparations were simulated on 48 extracted maxillary molars. Five groups (n = 12) were designed: 1. control (intact teeth), 2. non-endodontically treated and 3. endodontically treated teeth with direct CR restorations (GC-Posterior), and 4. non-endodontically treated and 5. endodontically treated teeth with direct biomimetic bilayered restorations. Groups 4 and 5 included an anatomically shaped short-FRC base (everX Posterior), covered with a 2 mm CR layer (GC-Posterior). Restorations were subjected to chewing in water (1.5 Hz), with load of 85 N. Specimens were loaded until fracture or to a maximum of 120 000 cycles. Restorations that survived the chewing cycle were submitted to static load test (post-chewing test). The data were statistically analyzed using two-way ANOVA (p = 0.05) and fracture types with the chi-square test (p = 0.05). Fractures were classified into reparable, possibly reparable or non-reparable. All specimens survived the chewing cycle. The chewing fracture resistance of the direct biomimetic restorations prepared on non-endodontically treated teeth (2889 N) was statistically significantly higher than the direct CR counterparts (1966 N) (p = 0.00015), which was not the case for the groups with endodontically treated teeth (p = 0.257). Inclusion of a short-FRC base also influenced the fracture type resulting in most reparable fractures (67-75% versus 25% for biomimetic and CR groups respectively) (p = 0.054). Anatomically shaped i.e. a cusp-supporting design made of short-FRC base (everX Posterior) improved the chewing fracture resistance and fracture manner of compromised molars regardless of whether they were endodontically treated or not.

Immediate Repair Bond Strength of Fiber-reinforced Composite after Saliva or Water Contamination.

PURPOSE: This in vitro study aimed to evaluate the shear bond strength (SBS) of particulate filler composite (PFC) to saliva- or water-contaminated fiber-reinforced composite (FRC). MATERIALS AND METHODS: One type of FRC substrate with semi-interpenetrating polymer matrix (semi-IPN) (everStick C&B) was used in this investigation. A microhybrid PFC (Filtek Z250) substrate served as control. Freshly cured PFC and FRC substrates were first subjected to different contamination and surface cleaning treatments, then the microhybrid PFC restorative material (Filtek Z250) was built up on the substrates in 2-mm increments and light cured. Uncontaminated and saliva- or water-contaminated substrate surfaces were either left untreated or were cleaned via phosphoric acid etching or water spray accompanied with or without adhesive composite application prior applying the adherent PFC material. SBS was evaluated after thermocycling the specimens (6000 cycles, 5°C and 55°C). RESULTS: Three-way ANOVA showed that both the surface contamination and the surface treatment signficantly affected the bond strength (p < 0.05). Saliva contamination reduced the SBS more than did the water contamination. SBS loss after saliva contamination was 73.7% and 31.3% for PFC and FRC, respectively. After water contamination, SBS loss was 17.2% and 13.3% for PFC and FRC, respectively. The type of surface treatment was significant for PFC (p < 0.05), but not for FRC (p = 0.572). CONCLUSION: Upon contamination of freshly cured PFC or semi-IPN FRC, surfaces should be re-prepared via phosphoric acid etching, water cleaning, drying, and application of adhesive composite in order to recover optimal bond strength.

Mechanical and structural characterization of discontinuous fiber-reinforced dental resin composite.

OBJECTIVES: This study evaluated several fiber- and matrix related factors and investigated different mechanical properties of discontinuous i.e. short fiber-reinforced composite (SFRC) (everX Posterior, eXP). These were compared with three conventional composites, microfilled G-ænial Anterior (GA), nanofilled Supreme XTE (SXTE) and bulk-fill Filtek Bulk-Fill (FBF). METHODS: Fracture toughness (KIC), flexural strength (FS), flexural modulus (FM), compressive strength (CS), diametral tensile strength (DTS), apparent horizontal shear strength (AHSS) and fracture work (Wf) were determined for each composite (n=8) stored dry or in water. SEM analysis of the fiber diameter (df) (n=6) and orientation (n=6) were performed. The theoretical critical fiber length (lfc) and the aspect ratio (l/d) of SFRC were calculated and the volume fraction of discontinuous fibers (Vf%) and the fiber length (lf) of SFRC were evaluated. The results were statistically analyzed with two-way ANOVA (α=0.05). RESULTS: The mechanical properties of SFRC (eXP) were generally superior (p<0.05) compared with conventional composites. GA had the highest FM (p>0.05), whereas FBF had the highest AHSS (p<0.05). The fiber related properties Vf%, l/d, lf, lfc and df of eXP were 7.2%, 18-112, 0.3-1.9mm, 0.85-1.09mm and 17µm respectively. SEM results suggested an explanation to several toughening mechanisms provided by the discontinuous fibers, which were shown to arrest crack propagation and enable a ductile fracture. Water exposure weakened the mechanical properties regardless of material type. Wf was unaffected by the water storage. CONCLUSION: The properties of this high aspect ratio SFRC were dependent on the fiber geometry (length and orientation) and matrix ductility. CLINICAL SIGNIFICANCE: The simultaneous actions of the toughening mechanisms provided by the short fibers accounted for the enhanced toughness of this SFRC, which toughness value matched the toughness of dentin. Hence, it could yield an inherently uniform distribution of stresses to the hard biological tissues.

Mechanical properties, fracture resistance, and fatigue limits of short fiber reinforced dental composite resin.

STATEMENT OF PROBLEM: Cycling masticatory loads decrease the strength of particulate filler composites (PFCs) and initiate the failure process by fatigue. The life expectancy of a composite resin restoration under stress remains difficult to predict. PURPOSE: The purpose of this study was to determine the fracture resistance and the compressive fatigue limits (CFL) of anterior crown restorations made of a short-fiber reinforced composite resin (SFC), to investigate selected mechanical properties of the material following standard test methods, and to observe their correlation with the CFL. MATERIAL AND METHODS: Specimens (n=10) were fabricated either from SFC (everX Posterior, GC Corp) or PFC (G-ænial anterior, GC Corp). The properties investigated were flexural strength (FS), compression strength (CS), diametral-tensile strength (DTS), and single-edge-notched-bend fracture toughness (FT) following ISO standards. Fracture resistance was determined by static load (n=10) and the CFL at 10000 cycles was determined using a staircase approach (n=20), both on anterior composite resin crowns. The results were analyzed with 1-way ANOVA (α=.05) or 2-way ANOVA (α=.05) followed by a Tukey B post hoc test and the Pearson-correlation analysis. RESULTS: The SFC crowns had higher fracture resistance (954 ±121 N) than the PFC crowns (415 ±75 N) (P<.001) and higher CFL (267 ±23 N) than the PFC crowns (135 ±64 N) (P<.001). SFC revealed also higher FT (2.6 ±0.6 MPa·m(1/2)) than the PFC (1.0 ±0.2 MPa·m(1/2)) (F=69.313, P<.001). A significant correlation was observed only between the FT and the CFL (r(2)=0.899; P<.001). CONCLUSIONS: SFC crowns showed good performance under static and fatigue loading. FT was the only in vitro test method that filtered as a clinically relevant parameter.

Oxygen inhibition layer of composite resins: effects of layer thickness and surface layer treatment on the interlayer bond strength.

An oxygen inhibition layer develops on surfaces exposed to air during polymerization of particulate filling composite. This study assessed the thickness of the oxygen inhibition layer of short-fiber-reinforced composite in comparison with conventional particulate filling composites. The effect of an oxygen inhibition layer on the shear bond strength of incrementally placed particulate filling composite layers was also evaluated. Four different restorative composites were selected: everX Posterior (a short-fiber-reinforced composite), Z250, SupremeXT, and Silorane. All composites were evaluated regarding the thickness of the oxygen inhibition layer and for shear bond strength. An equal amount of each composite was polymerized in air between two glass plates and the thickness of the oxygen inhibition layer was measured using a stereomicroscope. Cylindrical-shaped specimens were prepared for measurement of shear bond strength by placing incrementally two layers of the same composite material. Before applying the second composite layer, the first increment's bonding site was treated as follows: grinding with 1,000-grit silicon-carbide (SiC) abrasive paper, or treatment with ethanol or with water-spray. The inhibition depth was lowest (11.6 µm) for water-sprayed Silorane and greatest (22.9 µm) for the water-sprayed short-fiber-reinforced composite. The shear bond strength ranged from 5.8 MPa (ground Silorane) to 36.4 MPa (water-sprayed SupremeXT). The presence of an oxygen inhibition layer enhanced the interlayer shear bond strength of all investigated materials, but its absence resulted in cohesive and mixed failures only with the short-fiber-reinforced composite. Thus, more durable adhesion with short-fiber-reinforced composite is expected.