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2.
J Anal Toxicol ; 4(5): 217-21, 1980.
Artigo em Inglês | MEDLINE | ID: mdl-7442133

RESUMO

A retrospective study of illicit phencyclidine (PCP), which consisted of 94 different cases or 213 individual samples, has shown that one third of both the powder/tablets and green plant material contained the synthetic contaminant 1-piperidinocyclohexanecarbonitrile (PCC). The mole % PCC/PCP ranged from 1 to 68%. The method of analysis was gas chromatography (3% OV-7, 205 degrees C) and in preparation for analysis the sample was dissolved directly in chloroform or extracted from a strongly acidic solution (0.1 N HCl). Using these extraction conditions PCC was found not to undergo measurable decomposition.


Assuntos
Nitrilas/análise , Fenciclidina/análise , Piperidinas/análise , Cromatografia Gasosa/métodos , Contaminação de Medicamentos , Drogas Ilícitas/análise
5.
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