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Radiat Prot Dosimetry ; 167(4): 419-24, 2015 Dec.
Artigo em Inglês | MEDLINE | ID: mdl-25398396

RESUMO

Nano-CaF2, prepared by the co-precipitation method, was annealed under different annealing conditions to improve its thermoluminescence (TL) characteristics. Different annealing parameters, such as temperature (400-700°C), duration (1-4 h) and environment (vacuum and air), were explored. The effect on TL sensitivity, peak position (Tm) and full-width at half-maximum (FWHM) with respect to the different annealing conditions are discussed as they are the measure of crystallinity of the material. Annealing temperature of 500°C with annealing duration of two and a half hours in vacuum provided the highest luminescence response (i.e. maximum sensitivity, minimum peak temperature and FWHM). Wide detectable dose range (5 mGy to 2 kGy), absence of thermal quenching and sufficient activation energy (1.04 eV) of this phosphor make it suitable for dosimetric applications.


Assuntos
Fluoreto de Cálcio/química , Luminescência , Nanoestruturas/química , Temperatura , Dosimetria Termoluminescente/métodos , Relação Dose-Resposta a Droga , Difração de Raios X
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