1.
Chemistry
; 20(10): 2746-9, 2014 Mar 03.
Artigo
em Inglês
| MEDLINE
| ID: mdl-24519685
RESUMO
A highly efficient one-pot procedure for the preparation of 1-chloroalkynes and 1-chlorobutadiynes from terminal and trialkylsilyl-protected precursors is reported. This convenient reaction, proceeding under mild conditions, utilizes N-chlorosuccinimide as the chlorinating agent and tolerates a range of functional groups.