Surface treatments of the zirconia-reinforced lithium disilicate ceramic in the adhesion to the resin cement.

This study verified the effect of surface treatments of the zirconia-reinforced lithium disilicate ceramic bonded to resin cement. Ceramic blocks were divided according to treatments (n=10): FA+SRX (Fluoric acid + silane RX), FA+MDP (Fluoric acid + MDP), FA+SCF+MDP (Fluoric acid + silane CF + MDP), FA+MEP (Fluoric acid + MEP), and MEP (Self-etch primer). Resin cement cylinders were made in the ceramic blocks, photoactivated with 1,200 mW/cm² for 40s, stored in water at 37°C for 24h, and evaluated by the microshear strength test, optical failure descriptive analysis (%), surface characterization (SEM) and contact angle (Goniometer). Other samples were submitted to 10,000 thermocycles between 5°C and 55°C. Bond strength data were submitted to two-way ANOVA and Tukey's test. Contact angle to one-way ANOVA and Games-Howell's test (5%). At 24h, MEP showed higher bond strength, and FA+SRX the lower. FA+MDP and FA+SCF+MDP showed similar values and FA+MEP was intermediate. After thermocycling, FA+SCF+MDP, FA+MEP, and MEP showed higher values, and FA+SRX the lower while FA+MDP was intermediate. When the periods were compared, FA+MDP, FA+SCF+MDP, FA+MEP, and MEP showed higher values for 24h while FA+SRX was similar. SEM showed retentive surface and crystal exposure when treated with FA+SCF+MDP. The less retentive surface was obtained with MEP, and the other treatments promoted intermediate irregularities. In conclusion, surface treatment and thermocycling promoted different values of adhesive strength and contact angle in a zirconia-reinforced lithium silicate ceramic. Failures were predominantly adhesive, and the ceramic surface was characterized by different levels of roughness and selective exposure of crystals.

Surface treatments of the zirconia-reinforced lithium disilicate ceramic in the adhesion to the resin cement

Abstract This study verified the effect of surface treatments of the zirconia-reinforced lithium disilicate ceramic bonded to resin cement. Ceramic blocks were divided according to treatments (n=10): FA+SRX (Fluoric acid + silane RX), FA+MDP (Fluoric acid + MDP), FA+SCF+MDP (Fluoric acid + silane CF + MDP), FA+MEP (Fluoric acid + MEP), and MEP (Self-etch primer). Resin cement cylinders were made in the ceramic blocks, photoactivated with 1,200 mW/cm² for 40s, stored in water at 37°C for 24h, and evaluated by the microshear strength test, optical failure descriptive analysis (%), surface characterization (SEM) and contact angle (Goniometer). Other samples were submitted to 10,000 thermocycles between 5°C and 55°C. Bond strength data were submitted to two-way ANOVA and Tukey's test. Contact angle to one-way ANOVA and Games-Howell's test (5%). At 24h, MEP showed higher bond strength, and FA+SRX the lower. FA+MDP and FA+SCF+MDP showed similar values and FA+MEP was intermediate. After thermocycling, FA+SCF+MDP, FA+MEP, and MEP showed higher values, and FA+SRX the lower while FA+MDP was intermediate. When the periods were compared, FA+MDP, FA+SCF+MDP, FA+MEP, and MEP showed higher values for 24h while FA+SRX was similar. SEM showed retentive surface and crystal exposure when treated with FA+SCF+MDP. The less retentive surface was obtained with MEP, and the other treatments promoted intermediate irregularities. In conclusion, surface treatment and thermocycling promoted different values of adhesive strength and contact angle in a zirconia-reinforced lithium silicate ceramic. Failures were predominantly adhesive, and the ceramic surface was characterized by different levels of roughness and selective exposure of crystals.

Resumo O objetivo neste estudo foi verificar o efeito de tratamentos de superfície da cerâmica de dissilicato de lítio reforçada com zircônia fixada ao cimento resinoso. Os blocos cerâmicos foram separados de acordo com os tratamentos (n=10): AF+SRX (ácido fluorídrico + silano), AF+MDP (ácido fluorídrico + MDP), AF+SCF+MDP (ácido fluorídrico + silano + MDP), AF+MEP (Ácido fluorídrico + MEP) e MEP (Primer auto condicionante). Cilindros de cimento resinoso foram confeccionados em cada bloco cerâmico, foto ativados com 1.200 mW/cm² por 40 segundos, armazenados em água a 37°C por 24 horas e avaliados pelo teste de resistência ao micro cisalhamento, falha por análise descritiva em microscopia óptica (%), caracterização da superfície por imagens MEV e ângulo de contato (Goniômetro). Outras amostras foram submetidas a 10.000 ciclos térmicos (5° e 55°C). Os dados de resistência de união foram submetidos a ANOVA dois fatores e teste de Tukey (5%). Ângulo de contato com ANOVA um fator e teste de Games-Howell (5%). Em 24 horas, MEP apresentou maior resistência de união e AF+S a menor. AF+MDP e AF+SCF+MDP apresentaram valores similares e AF+MEP foi intermediário. Após a ciclagem térmica, AF+SCF+MDP, AF+MEP e MEP apresentaram valores maiores e AF+SRX o menor enquanto AF+MDP foi intermediário. Quando comparados os períodos, AF+MDP, AF+SCF+MDP, AF+MEP e MEP apresentaram valores maiores em 24 horas enquanto AF+SRX foi similar. MEV mostrou superfície mais retentiva e exposição de cristais quando tratada com AF+SCF+MDP. A superfície menos retentiva foi obtida com MEP, e os demais tratamentos promoveram irregularidades de superfície intermediárias. Conclui-se que o tratamento superficial e a termociclagem promoveram diferentes valores de resistência adesiva e ângulo de contato em cerâmica de silicato de lítio reforçada com zircônia. As falhas foram predominantemente adesivas, e a superfície cerâmica foi caracterizada com diferentes níveis de rugosidade e exposição seletiva de cristais.

Effect of the combination of a crosslinking agent and a thiourethane additive on the properties of acrylic denture bases processed with microwave energy.

Thiourethane (TU) additives and difunctional, polymerizable crosslinking agents have been demonstrated to increase toughness in methacrylate-based materials. The aim of this study was to evaluate the potential reinforcement of acrylic denture bases by combining thiourethane additives and 1,6 hexanediol dimethacrylate (HDDMA) as an additional crosslinking agent. One commercial acrylic resin (Nature-Cryl MC; GC America) was tested by adding 0 (control) or 10 wt% TU, each of them combined with 0 (control), 10, 20 and 30 wt% HDDMA, for a total of 8 experimental groups. Materials were processed using microwave energy (500 W for 3 min) using microwave-safe molds and flasks. Flexural strength, modulus and toughness were obtained in 3-point bending (ISO 4049) using bars measuring 2 × 2x25 mm (n = 6). Dynamic mechanical analysis was used to determine glass transition temperature (Tg), breadth of tan delta (as a measure of polymer heterogeneity) and crosslinking density in 1 × 3x15 mm bars (n = 6) tested in tension, using a 3 °C/min heating rate (-30 to 180 °C). Viscosity samples were evaluated in a parallel plate reometer. Data were analyzed by two-way ANOVA and Tukey's test (α = 0.05). Results showed that on the samples not containing TU, HDDMA up to 20 wt% increased the flexural strength and thoughness (and up to 30 wt% HDDMA increased the modulus). The addition of TU did not affect those properties (except for the increase in elastic modulus), but the combination TU + HDDMA led to decreased properties overall. The addition of HDDMA decreased the viscosity for all materials, and the presence of TU did not affect viscosity. The Tg increased linearly with the concentration of HDDMA, except in the groups containing TU - in general, the addition of TU reduced Tg. The crosslinking density increased with the addition of HDDMA for all materials, regardless of the presence of TU. The addition of TU significantly decreased crosslinking density. The breadth of tan delta was not affected by the addition of HDDMA, but significantly increased with the addition of TU. In conclusion, the chain-breaking effect of TU on polymerizing methacrylates was deleterious in the case of methyl methacrylate, since it forms a linear polymer. The addition of HDDMA up to 20 wt% and not combined with TU significantly improved the tested properties.

Influence of Cross-Section Design and Vertical Misfit on Stress Distribution in Overdenture Retaining System: 3-Dimensional Finite Element Analysis.

PURPOSE: To evaluate by 3-dimensional (3-D) finite element analysis the stress generated on overdenture-retaining bar system with different cross sections (round, ovoid, or Hader) and misfit levels (50, 100, and 200 µm) manufactured with different metallic alloys (Au type IV, Ag-Pd, Ti cp, and Co-Cr). MATERIALS AND METHODS: Three-dimensional finite element models were modeled using specific 3-D software (SolidWorks) and imported into mechanical simulation software (ANSYS). A displacement simulating the settlement of the screw was performed until the infrastructure was settled properly on the prosthetic platform. RESULTS: Higher misfit levels caused higher stress on the overdenture-retaining bar system components, where (1) Hader bar presented the highest values (bar = 730.71; screw = 59.66, and periimplant bone tissue = 42.96, in megapascal) and (2) round bars made with type IV Au alloy presented lower stress values on the bar framework (193.99 MPa) and screw (10.27 MPa). CONCLUSIONS: Higher vertical misfit increased the stress values on the overdenture-retaining bar system; complex cross-sectional designs increased stress values on the bar framework, prosthetic screw, and periimplant bone tissue; stiffer alloys caused higher stress values on all the studied conditions.

Production of a biofunctional titanium surface using plasma electrolytic oxidation and glow-discharge plasma for biomedical applications.

In this study, the authors tested the hypotheses that plasma electrolytic oxidation (PEO) and glow-discharge plasma (GDP) would improve the electrochemical, physical, chemical, and mechanical properties of commercially pure titanium (cpTi), and that blood protein adsorption on plasma-treated surfaces would increase. Machined and sandblasted surfaces were used as controls. Standard electrochemical tests were conducted in artificial saliva (pHs of 3.0, 6.5, and 9.0) and simulated body fluid. Surfaces were characterized by scanning electron microscopy, energy-dispersive spectroscopy, x-ray photoelectron spectroscopy, atomic force microscopy, x-ray diffraction, profilometry, Vickers microhardness, and surface energy. For biological assay, the adsorption of blood serum proteins (i.e., albumin, fibrinogen, and fibronectin) was tested. Higher values of polarization resistance and lower values of capacitance were noted for the PEO and GDP groups (p < 0.05). Acidic artificial saliva reduced the corrosion resistance of cpTi (p < 0.05). PEO and GDP treatments improved the surface properties by enrichment of the surface chemistry with bioactive elements and increased surface energy. PEO produced a porous oxide layer (5-µm thickness), while GDP created a very thin oxide layer (0.76-µm thickness). For the PEO group, the authors noted rutile and anatase crystalline structures that may be responsible for the corrosion barrier improvement and increased microhardness values. Plasma treatments were able to enhance the surface properties and electrochemical stability of titanium, while increasing protein adsorption levels.

Stress on external hexagon and Morse taper implants submitted to immediate loading.

BACKGROUND/AIMS: This study aimed to evaluate the stress distribution around external hexagon (EH) and Morse taper (MT) implants with different prosthetic systems of immediate loading (distal bar (DB), casting technique (CT), and laser welding (LW)) by using photoelastic method. METHODS: Three infrastructures were manufactured on a model simulating an edentulous lower jaw. All models were composed by five implants (4.1 mm × 13.0 mm) simulating a conventional lower protocol. The samples were divided into six groups. G1: EH implants with DB and acrylic resin; G2: EH implants with titanium infrastructure CT; G3: EH implants with titanium infrastructure attached using LW; G4: MT implants with DB and acrylic resin; G5: MT implants with titanium infrastructure CT; G6: MT implants with titanium infrastructure attached using LW. After the infrastructures construction, the photoelastic models were manufactured and a loading of 4.9 N was applied in the cantilever. Five pre-determined points were analyzed by Fringes software. RESULTS: Data showed significant differences between the connection types (p < 0.0001), and there was no significant difference among the techniques used for infrastructure. CONCLUSION: The reduction of the stress levels was more influenced by MT connection (except for CT). Different bar types submitted to immediate loading not influenced stress concentration.

Teeth movement in denture and implant-supported prosthesis influenced by microwave flask systems.

BACKGROUND/AIMS: This study evaluated the teeth movement in maxillary dentures and mandibular implantsupported prostheses processed by microwave flasks. METHODS: A model mounted on articulator was used to manufacture Co-Cr frameworks. Pins were placed for measurements on the incisal edge of upper and lower central incisors (I), buccal cusp of first upper and lower premolars (PM), and mesiobuccal cusps of upper and lower second molars (M). Distances I-I (incisor to incisor), PM-PM (premolar to premolar), M-M (molar to molar), RI-RM (right incisor to right molar), and LI-LM (left incisor to left molar) were measured before and after processing using a microscope (0.0005 mm). Vertical misfit between abutment and implant platform was evaluated for regions A (left distal implant), B (left median implant), C (medial implant), D (right median implant), and E (right distal implant) in predetermined labial and lingual sites. Prostheses were divided into groups G1 - conventional flask, and G2 - experimental HH flask. Acrylic resin was microwaved at 1400 W (30% for 3 min, 0% for 3 min, and 60% for 3 min). Horizontal teeth displacement and vertical misfit between abutment and implant platform were considered before and after procedures. Data were submitted to three-way ANOVA and Tukey's test (α = 0.05). RESULTS: Except for M-M distance, the teeth showed displacements without statistical difference for prosthesis and flask factors. There was no significant difference for vertical misfit values for both flasks. CONCLUSION: Diferente flasks did not cause significant changes in the teeth displacement, except for M-M. Vertical misfit values were not influenced by the flasks.

Photoelastic analysis of stresses transmitted by complete dentures lined with hard or soft liners.

Stresses transmitted on the alveolar bone ridge by lined conventional complete mandibular dentures can decrease the bone absorption level. The aim of this in vitro study was to evaluate the stresses induced on the alveolar bone ridge of lined conventional complete mandibular dentures by using photoelastic analysis. One maxillary and three mandibular conventional dentures were developed for the following treatments: 1 - Unlined denture (control), 2 - Denture lined with resin-based material, and 3 - Denture lined with silicone-based material. The photoelastic analysis took place with the dentures in the position of maximum intercuspation, and the mandibular photoelastic models were axially loaded with 10 kgf (98 N). Unlined denture (control) presented stresses along the model, especially on the anterior and left lateral sides with less stresses on the right side. On the left lateral side, the denture base lined with resin-based material demonstrated similar stresses to that of the control; however, lower stresses occurred in the premolar and retromolar regions. Denture bases lined with silicone-based material showed decreased fringe orders and homogeneous distribution of induced stresses. Both lined dentures exhibited lower stresses when compared to unlined dentures. Silicone-based material provided a more homogeneous distribution of stresses.

Thio-urethane oligomers improve the properties of light-cured resin cements.

Thio-urethanes were synthesized by combining 1,6-hexanediol-diissocyante (aliphatic) with pentaerythritol tetra-3-mercaptopropionate (PETMP) or 1,3-bis(1-isocyanato-1-methylethyl)benzene (aromatic) with trimethylol-tris-3-mercaptopropionate (TMP), at 1:2 isocyanate:thiol, leaving pendant thiols. Oligomers were added at 10-30 phr to BisGMA-UDMA-TEGDMA (5:3:2, BUT). 25 wt% silanated inorganic fillers were added. Commercial cement (Relyx Veneer, 3M-ESPE) was also evaluated with 10-20 phr of aromatic oligomer. Near-IR was used to follow methacrylate conversion (DC) and rate of polymerization (Rpmax). Mechanical properties were evaluated in three-point bending (ISO 4049) for flexural strength/modulus (FS/FM, and toughness), and notched specimens (ASTM Standard E399-90) for fracture toughness (KIC). Polymerization stress (PS) was measured on the Bioman. Volumetric shrinkage (VS, %) was measured with the bonded disk technique. Results were analyzed with ANOVA/Tukey's test (α=5%). In general terms, for BUT cements, conversion and mechanical properties in flexure increased for selected groups with the addition of thio-urethane oligomers. The aromatic versions resulted in greater FS/FM than aliphatic. Fracture toughness increased by two-fold in the experimental groups (from 1.17 ± 0.36 MPam(1/2) to around 3.23 ± 0.22 MPam(1/2)). Rpmax decreased with the addition of thio-urethanes, though the vitrification point was not statistically different from the control. VS and PS decreased with both oligomers. For the commercial cement, 20 phr of oligomer increased DC, vitrification, reduced Rpmax and also significantly increased KIC, and reduced PS and FM. Thio-urethane oligomers were shown to favorably modify conventional dimethacrylate networks. Significant reductions in polymerization stress were achieved at the same time conversion and fracture toughness increased.

Stress distribution in fixed-partial prosthesis and peri-implant bone tissue with different framework materials and vertical misfit levels: a three-dimensional finite element analysis.

The purpose of this study was to evaluate the influence of superstructure material and vertical misfits on the stresses created in an implant-supported partial prosthesis. A three-dimensional (3-D) finite element model was prepared based on common clinical data. The posterior part of a severely resorbed jaw with two osseointegrated implants at the second premolar and second molar regions was modeled using specific modeling software (SolidWorks 2010). Finite element models were created by importing the solid model into mechanical simulation software (ANSYS Workbench 11). The models were divided into groups according to the prosthesis framework material (type IV gold alloy, silver-palladium alloy, commercially pure titanium, cobalt-chromium alloy, or zirconia) and vertical misfit level (10 µm, 50 µm, and 100 µm) created at one implant-prosthesis interface. The gap of the vertical misfit was set to be closed and the stress values were measured in the framework, porcelain veneer, retention screw, and bone tissue. Stiffer materials led to higher stress concentration in the framework and increased stress values in the retention screw, while in the same circumstances, the porcelain veneer showed lower stress values, and there was no significant difference in stress in the peri-implant bone tissue. A considerable increase in stress concentration was observed in all the structures evaluated within the misfit amplification. The framework material influenced the stress concentration in the prosthetic structures and retention screw, but not that in bone tissue. All the structures were significantly influenced by the increase in the misfit levels.

Influence of different mucosal resiliency and denture reline on stress distribution in peri-implant bone tissue during osseointegration. A three-dimensional finite element analysis.

OBJECTIVE: The aim of this study was to evaluate the influence of mucosal properties and relining material on the stress distribution in peri-implant bone tissue during masticatory function with a conventional complete denture during the healing period through finite element analysis. MATERIALS AND METHODS: Three-dimensional models of a severely resorbed mandible with two recently placed implants in the anterior region were created and divided into the following situations: (i) conventional complete denture and (ii) relined denture with soft lining material. The mucosal tissue properties were divided into soft, resilient and hard. The models were exported to mechanical simulation software; two simulations were carried out with a load at the lower right canine (35 N) and the lower right first molar (50 N). Data were qualitatively evaluated using Maximum Principal Stress, in MPa, given by the software. RESULTS: All models showed stress concentrations in the cortical bone corresponding to the cervical part of the implant. The mucosal properties influenced the stress in peri-implant bone tissue showing a different performance according to the denture base material. The simulations with relined dentures showed lower values of stress concentration than conventional ones. CONCLUSIONS: It seems that the mucosal properties and denture reline have a high influence on the stress distribution in the peri-implant bone during the healing period.

Effect of toothbrushing, chemical disinfection and thermocycling procedures on the surface microroughness of denture base acrylic resins.

OBJECTIVE: This study verified the surface microroughness of denture acrylic resins submitted to toothbrushing, chemical disinfection and thermocycling procedures. MATERIAL AND METHODS: Samples were prepared according to conventional, microwaved and boiled resins and submitted to microroughness measurements before and after procedures using a profilometer (Ra). Data were subjected to anova and Tukey's test (5%). RESULTS: Before thermocycling, a difference was found among treatments for microwaved and boiled resins, with greater values for toothbrushing and lower values for Efferdent and hypochlorite; control was intermediate. Differences among resins were observed for treatments, with higher values for boiled resin and lower values for conventional and microwaved resins. After thermocycling, differences were found for microwaved resin, with a higher value for toothbrushing and a lower value for Efferdent and hypochlorite; control was intermediate. Tooth-brushed boiled resin presented higher values and hypochlorite lower values; control and Efferdent were intermediates. Differences among resins were seen for treatments, with higher values for boiled resin and lower values for conventional and microwaved resins. Boiled resin presented differences for toothbrushing and hypochlorite, before and after thermocycling procedures were compared. CONCLUSIONS: For microwaved and boiled resins, toothbrushing and chemical disinfection promoted different levels of surface microroughness when associated or not with thermocycling.

Fatigue strength: effect of welding type and joint design executed in Ti-6Al-4V structures.

BACKGROUND: This study evaluated the fatigue strength of Ti-6Al-4V-machined structures submitted to laser (L)-welding and TIG (TIG)-welding procedures, varying the joint designs. MATERIALS AND METHODS: Seventy dumbbell rods were machined in Ti-6Al-4V alloy with central diameters of 3.5 mm. The specimens were sectioned and welded using TIG or L and three joint designs {'I' design, varying welding distances [0.0 mm (I00) or 0.6 mm (I06)], or 'X' [X] design}. The combinations of variables created six groups, which, when added to the intact group, made a total of seven groups (n = 10). L was executed as follows: 360 V/8 ms (X) and 390 V/9 ms (I00 and I06), with focus and frequency regulated to zero. TIG was executed using 2:2 (X) and 3:2 (I00 and I06) as welding parameters. Joints were finished, polished and submitted to radiographic examination to be analysed visually for the presence of porosity. The specimens were then subjected to mechanical cyclic tests, and the number of cycles completed until failure was recorded. The fracture surface was examined using a scanning electron microscope. RESULTS: The Kruskal-Wallis and Dunn test (α = 0.05) indicated that the number of cycles resisted for fracture was higher to X for both welding procedures. To L, I06 was as resistant as X. The Mann-Whitney U-test (α = 0.05) indicated that L joints were more resistant than TIG to I00 and I06. Spearman's correlation coefficient (α = 0.05) indicated a negative correlation between the number of cycles and presence of porosity. CONCLUSION: Thus, to weld Ti-6Al-4V structures, the best condition is X, independent of the welding method employed.

Effect of repeated microwave disinfections on bonding of different commercial teeth to resin denture base.

OBJECTIVE: To verify the influence of repeated microwave disinfections on the shear bond strength of two commercial types of teeth to acrylic resin, when the ridge lap surfaces were unmodified, bur abraded, bur grooved or etched by monomer. MATERIAL AND METHODS: Eighty specimens (n = 10) were adhered to the tooth ridge lap surface, polymerised in a water bath at 74°C for 9 h. Microwaved specimens were individually immersed in 150 ml of water and submitted to five simulated disinfections in a microwave oven calibrated at 650 W for 3 min. Control specimens were not microwave treated. Shear bond strength tests were performed in an Instron machine with a cross-speed of 1 mm/min. The fracture load values were transformed into shear bond strength as a function of the bonding area (0.28 cm(2)). Data were submitted to ANOVA and Tukey's test (α = 0.05). Fractured areas were classified as adhesive, cohesive (resin or tooth) or mixed failures. RESULTS: Repeated microwave disinfections increased the shear strength of the tooth/resin bond. Mechanical retention in microwaved and non-microwaved procedures improved the shear bond strength. CONCLUSIONS: The different commercial types of teeth influenced shear bond strength values, with Biotone teeth showing the lower values.

Effect of ridge-lap surface treatments on the bond of resin teeth to denture base.

PURPOSE: To test in vitro the shear bond strength of resin teeth to an acrylic resin denture base given different ridgelap surface treatments. MATERIALS AND METHODS: Ninety rectangular dies were made with wax and traditionally invested in metallic or plastic flasks. The stone molds were covered with silicone, in which were included an acrylic molar with a wax stick fixed on the ridge lap surface. After deflasking, the wax sticks were removed, the teeth were cleaned with detergent, the ridge lap surface was submitted to different treatments (unmodified, bur-cut grooves, aluminum oxide particle sandblasting, monomer swelling, and primer swelling), and the teeth were replaced in the silicone molds. Metallic flasks were placed in a thermopolymerizing unit to polymerize heat-curing denture-base polymer, and plastic flasks were placed in a domestic microwave oven at 900 W to polymerize microwaveable denture base polymer. After deflasking, the specimens were submitted to the shear bond test in an Instron machine at a cross-speed of 1 mm/min. Results were submitted to ANOVA and Tukey's test (5%). RESULTS: Shear bond strength values were influenced by the ridge-lap surface treatments only in the microwaved polymer. Sandblasting + monomer swelling and sandblasting + primer swelling interactions yielded lower strengths for microwaved polymer. Only the unmodified surfaces presented a significant difference when the resins were compared, where the microwaved polymer showed a higher value. CONCLUSION: Different tooth ridge-lap surface treatments promoted different strengths of the tooth/resin bond.

Effect of microwave treatment on the shear bond strength of different types of commercial teeth to acrylic resin.

OBJECTIVE: The purpose of this study was to verify the effect of microwave treatment on the shear bond strength of commercial types of teeth to acrylic resin, when the glossy ridge laps were unmodified (groups 1 and 5), bur abraded (groups 2 and 6), bur grooved (groups 3 and 7) or etched by monomer (groups 4 and 8). BACKGROUND: Controversial findings have shown that mechanical or chemical changes in ridge-lap surface of the tooth increase or decrease the bond strength between tooth and acrylic resin, and the microwave disinfection may cause different changes on this bond strength. MATERIALS AND METHODS: Eighty specimens (n = 10) were made with the acrylic resin bonded to tooth glossy ridge lap, polymerised in water at 74 degrees C for 9 h, and deflasked after flask cooling. Specimens of the groups 5, 6, 7 and 8 were individually immersed in 150 ml of water and submitted to microwave treatment in an oven at 650 W for 3 min. Control specimens (groups 1, 2, 3 and 4) were not microwave treated. Shear bond strength test was performed in an Instron machine with a cross-speed of 1 mm/min. Collected data were submitted to anova and Tukey's test (alpha = 0.05). RESULTS: Microwave treatment decreased the shear bond strength values of the tooth/resin bond. In the microwaved and non-microwaved procedures, mechanical retention improved the shear bond strength when compared with the control and monomer treatments. CONCLUSION: Shear bond strength of the tooth/resin bond was influenced by the microwave treatment and different commercial teeth association, and was lower for the Biotone tooth.

Effect of flask closure method and post-pressing time on the upper denture base adaptation.

OBJECTIVES: The purpose of this study was to evaluate the effect of flask-closure methods, post-pressing times and acrylic resins on denture base adaptation. MATERIALS AND METHODS: The resins were flasked using a hydraulic press and closed with the traditional clamp or RS system. Conventional heat-cure resin was polymerised immediately or at 6 h post-pressing at 74 degrees C for 9 h. Rapid cycle heat-cure resin was polymerised in boiling water for 20 min. After cooling, the bases were deflasked and the sets of cast-base transversally sectioned in the regions distal to the canine, mesial to the first molar and in the posterior palatal zone. The adaptation was measured with an optical microscope (0.0005 mm) at five reference points for each section. Data were analysed using anova and Tukey's test (alpha = 0.05). RESULTS: Traditional clamp and immediate post-pressing time improved base adaptation for conventional heat-cure resin. Both post-pressing times showed most accurate base adaptation for conventional heat-cure resin when the traditional clamp was used. Immediate post-pressing time improved base adaptation for conventional heat-cure resin and the 6-h delay in time was significant for the rapid cycle heat-cure resin. CONCLUSIONS: Traditional clamp and immediate post-pressing time improved base adaptation for conventional heat-cure resin.

Effect of flask closure method and post-pressing time on the displacement of maxillary denture teeth.

The purpose of this study was to verify the influence of flask closure methods and post-pressing times on tooth displacement in maxillary dentures. Twenty similar maxillary dentures were made using a heat-polymerized acrylic resin, and randomly assigned to 4 experimental groups (n=5) according to the protocol: 1-conventional flask closure and immediate polymerization; 2- conventional flask closure and polymerization after 6-hour post-pressing time; 3- RS flask closure system and immediate polymerization; and 4- RS flask closure system and polymerization after 6-hour post-pressing time. Three transverse and 2 anteroposterior linear distances between teeth were measured before and after the denture processing with an optical microscope with accuracy of 0.0005mm. Analysis of variance (ANOVA) and Tukey's test were performed to compare the results. The 6-hour post-pressing time (conventional = 0.44mm and RS = 0.33mm) showed no statistically significant difference in tooth movement, in relation to the flask closure methods, when compared to the immediate time (conventional = 0.40mm and RS = 0.28mm). The RS system standardized the tooth displacement, independently of the post-pressing times. Dimensional changes were more uniform when the dentures were submitted to the 6-hour post-pressing time and RS flask closure method, suggesting that these factors may reduce the magnitude of tooth movement.

Effect of the simulated disinfection by microwave energy on the impact strength of the tooth/acrylic resin adhesion.

The objective of this study was to determine the effect of simulated microwave disinfection on the tooth/acrylic resin impact strength. Acrylic molar teeth with a wax stick attached to the ridge lap were included in brass flasks. Specimens were made with Classico thermopolymerized acrylic resin, according to the groups: 1 and 5 - tooth with no treatment (control); 2 and 6 - tooth bur abrasion; 3 and 7 - tooth bur retention; and 4 and 8 - tooth monomer etch. Eighty specimens (n=10) were polymerized in bath cycle at 74( masculine)C for 9 hours and deflasked after flask cooling. Specimen from groups 2, 4, 6 and 8 was submitted to simulated microwave disinfection in a microwave oven at 650W for 3 minutes. Impact strength test was performed with an Otto Wolpert-Werke machine (Charpy system) with an impact load of 40 kpcm. Fracture load value was transformed into impact strength as a function of the bond area (kfg/cm(2)). Collected data were submitted to ANOVA and Tukey's test (alpha=.05) and results indicate that the simulated microwave disinfection decreased the impact strength in all treatments.