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1.
Beilstein J Nanotechnol ; 14: 781-792, 2023.
Artigo em Inglês | MEDLINE | ID: mdl-37441001

RESUMO

We present the in situ synthesis of silver nanoparticles (AgNPs) through ionotropic gelation utilizing the biodegradable saccharides lactose (Lac) and alginate (Alg). The lactose reduced silver ions to form AgNPs. The crystallite structure of the nanocomposite AgNPs@Lac/Alg, with a mean size of 4-6 nm, was confirmed by analytical techniques. The nanocomposite exhibited high catalytic performance in degrading the pollutants methyl orange and rhodamine B. The antibacterial activity of the nanocomposite is pH-dependent, related to the alterations in surface properties of the nanocomposite at different pH values. At pH 6, the nanocomposite demonstrated the highest antibacterial activity. These findings suggest that this nanocomposite has the potential to be tailored for specific applications in environmental and medicinal treatments, making it a highly promising material.

2.
Environ Sci Pollut Res Int ; 25(34): 34247-34261, 2018 Dec.
Artigo em Inglês | MEDLINE | ID: mdl-30291612

RESUMO

This study presents an efficient and facile method for biosynthesis of silver nanoparticles (AgNPs) and gold nanoparticles (AuNPs) using aqueous extract of burdock root (BR), A. lappa, and their applications. The nanoparticles were characterized by ultraviolet-visible spectrophotometry, X-ray diffraction, transmission electron microscopy, energy dispersive X-ray, thermogravimetry, and differential thermal analysis. AgNPs capped the BR extract (BR-AgNPs) possessed roughly spherical geometry with an average diameter of 21.3 nm while uneven geometry of AuNPs capped the BR extract (BR-AuNPs) showed multi shapes in average size of 24.7 nm. The BR-AgNPs strongly inhibited five tested microorganism strains. In particular, the nanoparticles showed excellent catalytic activity for the conversion of pollutants within wastewater. Pseudo-first-order rate constants for the degradation of 4-nitrophenol, methyl orange, and rhodamine B were respectively found 6.77 × 10-3, 3.70 × 10-3, and 6.07 × 10-3 s-1 for BR-AgNPs and 6.87 × 10-3, 6.07 × 10-3, and 7.07 × 10-3 s-1 for BR-AuNPs. Graphical abstract ᅟ.


Assuntos
Anti-Infecciosos/farmacologia , Arctium/química , Nanopartículas Metálicas/química , Extratos Vegetais/química , Poluentes Químicos da Água/química , Anti-Infecciosos/química , Compostos Azo/química , Catálise , Ouro/química , Ouro/farmacologia , Testes de Sensibilidade Microbiana , Microscopia Eletrônica de Transmissão , Nitrofenóis/química , Extratos Vegetais/metabolismo , Rodaminas/química , Prata/química , Prata/farmacologia , Espectrofotometria Ultravioleta , Termogravimetria , Difração de Raios X
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