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1.
Materials (Basel) ; 15(21)2022 Nov 04.
Artigo em Inglês | MEDLINE | ID: mdl-36363390

RESUMO

One of the most important design factors in the constitution of adhesive joints is the correct choice of adhesive. Currently, there is a full range of options on the commercial market in this regard, but there is increasing research into modifying adhesives for specific engineering applications. The aim of this study was to analyze the effect of physical modification with fillers on the properties of the adhesive composition and the adhesive joints. The adhesives used in the study were a composition of Epidian 5 epoxy resin and PAC curing agent modified with 1% montmorillonite, 5% calcium carbonate and 20% activated carbon. The adhesive compositions in the cured state were subjected to strength tests and SEM and DSC analyses. Using these compositions, adhesive joints of EN AW 2024 T3 aluminum alloy sheets were also made. The tests carried out showed that, due to the use of different fillers, their effects on certain properties of the adhesive compositions are different types. It was shown that physical modification of the adhesive composition does not always result in positive effects. The study also attempted to determine the correlation between the properties of the adhesive compositions in the cured state and the strength of the adhesive joints.

2.
Materials (Basel) ; 15(20)2022 Oct 19.
Artigo em Inglês | MEDLINE | ID: mdl-36295364

RESUMO

The parameters of surface roughness Ra, Rz and Rmax as well as surface topography Sa, Sz, Sp and Sv of the two-layer sandwich structure composed of an AW-2024 T3 aluminum alloy (Al) and a carbon-fiber-reinforced polymer (CFRP) were measured to determine an impact of the machining configuration (arrangement of the materials forming a sandwich structure) and the type of tool (presence of the tool coating) on the quality of the surface obtained through circumferential milling. The measurements revealed that milling produced different values of surface roughness for the aluminum alloy and the CFRP composite with values of 2D and 3D surface roughness being higher for the composite layer. The highest value of Ra of 1.10 µm was obtained for the surface of the CFRP composite using the CFRP/Al configuration and a TiAlN-coated tool. The highest values of the Rz (6.51 µm) and Rmax (8.85 µm) surface roughness parameters were also obtained for the composite layer using the same machining configuration and type of tool.

3.
Materials (Basel) ; 15(15)2022 Jul 25.
Artigo em Inglês | MEDLINE | ID: mdl-35897588

RESUMO

The aim of the paper is to determine the influence of the surface treatment on the adhesive properties of steel sheet surfaces and the strength of the adhesive joints of steel sheets. The paper also aims to assess the degree of steel sheets' surface treatment in the bonding process. Due to the many methods of surface treatment and types of materials, the assessment of the surface treatment method is extremely important in adhesive processes. Two variants of the surface treatment were used: without a paint coating and with a paint coating, divided into two groups (without degreasing and with degreasing). Additionally, in the case of the analysis of the steel samples without the paint coating, mechanical treatment was applied. Two-component epoxy adhesive, prepared on the basis of bisphenol A and a polyamide curing agent, was used to prepare the single-lap adhesive joints of the steel sheets. The tests determined: (i) the adhesive properties of the steel sheets' surface based on the measurement of the contact angle of polar and apolar liquids (including wettability, work of adhesion, and surface free energy), (ii) surface roughness parameters (PN EN ISO 4287), and (iii) mechanical properties (load capacity and shear strength) of the steel sheets' adhesive joints (EN DIN 1465). Contact angle measurements of the steel sheet surfaces showed that the polar liquid better reflects the obtained strength results of the analyzed adhesive joints than the apolar liquid. Furthermore, better wettability of the surface of steel sheets with both polar and apolar liquids was obtained for samples whose surface was subjected to degreasing. It can also be concluded that the wettability of the surface can be used as one of the indicators of the degree of the surface treatment for the bonding process.

4.
Materials (Basel) ; 14(21)2021 Nov 03.
Artigo em Inglês | MEDLINE | ID: mdl-34772150

RESUMO

In this study, the influence of sandblasting process parameters as a surface preparation method on the strength of single-lap adhesive joints of EN AW 2024 T3 aerospace aluminium alloy sheets was determined. Eleven sets of sandblasting parameters were used, which were determined according to a determined experimental plan. The variable factors in the sandblasting process were pressure, nozzle distance, and workpiece displacement speed. The sand jet incidence angle was constant. Garnet 80 E+ was the abrasive material that was used. The joints were made using an epoxy adhesive composition of Epidian 5 epoxy resin and a PAC curing agent. The influence of the surface preparation method on the surface roughness and contact angle to determine the surface free energy was evaluated. The shear strength of the adhesive joints was also determined, which finally allowed the evaluation of the applied surface treatment variants. The obtained results were subjected to statistical analysis, which indicated that the highest shear strength of the adhesive joints was obtained for samples whose surfaces were treated by sandblasting at parameter configurations in which the pressure was 5-6 × 105 Pa; the distance between the nozzle and the sandblasted surface should not be greater than 97 mm, and the speed at which the workpiece moves in relation to the nozzle should not be greater than 75 mm/min.

5.
Materials (Basel) ; 14(22)2021 Nov 12.
Artigo em Inglês | MEDLINE | ID: mdl-34832237

RESUMO

This study presents the results of research on the surface quality of hybrid sandwich structures after milling with a diamond blade tool. It identifies the effects of feed and machining strategy on the roughness and topography of the surface. It provides an analysis of Ra and Rz surface roughness parameters as well as Sp, Sz, and Sv surface topography parameters. The processed object was a two-layer sandwich structure consisting of aluminium alloy 2024 and CFRP (carbon fibre-reinforced polymer) composite. The minimum values of the Ra and Rz surface roughness parameters were obtained on the aluminium alloy surface, whereas the maximum values were obtained on the CFRP surface. The same was true for the 3D surface roughness parameters-the lowest values of Sp, Sz, and Sv parameters were obtained on the surface of the metal layer, while the highest values were obtained on the surface of the composite layer (the maximum value of the Sp parameter was an exception). A surface topography analysis has revealed a targeted and periodic pattern of micro-irregularities for the vast majority of the samples considered. The statistical analysis shows that the surface roughness of the aluminium alloy was only affected by the feed rate. For the CFRP, the feed rate and the interaction of milling strategy and feed rate (S × fz) had a statistically significant effect. The obtained results provide a basis for designing such sandwich element processing technology, for which differences in roughness and topography parameters for the component materials are lowest.

6.
Materials (Basel) ; 14(22)2021 Nov 16.
Artigo em Inglês | MEDLINE | ID: mdl-34832340

RESUMO

The purpose of the paper is to determine the impact of surface treatment on the strength of adhesive joints, made from various steel sheets. Two variants of the surface treatment steel adherends were used: without the varnish coat and with the varnish coat, using three polymer-based varnishes (a simple, a hybrid, and a gel). Two types of the adhesives were used to prepare the adhesive joints: a single-component cyanoacrylate adhesive and a two-component epoxy adhesive. A strength test of the adhesive joints (EN DIN 1465 standard), a coating adhesion test (ASTM D3359-B standard), and surface topography, as well as surface roughness, parameters (PN-EN ISO 11562, PN-EN ISO 4287, and PN-EN ISO 25178 standards) were used. Based on the strength tests, it was observed that the adhesive joints, with the hybrid varnish onto the adherend's surface, achieved markedly lower shear strength. The best results, in terms of the adhesive joint strength, made using the cyanoacrylate adhesive were achieved for the joints where the adherends were coated with a simple varnish, while in the joints made using the epoxy adhesive, the highest shear strength was achieved by the joints of sheets whose surfaces were coated with the gel varnish.

7.
Materials (Basel) ; 13(17)2020 Aug 26.
Artigo em Inglês | MEDLINE | ID: mdl-32858846

RESUMO

In this study, the effect of cutting parameters on the quality of an Al/CFRP sandwich structure (aluminium alloy-carbon fibre reinforced polymer) after milling with uncoated and TiAlN-coated tools was examined. The results of the cutting force were also investigated. The research was conducted in a VMC 800 HS vertical machining centre with a variable cutting speed and feed. The milling process was carried out using a non-coated, two-blade carbide milling cutter with a 35° helix angle and an analogous tool with a TiAlN coating. The surface quality was characterised in terms of the height deviation, which is one of the shape deviations after machining hybrid materials. The research showed that the maximum (77.60 µm) and minimum (1.78 µm) values of the height deviations were obtained using the tool with a TiAlN coating. It was found that the tested factors had significant effects on the height deviation, where the feed had the greatest influence and the cutting speed had the lowest influence on the surface quality. The tested factors were not statistically significant in terms of the cutting force.

8.
Materials (Basel) ; 13(7)2020 Apr 03.
Artigo em Inglês | MEDLINE | ID: mdl-32260144

RESUMO

Hybrid sandwich structures are more and more widely used in many industries. This is mainly due to their good properties. One of the limitations regarding the use of sandwich structures is their difficult processing. Therefore, it seems reasonable to determine the influence of cutting parameters and machining configuration on the characteristic defect (phase) formed at the boundary of the materials forming a hybrid sandwich structure. This study investigates the effects of layer orientations during milling and machining parameters such as the cutting speed Vc, the feed fz and the cutting width ae. The study is conducted on a two-layer sandwich structure composed of two materials: 2024 aluminum alloy and epoxy-carbon composite with 60% of high-strength carbon fibers. A statistical analysis is performed using the Statistica program. The results show that the change in the cutting parameters has a greater impact on the formation of a defect on the surface of samples when the machining process starts on the side of the composite rather than the metal. The highest defect value is obtained for the milling from the composite layer when the process is performed with the following cutting parameters: Vc = 300 m/min, fz = 0.08 mm/tooth, ae = 5 mm.

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