Dual-mode auto-calibrating resistance thermometer: A novel approach with Johnson noise thermometry.

A dual-mode auto-calibrating resistance thermometer (DART) is presented. The novel DART concept combines in one instrument the fast and accurate resistance thermometry with the primary method of Johnson noise thermometry. Unlike previous approaches, the new thermometer measures the spectral density of the thermal noise in the sensing resistor directly in a sequential measurement procedure without using correlation techniques. A sophisticated data analysis corrects the thermometer output for both the parasitic effects of the sensor wiring and the amplifier current noise. The instrument features a highly linear low-noise DC coupled amplifier with negative feedback as well as an accurate voltage reference and reference resistor to improve the gain stability over time and ambient temperature. Therefore, the system needs only infrequent calibrations with electrical quantum standards and can be operated over long intervals and a wide temperature range without recalibration. A first prototype is designed for the industrially relevant temperature range of the IEC 60751 (-200 °C to +850 °C); a later extension of the measurement range is being considered. A proof-of-principle measurement with a calibrated Pt100 sensor at room temperature yielded an uncertainty of about 100 µK/K. The final device is expected to reach uncertainties of below 10 µK/K, suitable for accurate measurements of the difference between thermodynamic temperatures and temperatures traceable to the International Temperature Scale of 1990 (ITS-90).

Noise-optimized ultrastable low-noise current amplifier.

We have developed a noise-optimized ultrastable low-noise current amplifier (ULCA) aimed at reducing the uncertainty at low currents. It involves a thin-film resistor network with 6.75 GΩ at the high-ohmic path which reduces the noise level to 1.6 fA/Hz. Noise investigations as well as short-term and long-term stability studies were carried out. The stability of the input current gain was measured using a cryogenic current comparator at ±6.1 nA. Methods for investigating the measurement accuracy at low input currents of about 100 pA at a level of below one part in 107 are introduced and experimentally verified. The performance of the noise-optimized ULCA is compared with that of the standard variant introduced in 2014. It is shown that the reduced noise floor is achieved without impairing the stability of the transresistance.

Measurement of sub-picoampere direct currents with uncertainties below ten attoamperes.

A new type of the ultrastable low-noise current amplifier (ULCA) is presented. It involves thick-film resistors to achieve a high feedback resistance of 185 GΩ at the input amplifier. An improved noise level of 0.4 fA/Hz with a 1/f corner of about 30 µHz and an effective input bias current well below 100 aA are demonstrated. For small direct currents, measurement uncertainties below 10 aA are achievable even without current reversal or on/off switching. Above about 1 pA, the stability of the ULCA's resistor network limits the relative measurement uncertainty to about 10 parts per million. The new setup is used to characterize and optimize the noise in the wiring installed on a dilution refrigerator for current measurements on single-electron transport pumps. In a test configuration connected to the wiring in a pulse tube refrigerator, a total noise floor of 0.44 fA/Hz was achieved including the contributions of amplifier and cryogenic wiring.

Reducing current noise in cryogenic experiments by vacuum-insulated cables.

We measure the current noise of several cryogenic cables in a pulse tube based dilution refrigerator at frequencies between about 1 mHz and 50 kHz. We show that vibration-induced noise can be efficiently suppressed by using vacuum-insulated cables between room temperature and the 2nd pulse tube stage. A noise peak below 4 fA at the 1.4 Hz operation frequency of the pulse tube and a white noise density of 0.44 fA/Hz in the millihertz range are obtained.

Primary current-sensing noise thermometry in the millikelvin regime.

The use of low-temperature platforms with base temperatures below 1 K is rapidly expanding, for fundamental science, sensitive instrumentation and new technologies of potentially significant commercial impact. Precise measurement of the thermodynamic temperature of these low-temperature platforms is crucial for their operation. In this paper, we describe a practical and user-friendly primary current-sensing noise thermometer (CSNT) for reliable and traceable thermometry and the dissemination of the new kelvin in this temperature regime. Design considerations of the thermometer are discussed, including the optimization of a thermometer for the temperature range to be measured, noise sources and thermalization. We show the procedure taken to make the thermometer primary and contributions to the uncertainty budget. With standard laboratory instrumentation, a relative uncertainty of 1.53% is obtainable. Initial comparison measurements between a primary CSNT and a superconducting reference device traceable to the PLTS-2000 (Provisional Low Temperature Scale of 2000) are presented between 66 and 208 mK, showing good agreement within the k=1 calculated uncertainty.

Ultrastable low-noise current amplifier: a novel device for measuring small electric currents with high accuracy.

An ultrastable low-noise current amplifier (ULCA) is presented. The ULCA is a non-cryogenic instrument based on specially designed operational amplifiers and resistor networks. It involves two stages, the first providing a 1000-fold current gain and the second performing a current-to-voltage conversion via an internal 1 MΩ reference resistor or, optionally, an external standard resistor. The ULCA's transfer coefficient is highly stable versus time, temperature, and current amplitude within the full dynamic range of ±5 nA. The low noise level of 2.4 fA/√Hz helps to keep averaging times short at small input currents. A cryogenic current comparator is used to calibrate both input current gain and output transresistance, providing traceability to the quantum Hall effect. Within one week after calibration, the uncertainty contribution from short-term fluctuations and drift of the transresistance is about 0.1 parts per million (ppm). The long-term drift is typically 5 ppm/yr. A high-accuracy variant is available that shows improved stability of the input gain at the expense of a higher noise level of 7.5 fA/√Hz. The ULCA also allows the traceable generation of small electric currents or the calibration of high-ohmic resistors.

Phase diagram of the topological superfluid 3He confined in a nanoscale slab geometry.

The superfluid phases of helium-3 ((3)He) are predicted to be strongly influenced by mesoscopic confinement. However, mapping out the phase diagram in a confined geometry has been experimentally challenging. We confined a sample of (3)He within a nanofluidic cavity of precisely defined geometry, cooled it, and fingerprinted the order parameter using a sensitive nuclear magnetic resonance spectrometer. The measured suppression of the p-wave order parameter arising from surface scattering was consistent with the predictions of quasi-classical theory. Controlled confinement of nanofluidic samples provides a new laboratory for the study of topological superfluids and their surface- and edge-bound excitations.

Note: Highly sensitive superconducting quantum interference device microsusceptometers operating at high frequencies and very low temperatures inside the mixing chamber of a dilution refrigerator.

We report the experimental results that show the operation of superconducting quantum interference device (SQUID) microsusceptometers immersed in the (3)He-(4)He mixture inside the mixing chamber of a dilution refrigerator at high frequency (1 MHz) and down to very low temperatures (13 mK). The devices are based on highly sensitive and easy-to-use commercial SQUID sensors. The integrated susceptometers are fabricated by rerouting some connections of the SQUID's input circuit. Examples of measurements on molecular magnets Mn(12) and HoW(10) are shown.

Discrimination of multiple sources using a SQUID vector magnetometer.

For many biomagnetic applications the discrimination between simultaneously active sources is required. To evaluate the performance of a given SQUID system in this respect, the angle between the signal vectors of different sources is used. If the angle reaches large values, discrimination between the multiple sources is possible. We tested this approach with the first module of a new vector magnetometer system consisting of 19 identical modules. Two examples of measurements illustrate the differentiation of multiple sources, i.e. the fetal and the mother's heart signal, and alpha rhythm and heart signal in MEG recordings. This first module of a vector magnetometer system containing 16 SQUIDs is operated at PTB in the new Berlin Magnetically Shielded Room (BMSR 2) The spatial configuration of the 16 integrated SQUID magnetometers of the module is such that all three vector components of the magnetic field can be calculated in three measurement planes at 1.5 cm, 5 cm, and 10.5 cm above the Dewar bottom, respectively. The SQUID magnetometer channels have a typical white noise level of less than 2.3 fT/square root of Hz1/2 at 1 kHz.

A sensor configuration for a 304 SQUID vector magnetometer.

A novel SQUID vector magnetometer system is introduced which has been specially designed for the use inside the strongly magnetically shielded room BMSR-2 of PTB. The system is housed in a dewar with a flat bottom and an inner diameter of Ø 250 mm. The SQUIDs are arranged so that in addition to the usually measured Z-component of the field the horizontal magnetic fields are measured too. A total of 304 DC-SQUID magnetometers are divided up into 19 identical modules. The 16 low-Tc SQUIDs of each module are located in such a way that an estimation of the magnetic field in all three dimensions is possible at three points inside the module. The 57 SQUIDs of the lowest Z plane of all modules form a hexagonal grid with a base length of 29 mm. The design criteria and the physical principle behind the complex SQUID arrangement are explained.

Magnetometry of evoked fields from human peripheral nerve, brachial plexus and primary somatosensory cortex using a liquid nitrogen cooled superconducting quantum interference device.

Superconducting Quantum Interference Devices (SQUIDs) can be used to detect neuromagnetic fields evoked in the peripheral and central nervous system. Up to now, such measurements had to be based on SQUIDs with a low critical temperature (Tc) requiring liquid helium cooling. Recent improvements in high-Tc SQUID technology relying on liquid nitrogen cooling led to a significant reduction in the system's noise level. Hare, first high-Tc recordings of weak neuromagnetic fields are demonstrated. In particular, along the entire somatosensory afferent pathway including peripheral nerves, brachial plexus and primary somatosensory neocortex evoked neuromagnetic activities were detected using conventional recording parameters for bandwidth and number of averages. This opens up a wide perspective for cost-effective high-Tc magnetometry in clinical neuroscience.

A 37-channel DC SQUID magnetometer system.

A 37-channel DC SQUID magnetometer system has been built for biomagnetic studies. The SQUID loop of each magnetometer serves as the active sensing element, thereby eliminating the need for flux coupling circuits. The magnetometers are located approximately 3 cm above the outer dewar bottom. The SQUIDs are directly coupled to highly simplified read-out electronics using only five wires per channel; no helium temperature impedance matching circuits are required. Each channel can be independently inserted into or removed from the dewar. Using a novel electronic noise reduction technique the system white and 1 Hz flux density noise values are typically 5 and 10 fT Hz-1/2, respectively, including the noise contribution of the in-house fabricated dewar and the magnetically shielded room. The two parts of the data-processing system allow independent handling of the acquisition and analysing task. Two example measurements demonstrate the advantage of the electronic noise reduction method.