1.
Acta Crystallogr E Crystallogr Commun
; 73(Pt 11): 1647-1651, 2017 Nov 01.
Artigo
em Inglês
| MEDLINE
| ID: mdl-29152342
RESUMO
The title compound, C11H7NS2, was prepared in high yield (87%) using a solvent-free microwave-assisted synthesis. The structure shows whole-mol-ecule disorder with occupancies for two orientations (A and B) of 0.4884â (10) and 0.5116â (10), respectively. The thio-phene and benzo-thia-zole rings are almost planar and make dihedral angles of 10.02â (18) and 12.54â (19)° for orientations A and B, respectively. Slipped π-π stacking between the aromatic rings, together with C-Hâ¯π, C-Hâ¯S and C-Hâ¯N inter-actions, result in a herringbone motif in the crystal packing.