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1.
Materials (Basel) ; 15(24)2022 Dec 14.
Artigo em Inglês | MEDLINE | ID: mdl-36556758

RESUMO

Aluminum-magnesium-scandium-zirconium (AlMgScZr) alloys need to be rapidly cooled from the liquid state to obtain a high degree of solute supersaturation that helps to exploit the precipitation hardening potential of the material. While AlMgScZr alloys have been successfully used in laser powder bed fusion (LPBF) processes, there has been little research in the field of laser directed energy deposition (DED) of the material. The limited previous studies have shown that the performance of AlMgScZr parts fabricated with DED only reached about 60% of that of the parts fabricated with LPBF. In view of breaking through the limitation associated with the process conditions of conventional DED, this work demonstrates the DED of AlMgScZr alloys in high-speed process regimes and elucidates the mechanism of enhancing the hardness and tensile strength of AlMgScZr alloys by increasing the cooling rate by one to two orders of magnitudes, as well as reducing the track overlapping and the porosity of the specimens during the process. A maximum average hardness of nearly 150 HV0.1 and a max. tensile strength of 407 MPa are obtained by using an energy per unit length of 5400 J/m and a powder feed rate per unit length of 0.25 g/m.

2.
Appl Opt ; 60(27): 8408-8418, 2021 Sep 20.
Artigo em Inglês | MEDLINE | ID: mdl-34612940

RESUMO

We present a study of the temporal prepulse contrast degradation of high focused intensity pulses produced in CPA laser systems due to imperfections in amplifier design, alignment of amplifier components, and crystal inhomogeneity. Using an extended cross-polarized imaging technique, we demonstrate the presence of multiple crystal domains inside Ti:sapphire slabs with ≈10cm diameter. The results of our numerical calculations show that crystalline c-axis orientation inhomogeneity caused by these crystal domains can lead to the generation of prepulses with a relative contrast of >10-10 within several picoseconds before the main pulse. In a multiple-slab amplifier head configuration sometimes used in high-repetition-rate systems, the misalignment of the crystalline c-axes of the amplifier slab with respect to each other can lead to the generation of prepulses with relative contrast as high as 10-6, depending on the magnitude of misalignment.

3.
Materials (Basel) ; 14(4)2021 Feb 22.
Artigo em Inglês | MEDLINE | ID: mdl-33671719

RESUMO

In the present study, we propose a hybrid manufacturing route to produce high-quality Ti6Al4V parts, combining additive powder laser directed energy deposition (L-DED) for manufacturing of preforms, with subsequent hot forging as a thermomechanical processing (TMP) step. After L-DED, the material was hot formed at two different temperatures (930 °C and 1070 °C) and subsequently heat-treated for stress relief annealing. Tensile tests were performed on small sub-samples, taking into account different sample orientations with respect to the L-DED build direction and resulting in very good tensile strengths and ductility properties, similar or superior to the forged material. The resulting microstructure consists of very fine grained, partially globularized alpha grains, with a mean diameter ~0.8-2.3 µm, within a beta phase matrix, constituting between 2 and 9% of the sample. After forging in the sub-beta transus temperature range, the typical L-DED microstructure was no longer discernible and the anisotropy in tensile properties, common in additive manufacturing (AM), was significantly reduced. However, forging in the super-beta transus temperature range resulted in remaining anisotropies in the mechanical properties as well as an inferior tensile strength and ductility of the material. It was shown, that by combining L-DED with thermomechanical processing in the sub-beta transus temperature range of Ti6Al4V, a suitable microstructure and desirable mechanical properties for many applications can be obtained, with the advantage of reducing the material waste.

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