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1.
Sensors (Basel) ; 23(8)2023 Apr 13.
Artigo em Inglês | MEDLINE | ID: mdl-37112306

RESUMO

This article presents aspects regarding the possibilities of optimizing the quality of the elaboration of metallurgical melts by determining their physical-chemical properties. Thus, the article analyzes and presents methods for determining the viscosity and electrical conductivity related to metallurgical melts. Among the viscosity determination methods, two methods are presented, namely: the rotary viscometer method and the electro-vibratory viscometer method. Determining the electrical conductivity of a metallurgical melt is also of particular importance for ensuring the quality of the elaboration and refining of the melt. The article also presents the possibilities of using and implementing computer systems that ensure the accuracy of determining the physical-chemical properties of metallurgical melts, as well as examples of the use of physical-chemical sensors and specific computer systems for determining the analyzed parameters. The specific electrical conductivity measurements of oxide melts are performed by direct methods (by contact), with Ohm's law as a starting point. Thus, the article presents the voltmeter-ammeter method and the point method (or the zero method). The novelty of this article is the description and the use of specific methods and sensors for certain determinations (viscosity and electrical conductivity) for metallurgical melts. The motivation here is the presentation of the authors' research in the addressed field. The article presents an original contribution of the adaptation and use of some methods for determining some physico-chemical parameters, including specific sensors, in the field of the elaboration of metal alloys, with the aim of optimizing their quality.

2.
Materials (Basel) ; 16(6)2023 Mar 18.
Artigo em Inglês | MEDLINE | ID: mdl-36984312

RESUMO

The authors present in this paper the experimental results and conclusions obtained after conducting a comparative study on three samples of forged semi-finished products from the steel brands 10CrMo9-10, 25CrMo4, and 42CrMo4. These are common heat-resistant alloy steels used in various industries nationally and internationally. This study aimed to test under the same identical experimental conditions of forging and heat treatment of three samples made of three different brands of steels 10CrMo9-10, 25CrMo4, and 42CrMo4. Analyzing the experimental results obtained, it can be seen for which of the three brands of tested steels the best forging and heat treatment parameters are obtained. Following experimental research, the best material was determined by analyzing the results obtained for the mechanical characteristics (tensile tests according to DNVGL-RP0034-SFC2 and NACE MR0175-hardness 207-235 HBW) and austenitic grain size. The authors determined that among the three types of steels analyzed, 10CrMo9-10 best meets the imposed requirements. This statement is in view of the comparative analysis of the results of experimental research.

3.
Materials (Basel) ; 16(1)2022 Dec 22.
Artigo em Inglês | MEDLINE | ID: mdl-36614457

RESUMO

A cellular concrete with a fine porous structure was experimentally made using the corrosion technique for aluminum powder as an expanding agent in an aqueous solution of Ca(OH)2. The originality of this paper was the use of our own production method for the fine aluminum powder through atomizing the recycled molten waste of this metal using concentrated jets of nitrogen. Additionally, the waste melting technique involved our own microwave heating method. A high weight proportion of calcined gypsum (maximum 82.3%) represented the main concrete binder. Using moderate contents of coal fly ash (3.6-11.1%) together with perlite (4.6-6.4%) to reduce the pore size and silica fume (0.3-1.2%) with pozzolanic properties, the aim was to obtain a macrostructure characterized by a very low pore size and to increase the compressive strength (by up to 4.1 MPa), despite the relatively low density (below 641 kg/m3). An industrial method of increasing the mechanical strength by steam curing fresh concrete was applied.

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