Effect of Particle Size and Application Pressure in Air-Borne Particle Abrasion on the Adhesion of Polyetheretherketone.

INTRODUCTION: This study aims to investigate the effect of different particle sizes and pressures on the shear bond strength (SBS) and the roughness (Ra) of polyetheretherketone. MATERIALS AND METHODS: A total of 117 polyetheretherketone specimens were fabricated and divided into a control (CN: no air-particle abrasion) and eight pre-treatment groups (air-abraded with 50- or 110-µm Al2O3 particles at 1(A), 1.5(B), 2(C), and 2.5(D) bar). The adhesive, Visio.link was used. Thermal aging was performed. Surface properties, SBS and failure mode were assessed. Data was analyzed by linear regression, Pearson correlation and Dunnett's T3 test for pairwise comparisons (p⟨0.05). RESULTS: The highest and lowest Ra were found in the 110D and CN groups respectively, and the highest SBS results were obtained from the 50B group. Pressure and particle size showed significant difference on the investigated properties (p⟨0.001). Only adhesive failure was observed in the CN, and resin cohesive failure was observed in addition to adhesive failure in the overall study groups. CONCLUSION: The air-borne particle abrasion procedures and the adhesive material combination are critical to the strength of the polyetheretherketone bond. The combination of visio.link with the pre-treatment option of 50-µm Al2O3 particles applied at 1.5-bar pressure delivered the most favorable results.

Comparison of the Color Change of Porcelain Laminate Veneers Produced by Different Materials After Luting with Three Resin Cements.

OBJECTIVES: This study aimed to compare color change of porcelain laminate veneers fabricated with two lithium disilicate ceramics and a zirconia-reinforced lithium silicate ceramic material after luting with conventional dual-cure, amine-free dual-cure, or light-cure resin cements using artificial accelerated aging (AAA). METHODS AND MATERIALS: Ninety noncarious human maxillary central incisors were embedded in autopolymerizing acrylic resin blocks to prepare conventional laminate veneers with incisal coverage. Prepared teeth were randomly divided into 3 groups (n=30) to fabricate laminate veneer restorations using: (1) lithium disilicate ceramic, (2) lithium disilicate ceramic with high-density micronization, and (3) zirconia-reinforced lithium silicate ceramic. Impressions of the preparations were taken with a laboratory scanner. Acquired 3D images were processed into a surface tessellation language file. Data were exported for 3D printing on a printer, and laminate veneers were printed in castable wax resin. Ceramic veneers were heat-pressed after investment according to the manufacturer's recommendations and further divided into three groups (n=10) according to luting cement type: (1) light-cure resin cement, (2) amine-free dual-cure resin cement, and (3) conventional dual-cure resin cement. Color measurements were performed from the middle of each specimen with a spectrophotometer before and after AAA for 300 hours with a total energy of 150 kJ/m2. Color changes were calculated with the CIEDE 2000 (ΔE00) formula. Color differences were assessed using two-way analysis of variance (ANOVA) (α=0.05), and the paired t-test was used to compare the L*, a*, and b* parameters in each group before and after aging. RESULTS: There were no significant differences between the ceramic groups (p>0.05). The color changes of the materials ranged from 2.26 to 3.13. All materials were above the clinically acceptable limit (ΔE00>1.8). The conventional dual-cure resin cement group showed more color change (p>0.05). CONCLUSIONS: Color changes were observed in all porcelain laminate veneers after artificial accelerated aging. The zirconia-reinforced lithium silicate veneers showed similar color changes as lithium disilicate veneers; the amine-free dual-cure resin cement showed a similar color change as light-cure resin cement after aging.