The effect of warm air-blowing on the microtensile bond strength of one-step self-etch adhesives to root canal dentin.

PURPOSE: The use of warm air-blowing to evaporate solvents of one-step self-etch adhesive systems (1-SEAs) has been reported to be a useful method. The purpose of this study was to evaluate the effect of warm air-blowing on root canal dentin. METHODS: Four 1-SEAs (Clearfil Bond SE ONE, Unifil Core EM self-etch bond, Estelink, BeautiDualbond EX) were used. Each 1-SEA was applied to root canal dentin according to the manufacturers' instructions. After the adhesives were applied, solvent was evaporated using either normal air (23±1°C) or warm air (80±1°C) for 20s, and resin composite was placed in the post spaces. The air from the dryer, which could be used in normal- or hot-air-mode, was applied at a distance of 5cm above the root canal cavity in the direction of tooth axis. The temperature of the stream of air from the dryer in the hot-air-mode was 80±1°C, and in the normal mode, 23±1°C. After water storage of the specimens for 24h, the µTBS were evaluated at the coronal and apical regions. The µTBSs were statistically analyzed using three-way ANOVA and Student's t-test with Bonferroni correction (α=0.05). RESULTS: The warm air-blowing significantly increased the µTBS of all 1-SEAs at the apical regions, and also significantly increased the µTBS of two adhesives (Estelink and BeautiDualBond EX) at coronal regions. CONCLUSIONS: The µTBS of 1-SEAs to root canal dentin was improved by using warm air-blowing.

Effect of air-drying dentin surfaces on dentin bond strength of a solvent-free one-step adhesive.

The purpose was to evaluate the effect of air-drying dentin surfaces on the microtensile bond strength (µTBS) of a solvent-free onestep adhesive (Bond 1 SF). Twelve human molars were ground with 600-grit SiC paper. Before applying bonding agent, the dentin surface was rinsed with distilled water and blot-dried with tissue paper, followed by air-drying for 0, 3, 30, and 60 s using with a dental air syringe. After applying and curing Bond 1 SF, resin composite was incrementally built up. Specimens were then stored in distilled water for 24 h and then µTBSs were measured at a cross-head speed of 1 mm/min. Higher µTBS were observed when the dentin surface was air-dried for 3 s (33.2±6.8MPa)>0 s (26.7±4.5MPa)>30 s (22.6±5.5MPa)=60 s (20.4±5.0MPa). The results suggested that prolonged air-drying of the dentin surface removed water and decreased the bond strengths of Bond 1 SF.

The influence of light intensities irradiated directly and indirectly through resin composite to self-etch adhesives on dentin bonding.

This study was designed to evaluate effects of light-irradiated intensities directly and indirectly through resin composites to one- and two-step self-etch adhesives on dentin bonding. One-step (Clearfil S(3) Bond; TS, Bond Force; BF) or two-step (Clearfil SE Bond; SE) self-etch adhesives was applied to dentin surface. The adhesive agent was light-cured with light-intensity of 350 or 600 mW/cm(2), and then resin composite with different colors (translucent or opaque shade) was filled and light-cured with the same light-intensity as the bonding procedure. After 24 h water storage, bond strengths to dentin were determined using µTBS test. For the 600 and 350 mW/cm(2) groups, translucent shade resin obtained higher µTBS than opaque shade resin. Using SE and BF, the 350 mW/cm(2) group in translucent shade resin was higher µTBS than the 600 mW/cm(2) group in opaque shade resin, while TS showed no different µTBS between them.

Dentin bond durability and water sorption/solubility of one-step self-etch adhesives.

The purpose of this study was to evaluate the dentin bonding durability of three HEMA-containing one-step self-etch adhesives after one-year water storage and to measure the amounts of their water sorption/solubility. OptiBond All-In-One (OP), Bond Force (BF) and Clearfil S³Bond (S³) were applied to the dentin surfaces according to manufacturers' instructions. Bond strengths to dentin were determined using µTBS test after water storage for 24 hours, six months, and one year. In addition, water sorption and solubility of the polymerized adhesives were measured. The µTBS of S³ and OP significantly decreased after one year. On the other hand, for BF there were no significant differences in µTBS between all storage periods. There were significant differences in water sorption and solubility among the adhesives (BF>S³>OP). The initial amounts of water sorption and solubility of the three adhesives did not affect their bonding durability to dentin.

Effect of filler content of flowable composites on resin-cavity interface.

The purpose of this in vitro study was to evaluate marginal integrity and wall adaptation in 1- and 2-mm-deep cavities restored with a high filler-loaded flowable composite in comparison to a flowable composite with lower filler content and a conventional hybrid composite. 1-mm-deep dentin and 2-mm-deep enamel-dentin Class I cavities were prepared and restored with a self-etch adhesive and with one of the composites. Samples were crosscut and evaluated for marginal integrity and gap formation using a digital microscope. Selected samples were also observed using a scanning electron microscope. For 1-mm-deep cavities, no differences in marginal integrity and wall adaptation were observed among the three composites. For 2-mm-deep cavities, those restored with the bulk technique and with the higher filler-loaded flowable composite demonstrated a similar outcome as that of the conventional hybrid composite. On the effect of restorative techniques, cohesive enamel defects were observed in bulk-filled 2-mm-deep cavities. However, when the incremental technique was used in conjunction with the higher filler-loaded flowable composite and the conventional hybrid composite for 2-mm-deep cavities, superior results were obtained.

Effects of light sources and visible light-activated titanium dioxide photocatalyst on bleaching.

The objective of this study was to evaluate, using methylene blue (MB), the effects of various light sources on the bleaching action of hydrogen peroxide (H(2)O(2)) with two titanium dioxide (TiO(2)) photocatalysts - an ultraviolet light-activated TiO(2) photocatalyst (UVTiO(2)) versus a visible light-activated TiO(2) photocatalyst (VL-TiO(2)). Five experimental solutions (VL-TiO(2)+H(2)O(2), UV-TiO(2)+H(2)O(2), H(2)O(2), VL-TiO(2), UV-TiO(2)) were prepared by mixing varying concentrations of H(2)O(2 )and/or TiO(2 )photocatalyst with MB solution. For H(2)O(2)-containing solutions (VL-TiO(2)+H(2)O(2), UV-TiO(2)+H(2)O(2), and H(2)O(2)), the concentration of H(2)O(2) was adjusted to 3.5%. For the four different light sources, low- and high-intensity halogen lamps and blue LED LCUs were used. All the experimental solutions were irradiated by each of the light sources for 7 minutes, and the absorbance at 660 nm was measured every 30 seconds to determine the concentration of MB as an indicator of the bleaching effect. On the interaction between the effects of light source and bleaching treatment, the high-intensity halogen with VL-TiO(2)+H(2)O(2) caused the most significant reduction in MB concentration. On the effect of light sources, the halogen lamps resulted in a greater bleaching effect than the blue LED LCUs.

Influence of abrasive particle size on surface properties of flowable composites.

The purpose of this investigation was to measure and compare both the surface roughness and gloss of flowable composites polished with standardized silicone carbide (SiC) papers. Four flowable and two conventional composites were used in this study. Polymerized specimens were subjected to a polishing procedure comprising 12 sequential steps from coarser to finer grits of SiC paper. At the initial polishing stage, flowable composites were more sensitive to the size of the polishing particles and thus yielded surfaces rougher than the conventional composites. Surface roughness became stable when polishing particles less than 13 microm size were used. However, although surface roughness was reduced, an esthetic gloss quality was not achieved on the resultant polished surface. On the influence of filler shape, composites with spherical fillers seemed to have the upper-hand advantage of attaining a high gloss by polishing. On the influence of polishing particle size, it was suggested that polishing should be completed with polishing particles less than 12 microm size so as to achieve clinically satisfactory surface roughness and gloss.

Effect of incremental filling technique on adhesion of light-cured resin composite to cavity floor.

The purpose of this study was to evaluate the effect of various incremental filling techniques on adhesion between composite and cavity floor using light-cured resin composite. Black ABS resin and hybrid resin composite were used as mold materials--instead of dentin--for the preparation of cavities, and standardized to 5x5x5 mm. Each cavity was then treated with a bonding system (Clearfil SE bond). Resin composite (Clearfil Photo Core) was placed on the bonding resin using different incremental filling techniques or in bulk and irradiated for a total of 80 seconds using a halogen light unit. Specimens were subjected to the micro-tensile bond test at a crosshead speed of 1 mm/min. Data were analyzed by two-way ANOVA. The results indicated that an incremental filling technique was more effective in improving adhesion to the cavity floor than a bulk filling technique.

Influence of elasticity on gap formation in a lining technique with flowable composite.

The purpose of this study was to investigate the effect of flowable composites as liners for direct composite restorations, with key focus on the elastic moduli of flowable and condensable composites. After treating the composite mold cavity surface with an adhesive system, one of the flowable composites was placed as a 1 mm-thick layer on the cavity floor and irradiated for 20 seconds. The rest of cavity was subsequently filled with a condensable composite and irradiated for 40 seconds. Gap formation at both interfaces--between the cavity floor and flowable composite, and between the flowable and condensable composites--was examined. No gaps were detected at the interface between the cavity floor and flowable composite. Gap percentage at the interface between the flowable and condensable composites was dependent on the difference in elastic modulus. It was concluded that flowable composite with high elastic modulus could inhibit gap formation between flowable and condensable composites.