Impact of construction parameters on ergonomic and thermo-physiological comfort performance of knitted occupational compression stocking materials.

This work investigates the effect of varying the knitting structure and stitch length (SL) on various thermo-physiological and ergonomic comfort properties of the occupational graduated compression socks. Thermo-physiological comfort, ergonomic comfort and dimensional stability of theses stockings were analysed in a comparative manner. Obtained results were evaluated statistically using the technique of analysis of variance (ANOVA). A Fisher's multiple comparison test was commissioned to analyze the relationship between the alteration of stitch length (SL) on various utility functions and properties desired in the occupational compression socks. In order to examine whether the difference of stitch length is significant, p values were determined. Further the influence of knitting structures e.g., plain, 2 × 2 Rib and 1 × 3 Rib was analysed on the selected properties. The interactive effect of both stitch length (SL) and knitting structure was studied using statistical techniques. It was concluded that knitting structure has a stronger impact on thermo-physiological and ergonomic comfort properties. Results showed a significant variation in thermo-physiological and ergonomic comfort by altering stitch length by means of the statistical analysis. An innovative approach for the manufacturers has been developed for optimizing performance in compression stockings. The construction of the compression socks can thus be optimized in terms of constructional parameters to provide optimum comfort to the users.

Facile-Solution-Processed Silicon Nanofibers Formed on Recycled Cotton Nonwovens as Multifunctional Porous Sustainable Materials.

Limited efficiency, lower durability, moisture absorbance, and pest/fungal/bacterial interaction/growth are the major issues relating to porous nonwovens used for acoustic and thermal insulation in buildings. This research investigated porous nonwoven textiles composed of recycled cotton waste (CW) fibers, with a specific emphasis on the above-mentioned problems using the treatment of silicon coating and formation of nanofibers via facile-solution processing. The findings revealed that the use of an economic and eco-friendly superhydrophobic (contact angle higher than 150°) modification of porous nonwovens with silicon nanofibers significantly enhanced their intrinsic characteristics. Notable improvements in their compactness/density and a substantial change in micro porosity were observed after a nanofiber network was formed on the nonwoven material. This optimized sample exhibited a superior performance in terms of stiffness, surpassing the untreated samples by 25-60%. Additionally, an significant enhancement in tear strength was observed, surpassing the untreated samples with an impressive margin of 70-90%. Moreover, the nanofibrous network of silicon fibers on cotton waste (CW) showed significant augmentation in heat resistance ranging from 7% to 24% and remarkable sound absorption capabilities. In terms of sound absorption, the samples exhibited a performance comparable to the commercial standard material and outperformed the untreated samples by 20% to 35%. Enhancing the micro-roughness of fabric via silicon nanofibers induced an efficient resistance to water absorption and led to the development of inherent self-cleaning characteristics. The antibacterial capabilities observed in the optimized sample were due to its superhydrophobic nature. These characteristics suggest that the proposed nano fiber-treated nonwoven fabric is ideal for multifunctional applications, having features like enhanced moisture resistance, pest resistance, thermal insulation, and sound absorption which are essential for wall covers in housing.

An Analysis of the Performance and Comfort Properties of Fire-Protective Material by Using Inherently Fire-Retardant Fibers and Knitting Structures.

This paper investigates the development of fabric materials using several blends of inherently fire-resistant (FR) fibers and various knitted structures. The samples are evaluated with respect to their performance and comfort-related properties. Inherently fire-resistant fibers, e.g., Nomex, Protex, carbon and FR viscose, were used to develop different structures of knitted fabrics. Cross-miss, cross-relief, and vertical tubular structures were knitted by using optimum fiber blend proportions and combinations of stitches. Several important aspects of the fabric samples were investigated, e.g., their physical, mechanical and serviceability performance. Thermo-physiological and tactile/touch-related comfort properties were evaluated in addition to flame resistance performance. An analysis of mechanical performance indicated that the knitted structure has a significant influence on the tensile strength, bursting strength and pilling resistance. The cross-relief structure proved to be the strongest followed by the cross-miss and vertical tubular structures. The FR station suits made from 70:30 Protex/Nomex exhibited the best combination of tensile and bursting strength; therefore, this material is recommended for making a stable and durable station suit. Interestingly, it was also concluded from the experimental study that knitted samples with a cross-relief structure exhibit the best fire-resistance performance. Fiber blends of 70:30 Protex/Nomex and 70:30 Nomex/carbon were found to be optimum in terms of overall performance. The best flame resistance was achieved with Nomex:carbon fiber blends. These results were confirmed with vertical flammability tests, TGA, DTGA and cone calorimetry analysis. The optimization of blend composition as well as knitting structure/architecture is a crucial finding toward designing the best FR station suit in terms of mechanical, dimensional, thermal, thermo-physiological and flame resistance performance.

Taguchi-TOPSIS based optimization of comfort in compression stockings for vascular disorders.

Compression stockings/socks are one of the most essential materials to treat vascular disorders in veins. However, the comfort of wearing such stockings over prolonged period of time is a major problem. There is limited research in the area of comfort optimization while retaining the compressional performance. The current work is carried out with an aim to determine the optimum level of the input factors e.g., knitting structure, plaiting yarn linear density and main yarn linear density for achieving desired stretch recovery percentage and thermo-physiological comfort properties of compression socks used in treatment of vascular disorders. Their optimum combination was determined by using Taguchi based techniques for order of preference by similarity to ideal solution i.e., TOPIS. In this study, thickness, areal density, air permeability, thermal resistance, over all moisture management capacity (OMMC), stretch and recovery % were optimized simultaneously by using Taguchi-TOPSIS method. The results showed that linear density of plaiting and main yarn has significant influence on all the comfort related properties for compression stockings/socks. The optimum sample had linear density 20 denier for Lycra covered by 70 denier of nylon 66 in the plaiting yarn. It also suggested 120 denier nylon 66 in the main yarn knitted into a plain single jersey structure. The percentage contribution of the factors i.e., structure, plaiting yarn linear density and main yarn linear density was obtained by using ANOVA which are 7%, 31% and 42% respectively. It is worth mentioning that in case of compression stockings, the main yarn linear density has more significant effect on comfort properties as compared to other independent parameters. The results were verified by experiment, and the accuracy was relatively high (maximum error 8.533%). This study helped to select suitable knit structure with the change of linear densities of plaiting yarn and main yarn for comfortable compression stocking/sock and will fulfill the potential requirement for treatment of venous/vascular disorders. The novel methodology involving TOPSIS method helped in analyzing the cumulative contribution of the input parameters to achieve optimum compression as well as comfort performance. This modern approach is based on contemporary scientific principles and statistical approximations. This study may provide benchmark solutions to complex problems involving multiple interdependent criteria.

Numerical and Experimental Analysis of Mechanical Properties in Hybrid Epoxy-Basalt Composites Partially Reinforced with Cellulosic Fillers.

The current work is focused on numerical and experimental studies of woven fabric composites modified by hybridisation with biological (cellulosic) filler materials. The mechanical performance of the composites is characterized under tensile, bending and impact loads and the effect of hybridisation is observed with respect to pure and nonhybrid composites. Numerical models are developed using computational tools to predict mechanical performance under tensile loading. The computational prediction results are compared and validated with relevant experimental results. This research is aimed at understanding the mechanical performance of basalt-epoxy composites partially reinforced with micro-/nano-sized bio-fillers from cellulose and intended for various application areas. Different weave structures, e.g., plain, twill, matt, etc., were investigated with respect to the mechanical properties of the hybrid composites. The effects of hybridizing with cellulose particles and different weave patterns of the basalt fabric are studied. In general, the use of high-strength fibres such as basalt along with cellulosic fillers representing up to 3% of the total weight improves the mechanical performance of the hybrid structures. The thermomechanical performance of the hybrid composites improved significantly by using basalt fabric as well as by addition of 3% weight of cellulosic fillers. Results reveal the advantages of hybridisation and the inclusion of natural cellulosic fillers in the hybrid composite structures. The material developed is suitable for high-end applications in components for construction that demand advanced mechanical and thermomechanical performance. Furthermore, the inclusion of biodegradable fillers fulfills the objectives of sustainable and ecological construction materials.

Evaluation of Mechanical Properties and Filler Interaction in the Field of SLA Polymeric Additive Manufacturing.

The paper deals with research focused on the use of fillers in the field of polymeric materials produced by additive technology SLA (stereolithography). The aim of the research is to evaluate 3D printing parameters, the mechanical properties (tensile strength, hardness), and the interaction of individual phases (polymer matrix and filler) in composite materials using SEM analysis. The tested fillers were cotton flakes and ground carbon fibres in different proportions. For the photosensitive resins, the use of cotton flakes as filler was found to have a positive effect on the mechanical properties not only under static but also under cyclic loading, which is a common cause of material failure in practice. The cyclic stress reference value was set at an amplitude of 5-50% of the maximum force required to break the pure resin in a static tensile test. A positive effect of fillers on the cyclic stress life of materials was demonstrated. The service life of pure resin was only 168 ± 29 cycles. The service life of materials with fillers increased to approximately 400 to 540 cycles for carbon fibre-based fillers and nearly 1000 cycles for cotton flake-based fillers, respectively. In this paper, new composite materials suitable for the use of SLA additive manufacturing techniques are presented. Research demonstrated the possibilities of adding cotton-based fillers in low-cost, commercially available resins. Furthermore, the importance of material research under cyclic loading was demonstrated.

Optimization of seismic performance in waste fibre reinforced concrete by TOPSIS method.

For a sustainable environment and to tackle the pollution problem, industrial wastes can be used in concrete composite materials. This is especially beneficial in places prone to earth quack and lower temperature. In this study, five different types of waste fibres such as polyester waste, rubber waste, rock wool waste, glass fibre waste and coconut fibre waste were used as an additive in 0.5% 1%, and 1.5% by mass in concrete mix. Seismic performance related properties of the samples were examined through evaluation of compressive strength, flexural strength, impact strength, split tensile strength, and thermal conductivity. Results showed that, impact strength of the concrete significantly improved by the addition of fibre reinforcement in concrete. Split tensile strength and flexural strength were significantly reduced. Thermal conductivity was also influenced by addition of polymeric fibrous waste. Microscopic analysis was performed to examine the fractured surfaces. In order to get the optimum mix ratio, multi response optimization technique was used to determine the desired level of impact strength at an acceptable level of other properties. Rubber waste was found to be the most attractive option followed by coconut fibre waste for the seismic application of concrete. The significance and percentage contribution of each factor was obtained by Analysis of variance ANOVA (α = 0.05) and pie chart which showed that Factor A (waste fibre type) is the main contributor. Confirmatory test was done on optimized waste material and their percentage. The order preference similarity to ideal solution (TOPSIS) technique was used for developed samples to obtain solution (sample) which is closest to ideal as per given weightage and preference for the decision making. The confirmatory test gives satisfactory results with error of 6.68%. Cost of reference sample and waste rubber reinforced concrete sample was estimated, which showed that 8% higher volume was achieved with waste fibre reinforced concrete at approximately same cost as pure concrete. Concrete reinforced with recycled fibre content is potentially beneficial in terms of minimizing resource depletion and waste. The addition of polymeric fibre waste in concrete composite not only improves seismic performance related properties but also reduces the environmental pollution from waste material which has no other end use.

Influence of Alkali Treatment of Jatropha Curcas L. Filler on the Service Life of Hybrid Adhesive Bonds under Low Cycle Loading.

The aim of this research was to evaluate the effect of untreated and 5% aqueous NaOH solution-treated filler of the plant Jatropha Curcas L. on the mechanical properties of adhesive bonds, especially in terms of their service life at different amplitudes of cyclic loading. As a result of the presence of phorbol ester, which is toxic, Jatropha oilseed cake cannot be used as livestock feed. The secondary aim was to find other possibilities for the utilization of natural waste materials. Another use is as a filler in polymer composites, that is, in composite adhesive layers. The cyclic loading of the adhesive bonds was carried out for 1000 cycles in two amplitudes, that is, 5-30% of the maximum force and 5-50% of the maximum force, which was obtained by the static tensile testing of the adhesive bonds with unmodified filler. The static tensile test showed an increase in the shear strength of the adhesive bonds with alkali-treated filler compared to the untreated filler by 3-41%. The cyclic test results did not show a statistically significant effect of the alkaline treatment of the filler surface on the service life of the adhesive bonds. Positive changes in the strain value between adhesive bonds with treated and untreated filler were demonstrated at cyclic stress amplitudes of 5-50%. SEM analysis showed the presence of interlayer defects in the layers of the tested materials, which are related to the oil-based filler used.

Research on Low-Cycle Fatigue Engineered Hybrid Sandwich Ski Construction.

This research is aimed at evaluating the effect of low-cycle fatigue on a newly designed hybrid sandwich ski structure to determine the changes that may occur due to cyclic loading and thus affect its use. This is primarily concerned with the fatigue behavior of the tested ski over different time intervals simulating its seasonal use and its effect on the mechanical properties of the ski, i.e., the durability and integrity of the individual layers of the sandwich ski structure. The ski was subjected to 70,000 deflections by moving the crossbar by 60 mm according to the ski deflection calculation in the arch. The results of the cyclic tests of the engineered ski design showed no significant changes in the ski during loading. The average force required to achieve deflection in the first 10,000 cycles was 514.0 ± 4.2 N. Thereafter, a secondary hardening of the structure occurred during relaxation and the force required increased slightly to 543.6 ± 1.7 N. The required force fluctuated slightly during the measurements and in the last series the value was 540.4 ± 0.8 N. Low-cycle fatigue did not have a significant effect on the mechanical properties of the ski; there was no change in shape or visual delamination of the individual layers of the structure. From the cross-section, local delamination was demonstrated by image analysis, especially between the Wood core and the composite layers E-Glass biaxial and Carbon triaxial.

Exploration of Effects of Graduated Compression Stocking Structures on Performance Properties Using Principal Component Analysis: A Promising Method for Simultaneous Optimization of Properties.

This paper focuses on the comfort properties of graduated and preventive compression stockings for people who work long hours in standing postures and for athletes for proper blood circulation. The present study was conducted in order to investigate the effects of the yarn insertion density and inlaid stitches on the performance of the compression stockings. The effects of these parameters on the thermo-physiological comfort properties were tested with standard and developed methods of testing. All compression stockings were maintained with class 1 pressure as per German standards. The structural parameters of the knitted fabric structures were investigated. The stretching and recovery properties were also investigated to determine the performance properties. The theoretical pressure was predicated using the Laplace's law by testing the stockings' tensile properties. The compression interface pressures of all stockings were also investigated using a medical stocking tester (MST) from Salzmann AG, St. Gallen, Switzerland. Correlation between the theoretical pressures and pressures measured using the MST system were also assessed. The current research used a multi-response optimization technique, i.e., principal component analysis (PCA), to identify the best structure based on the optimalization of the above-mentioned properties. The results also revealed that samples with higher insertion density levels exhibit better comfort properties. The results showed that sample R1 was the best sample, followed by R2 and P. In addition, all developed stocking samples exhibited better comfort properties than the control sample from the market.

Low-Cycle Fatigue Behavior of 3D-Printed PLA Reinforced with Natural Filler.

Additive production is currently perceived as an advanced technology, where intensive research is carried out in two basic directions-modifications of existing printing materials and the evaluation of mechanical properties depending on individual production parameters and the technology used. The current research is focused on the evaluation of the fatigue behavior of 3D-printed test specimens made of pure PLA and PLA reinforced with filler based on pinewood, bamboo, and cork using FDM (fused deposition modeling) technology. This research was carried out in response to the growing demand for filaments from biodegradable materials. This article describes the results of tensile fatigue tests and image analysis of the fracture surface determined by the SEM method. Biodegradable PLA-based materials have their limitations that influence their applicability in practice. One of these limitations is fatigue life, which is the cyclic load interval exceeding 50% of the tensile strength determined in a static test. Comparison of the cyclic fatigue test results for pure PLA and PLA reinforced with natural reinforcement, e.g., pinewood, bamboo, and cork, showed that, under the same loading conditions, the fatigue life of the 3D-printed specimens was similar, i.e., the filler did not reduce the material's ability to respond to low-cycle fatigue. Cyclic testing did not have a significant effect on the change in tensile strength and associated durability during this loading interval for PLA-based materials reinforced with biological filler. Under cyclic loading, the visco-elastic behavior of the tested materials was found to increase with increasing values of cyclic loading of 30%, 50% and 70%, and the permanent deformation of the tested materials, i.e., viscoelastic behavior (creep), also increased. SEM analysis showed the presence of porosity, interlayer disturbances, and at the same time good interfacial compatibility of PLA with the biological filler.

Service Life of Adhesive Bonds under Cyclic Loading with a Filler Based on Natural Waste from Coconut Oil Production.

The research is focused on the evaluation of mechanical properties of adhesive bonds with a composite layer of adhesive to increase their service life (safety) under cyclic loading of different intensities. Cyclic loading represents a frequent cause of adhesive bond failure and, thus, a reduction in their service life. Waste from the production of coconut oil, that is, coconut shells in the form of particles, was used as a filler. Coconut shells are in most cases incinerated or otherwise uselessly incinerated, but they can also be used as a natural filler. Cyclic loading (quasi-static tests) was performed for 1000 cycles in two intensities, that is, 5-30% (157-940 N) of maximum force and 5-50% (157-1567 N) of maximum force. The results of the experiment showed a positive effect of the added filler, especially at an intensity of 5-50%, when the service life of adhesive bonds with a composite adhesive layer (AB10, AB20, AB30) increased compared to adhesive bonds without added AB0 filler, which did not withstand the given intensity. A more pronounced viscoelastic behavior of adhesive bonds was demonstrated at an intensity of 5-50% between the 1st and 1000th cycle. SEM analysis showed reduced wetting of the filler and matrix and delamination due to cyclic loading.

Effect of Waterjet Machining Parameters on the Cut Quality of PP and PVC-U Materials Coated with Polyurethane and Acrylate Coatings.

The article focuses on the machining of polymeric materials polypropylene (PP) and un-plasticized poly vinyl chloride (PVC-U) after surface treatment with polyurethane and acrylate coatings using waterjet technology. Two types of waterjet technologies, abrasive waterjet (AWJ) and waterjet without abrasive (WJ), were used. The kerf width and its taper angle, at the inlet and outlet of the waterjet from the workpiece, were evaluated. Significant differences between AWJ and WJ technology were found. WJ technology proved to be less effective due to the creation of a nonuniform cutting gap and significant burrs. AWJ technology was shown to be more efficient, i.e., more uniform cuts were achieved compared to WJ technology, especially at a cutting head traverse speed of 50 mm·min-1. The most uniform kerf width or taper angle was achieved for PP + MOBIHEL (0.09°). The materials (PP and PVC-U) with the POLURAN coating had higher values of the taper angle of the cutting gap than the material with the MOBIHEL coating at all cutting head traverse speeds. The SEM results showed that the inappropriate cutting head traverse speed and the associated WJ technology resulted in significant destruction of the material to be cut on the underside of the cut. Delamination of the POLURAN and MOBIHEL coatings from the base material PP and PVC-U was not demonstrated by SEM analysis over the range of cutting head traverse speeds, i.e., 50 to 1000 mm·min-1.

Design, Development, and Characterization of Advanced Textile Structural Hollow Composites.

The research is focused on the design and development of woven textile-based structural hollow composites. E-Glass and high tenacity polyester multifilament yarns were used to produce various woven constructions. Yarn produced from cotton shoddy (fibers extracted from waste textiles) was used to develop hybrid preforms. In this study, unidirectional (UD), two-dimensional (2D), and three-dimensional (3D) fabric preforms were designed and developed. Further, 3D woven spacer fabric preforms with single-layer woven cross-links having four different geometrical shapes were produced. The performance of the woven cross-linked spacer structure was compared with the sandwich structure connected with the core pile yarns (SPY). Furthermore, three different types of cotton shoddy yarn-based fabric structures were developed. The first is unidirectional (UD), the second is 2D all-waste cotton fabric, and the third is a 2D hybrid fabric with waste cotton yarn in the warp and glass multifilament yarn in the weft. The UD, 2D, and 3D woven fabric-reinforced composites were produced using the vacuum-assisted resin infusion technique. The spacer woven structures were converted to composites by inserting wooden blocks with an appropriate size and wrapped with a Teflon sheet into the hollow space before resin application. A vacuum-assisted resin infusion technique was used to produce spacer woven composites. While changing the reinforcement from chopped fibers to 3D fabric, its modulus and ductility increase substantially. It was established that the number of crossover points in the weave structures offered excellent association with the impact energy absorption and formability behavior, which are important for many applications including automobiles, wind energy, marine and aerospace. Mechanical characterization of honeycomb composites with different cell sizes, opening angles and wall lengths revealed that the specific compression energy is higher for regular honeycomb structures with smaller cell sizes and a higher number of layers, keeping constant thickness.

Experimental Investigation of Wavy-Lap Bonds with Natural Cotton Fabric Reinforcement under Cyclic Loading.

This study is focused on the mechanical properties and service life (safety) evaluation of hybrid adhesive bonds with shaped overlapping geometry (wavy-lap) and 100% natural cotton fabric used as reinforcement under cyclic loading using various intensities. Cyclic loading were implemented between 5-50% (267-2674 N) and 5-70% (267-3743 N) from the maximum strength (5347 N) measured by static tensile test. The adhesive bonds were loaded by 1000 cycles. The test results demonstrated a positive influence of the used reinforcement on the mechanical properties, especially during the cyclic loading. The adhesive bonds Tera-Flat withstood the cyclic load intensity from 5-70% (267-3743 N). The shaped overlapping geometry (wavy-lap bond) did not have any positive influence on the mechanical performance, and only the composite adhesive bonds Erik-WH1 and Tera-WH1 withstood the complete 1000 cycles with cyclic loading values between 5-50% (267-2674 N). The SEM analysis results demonstrated a positive influence on the fabric surface by treatment with 10% NaOH aqueous solution. The unwanted compounds (lignin) were removed. Furthermore, a good wettability has been demonstrated by the bonded matrix material. The SEM analysis also demonstrated micro-cracks formation, with subsequent delamination of the matrix/reinforcement interface caused by cyclic loading. The experimental research was conducted for the analysis of hybrid adhesive bonds using curved/wavy overlapping during both static and cyclic loading.

Influence of Alkali Treatment on the Microstructure and Mechanical Properties of Coir and Abaca Fibers.

Composite materials with natural fillers have been increasingly used as an alternative to synthetically produced materials. This trend is visible from a representation of polymeric composites with natural cellulose fibers in the automotive industry of the European Union. This trend is entirely logical, owing to a preference for renewable resources. The experimental program itself follows pronounced hypotheses and focuses on a description of the mechanical properties of untreated and alkali-treated natural vegetable fibers, coconut and abaca fibers. These fibers have great potential for use in composite materials. The results and discussion sections contribute to an introduction of an individual methodology for mechanical property assessment of cellulose fibers, and allows for a clear definition of an optimal process of alkalization dependent on the content of hemicellulose and lignin in vegetable fibers. The aim of this research was to investigate the influence of alkali treatment on the surface microstructure and tensile properties of coir and abaca fibers. These fibers were immersed into a 5% solution of NaOH at laboratory temperature for a time interval of 30 min, 1 h, 2 h, 3 h, 6 h, 12 h, 24 h, and 48 h, rinsed and dried. The fiber surface microstructures before and after the alkali treatment were evaluated by SEM (scanning electron microscopy). SEM analysis showed that the alkali treatment in the NaOH solution led to a gradual connective material removal from the fiber surface. The effect of the alkali is evident from the visible changes on the surface of the fibers.

Quasi-Static Shear Test of Hybrid Adhesive Bonds Based on Treated Cotton-Epoxy Resin Layer.

This research evaluates the mechanical properties of hybrid adhesive bonds with various 100% cotton fabrics in static and quasi-static conditions and the influence of alkali surface treatment (NaOH) of the cotton fabrics on the mechanical properties. Biological fibers in polymers are characterized by low wettability with the matrix, which decreases mechanical properties. Adhesive bonds usually operate in cyclic stress, which causes irreversible failure before maximal strength. In this paper, a quasi-static test was used to load the adhesive bonds in 5-50% (192-1951 N) and 5-70% (192-2732 N) intervals with 1000 cycles. The results of SEM analysis showed good wettability of alkali treated cotton fabric with NaOH solution in hybrid adhesive bonds. The static test proved the influence of reinforcing cotton fabrics on shear tensile strength against pure resin, i.e., sample Erik up to 19% on 14.90 ± 1.15 MPa and sample Tera up to 21% on 15.28 ± 1.05 MPa. The adhesive bonds with pure resin did not resist either quasi-static tests. Reinforcing cotton fabrics resisted both quasi-static tests, even shear tensile strength increases up to 10% on 16.34 ± 1.24 MPa for the fabric Erik. The results of strain difference of adhesive bonds with Tera and Erik confirmed that a lower value of the difference during cyclic loading positively influenced the ultimate shear tensile strength.

Quasi-Static Tests of Hybrid Adhesive Bonds Based on Biological Reinforcement in the Form of Eggshell Microparticles.

The paper is focused on the research of the cyclic loading of hybrid adhesive bonds based on eggshell microparticles in polymer composite. The aim of the research was to characterize the behavior of hybrid adhesive bonds with composite adhesive layer in quasi-static tests. An epoxy resin was used as the matrix and microparticles of eggshells were used as the filler. The adhesive bonds were exposed to cyclic loading and their service life and mechanical properties were evaluated. Testing was performed by 1000 cycles at 5-30% (165-989 N) and 5-70% (165-2307 N) of the maximum load of the filler-free bond in the static test. The results of the research show the importance of cyclic loading on the service life and mechanical properties of adhesive bonds. Quasi-static tests demonstrated significant differences between measured intervals of cyclic loading. All adhesive bonds resisted 1000 cycles of the quasi-static test with an interval loading 5-30%. The number of completed quasi-static tests with the interval loading 5-70% was significantly lower. The filler positively influenced the service life of adhesive bonds at a higher amount of quasi-static tests, i.e., the safety of adhesive bonds increased. The filler had a positive effect on adhesive bonds ABF2, where the strength significantly increased up to 20.26% at the loading of 5-30% against adhesive bonds ABF0. A viscoelasticity characteristic (creep) of the adhesive layer occurred at higher values of loading, i.e., between loading 5-70%. The viscoelasticity behavior did not occur at lower values of loading, i.e., between loading 5-30%.

Material Utilization of Cotton Post-Harvest Line Residues in Polymeric Composites.

This paper deals with a research focused on utilization of microparticle and short-fiber filler based on cotton post-harvest line residues in an area of polymeric composites. Two different fractions of the biological filler (FCR-reinforced cotton filler) of 20 and 100 µm and the filler with short fibers of a length of 700 µm were used in the research. The aim of the research was to evaluate mechanical characteristics of composites and adhesive bonds for the purpose of gaining new pieces of knowledge which will be applicable in the area of material engineering and assessing application possibilities of residues coming into being from agricultural products processing. Mechanical properties of the composite material produced by a vacuum infusion and tested at temperatures 20, 40, and 60 °C and adhesive bonds which were exposed to a low-cyclic loading, i.e., 1000 cycles at 30% to 70% from reference value of the maximum strength, were evaluated. Composite systems with the FCR adjusted in 5% water solution of NaOH showed higher strength values on average compared to untreated FCR. Unsuitable size of the FCR led to a deterioration of the strength. The filler in the form of 700 FCR microfibers showed itself in a positive way to composite materials, and the particle in the form of 20 FCR did the same to adhesive bonds. Results of adhesive bond cyclic tests at higher stress values (70%) demonstrated viscoelastic behavior of the adhesive layer.