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J Mater Sci Mater Med ; 23(2): 349-56, 2012 Feb.
Artigo em Inglês | MEDLINE | ID: mdl-22183790

RESUMO

This paper reports electrochemical polishing (EP) of 316L stainless-steel structures patterned using micro-electro-discharge machining (µEDM) for application to stents including intelligent stents based on micro-electro-mechanical-systems technologies. For the process optimization, 10 µm deep cavities µEDMed on the planar material were polished in a phosphoric acid-based electrolyte with varying current densities and polishing times. The EP condition with a current density of 1.5 A/cm(2) for an EP time of 180 s exhibited the highest surface quality with an average roughness of 28 nm improved from~400 nm produced with high-energy µEDM. The EP of µEDMed surfaces was observed to produce almost constant smoothness regardless of the initial roughness determined by varying discharge energies. Energy-dispersive X-ray spectroscopy was performed on the µEDMed surfaces before and after EP. A custom rotational apparatus was used to polish tubular test samples including stent-like structures created using µEDM, demonstrating uniform removal of surface roughness and sharp edges from the structures.


Assuntos
Eletroquímica/métodos , Aço Inoxidável/química , Materiais Revestidos Biocompatíveis/química , Eletrólitos , Desenho de Equipamento , Teste de Materiais , Microscopia Eletrônica de Varredura/métodos , Miniaturização , Ácidos Fosfóricos/química , Espectrometria por Raios X/métodos , Propriedades de Superfície
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