RESUMO
Cast steel is commonly used to produce structural and safety parts. Foundry processes allow producing parts from scrap steel directly to the required dimensions without any forming operation. Cast components may, however, exhibit macro- and micro-shrinkage porosities. The combined effect of macro- and micro-shrinkages on the fatigue behavior of cast steel has been characterized in the literature. Macro-shrinkages may nowadays be eliminated by adequate positioning of risers. However, micro-shrinkages will always be present in cast steel components. Present work addresses the influence of micro-shrinkage porosity on a G20Mn5 cast steel. G20Mn5 (normalized) ingots have been cast under industrial conditions, but ensuring the absence of macro-porosities. Solidification leads to two very different microstructures prior to the normalization treatment: columnar dendrites beneath the surface (Skin) and equiaxed microstructures close to the center (Core). First, metallographic observations of the whole ingot revealed the same grain size in both areas. Fatigue samples were extracted, by differentiating two sampling volumes corresponding to columnar (S) and equiaxed solidification (C), respectively. The distribution of micro-porosities was determined on all samples by Micro-CT-scans. Core samples exhibit micro-porosities with volumes 1.7 larger than Skin samples. Low cycle fatigue tests (3 levels of fixed plastic strain) were run on both sample series (C, S). Results follow a Manson-Coffin law. Core specimens exhibit lower fatigue life than Skin specimens. The differences in fatigue life have been related successfully to the differences in micro-porosities sizes.
RESUMO
The purpose of the present study is to predict the whole chromatic path traveled by the colors of glossy anodized titanium samples in every specular geometry. It is based on measurements of the samples' reflectance spectra in a limited number of specular geometries, which allow us to obtain the oxide layer structural parameters (thickness, refractive index), which are then put into an optical model to predict the samples' reflectance spectra in every specular geometry. A good color prediction performance is obtained, with an average ΔE94 color distance over all samples and geometries of 1.9. The oxide layer structural parameters are also in good agreement with refractive index values extracted from the literature and thicknesses measured on electron microscopy images of sample sections.
RESUMO
A novel additive surface structuring process is devised, which involves localized, intense femtosecond laser irradiation. The irradiation induces a phase explosion of the material being irradiated, and a subsequent ejection of the ablative species that are used as additive building blocks. The ejected species are deposited and accumulated in the vicinity of the ablation site. This redistribution of the material can be repeated and controlled by raster scanning and multiple pulse irradiation. The deposition and accumulation cause the formation of µm-scale three-dimensional structures that surpass the initial surface level. The above-mentioned ablation, deposition, and accumulation all together constitute the proposed additive surface structuring process. In addition, the geometry of the three-dimensional structures can be further modified, if desirable, by a subsequent substractive ablation process. Microstructural analysis reveals a quasi-seamless conjugation between the surface where the structures grow and the structures additively grown by this method, and hence indicates the mechanic robustness of these structures. As a proof of concept, a sub-mm sized re-entrant structure and pillars are fabricated on aluminum substrate by this method. Single units as well as arrayed structures with arbitrary pattern lattice geometry are easily implemented in this additive surface structuring scheme. Engineered surface with desired functionalities can be realized by using this means, i.e., a surface with arrayed pillars being rendered with superhydrophobicity.
