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1.
Sci Rep ; 8(1): 6982, 2018 May 03.
Artigo em Inglês | MEDLINE | ID: mdl-29725127

RESUMO

An Advanced MOCVD (A-MOCVD) reactor was used to deposit 4.8 µm thick (Gd,Y)BaCuO tapes with 15 mol% Zr addition in a single pass. A record-high critical current density (J c ) of 15.11 MA/cm2 has been measured over a bridge at 30 K, 3T, corresponding to an equivalent (I c ) value of 8705 A/12 mm width. This corresponds to a lift factor in critical current of ~11 which is the highest ever reported to the best of author's knowledge. The measured critical current densities at 3T (B||c) and 30, 40 and 50 K, respectively, are 15.11, 9.70 and 6.26 MA/cm2, corresponding to equivalent Ic values of 8705, 5586 and 3606 A/12 mm and engineering current densities (J e ) of 7068, 4535 and 2928 A/mm2. The engineering current density (J e ) at 40 K, 3T is 7 times higher than that of the commercial HTS tapes available with 7.5 mol% Zr addition. Such record-high performance in thick films (>1 µm) is a clear demonstration that growing thick REBCO films with high critical current density (J c ) is possible, contrary to the usual findings of strong J c degradation with film thickness. This achievement was possible due to a combination of strong temperature control and uniform laminar flow achieved in the A-MOCVD system, coupled with optimization of BaZrO3 nanorod growth parameters.

2.
J Prosthodont ; 18(7): 618-25, 2009 Oct.
Artigo em Inglês | MEDLINE | ID: mdl-19432759

RESUMO

PURPOSE: The purpose of this study was to determine perceptibility and acceptability thresholds for color differences in light and dark skin-colored maxillofacial elastomers. MATERIALS AND METHODS: A total of 15 pairs of light specimens (mimicking white, Asian, and Hispanic skin) and 15 pairs of dark specimens (mimicking African-American skin) were made using skin-colored maxillofacial silicone elastomers, combined with opacifiers and pigments. Color match/mismatch and acceptable/unacceptable mismatch of each pair of specimens were visually evaluated by 45 evaluators under controlled conditions of a viewing booth. Color differences were calculated using CIELAB and CIEDE2000 formulae. After calculating the model parameters, receiver operating characteristics (ROC) curves and area under the ROC curve (AUC) were analyzed. Repeated measures ANOVA and Tukey's HSD test were used in a statistical analysis (alpha= 0.05). RESULTS: CIELAB/CIEDE2000 perceptibility and acceptability thresholds for light specimens were 1.1/0.7 and 3.0/2.1, respectively. Corresponding values for dark specimens were 1.6/1.2 and 4.4/3.1, respectively. Differences in primary specimen color and type of threshold were found to be significant (p < 0.001). Only the primary specimen color effect was found to be significant in AUC comparisons. CONCLUSIONS: Within the limitations of this study, both main effects of threshold type (perceptibility and acceptability) and primary color (light and dark) on 50:50% color-difference thresholds of colored maxillofacial elastomers were found significant for both color-difference formulae used (CIELAB, CIEDE2000). In addition, significant interaction between the two main effects was found, indicating a stronger effect of skin type on acceptability than perceptibility thresholds. Primary specimen color (light vs. dark) was found to be the only significant main effect on the AUC of ROC curves constructed from logistic regression.


Assuntos
Percepção de Cores , Limiar Diferencial , Prótese Maxilofacial , Pigmentação em Prótese/normas , Elastômeros de Silicone , Análise de Variância , Colorimetria/métodos , Humanos , Variações Dependentes do Observador , Curva ROC , Estatísticas não Paramétricas
3.
J Prosthodont ; 16(4): 269-76, 2007.
Artigo em Inglês | MEDLINE | ID: mdl-17451478

RESUMO

PURPOSE: One critical prerequisite for dental shade guides is to match the color range and distribution of human teeth. The purpose of this study was to design computer models for dental shade guides and compare them with an existing shade guide. A targeted coverage error for a newly developed shade guide was DeltaE(ab) < 2 with a corresponding CIE2000 value. MATERIALS AND METHODS: A total of 1064 teeth were evaluated in vivo using an intra-oral spectrophotometer. Shade guide models were designed using different methods for representation of the data set, hierarchical clustering, and nonlinear constrained optimization. Coverage error was calculated for both CIELAB and CIE2000 values. Recorded values were compared with coverage error of Vitapan Classical (VC) shade guide. Wilcoxon signed-rank test for paired samples and linear regression were used in statistical analysis. RESULTS: Coverage error of VC was 4.1 (SD 1.8), ranging from 0.5 to 11.5 DeltaE(ab). Group A shades had the best match for human teeth (43.9%) followed by Groups C (24.1%), B (20.4%), and D (11.7%) shades, respectively. CIELAB coverage error of the newly designed 24-tab shade guide using clustering and optimization was 2.05 (0.95) and 1.96 (0.92), respectively. Corresponding CIE2000 coverage error values were 1.43 (0.68) and 1.40 (0.65), respectively. A significant difference between results obtained using clustering and optimization was determined. CIELAB color differences were greater, but highly correlated as compared with their CIE2000 counterparts (DeltaE(00)= 0.64 x DeltaE(76)+ 0.13, r > 0.99). DISCUSSION: This study demonstrated that, compared with existing shade guides, future shade guides can provide either (a) similar coverage of tooth color with fewer tabs, thus simplifying shade matching procedure, or (b) better coverage of tooth color with a similar number of tabs, in both cases increasing the chances of satisfactory matches and, consequently, better esthetics. CONCLUSIONS: Both clustering and optimization enabled better representation of tooth color as compared with an existing dental shade guide. Optimization outperformed clustering and is therefore recommended as a method of choice for representation of tooth color and designing of dental shade guides.


Assuntos
Planejamento de Prótese Dentária , Pigmentação em Prótese , Dente/anatomia & histologia , Algoritmos , Análise por Conglomerados , Cor , Colorimetria , Simulação por Computador , Planejamento de Prótese Dentária/instrumentação , Estética Dentária , Humanos , Modelos Biológicos , Dinâmica não Linear , Pigmentação em Prótese/instrumentação , Espectrofotometria
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