Development of TEM and SEM high brightness electron guns using cold-field emission from a carbon nanotip.

A newly developed carbon cone nanotip (CCnT) has been used as field emission cathode both in low voltage SEM (30 kV) electron source and high voltage TEM (200 kV) electron source. The results clearly show, for both technologies, an unprecedented stability of the emission and the probe current with almost no decay during 1h, as well as a very small noise (rms less than 0.5%) compared to standard sources which use tungsten tips as emitting cathode. In addition, quantitative electric field mapping around the FE tip have been performed using in situ electron holography experiments during the emission of the new tip. These results show the advantage of the very high aspect ratio of the new CCnT which induces a strong enhancement of the electric field at the apex of the tip, leading to very small extraction voltage (some hundred of volts) for which the field emission will start. The combination of these experiments with emission current measurements has also allowed to extract an exit work function value of 4.8 eV.

Ferromagnetic domain nucleation and growth in colossal magnetoresistive manganite.

Colossal magnetoresistance is a dramatic decrease in resistivity caused by applied magnetic fields, and has been the focus of much research because of its potential for magnetic data storage using materials such as manganites. Although extensive microscopy and theoretical studies have shown that colossal magnetoresistance involves competing insulating and ferromagnetic conductive phases, the mechanism underlying the effect remains unclear. Here, by directly observing magnetic domain walls and flux distributions using cryogenic Lorentz microscopy and electron holography, we demonstrate that an applied magnetic field assists nucleation and growth of an ordered ferromagnetic phase. These results provide new insights into the evolution dynamics of complex domain structures at the nanoscale, and help to explain anomalous phase separation phenomena that are relevant for applications. Our approach can also be used to determine magnetic parameters of nanoscale regions, such as magnetocrystalline anisotropy and exchange stiffness, without bulk magnetization results or neutron scattering data.