Effect of Post-Printing Conditions on the Mechanical and Optical Properties of 3D-Printed Dental Resin.

This study aimed to evaluate the flexural strength (FS), surface wear, and optical properties of 3D-printed dental resins subjected to different post-printing conditions. A total of 240 specimens (2 × 2 × 25 mm³) were 3D-printed using resin materials for permanent (VaresoSmile Crown Plus) VSC and temporary (VaresoSmile Temp) VST restorations. Specimens underwent five post-printing conditions: no post-printing cure; post-cured in a Form Cure curing unit; Visio Beta Vacuum; Ivoclar Targis; or heat-cured (150 °C) for 30 min. Each group of specimens (n = 24) was tested either directly after post-curing, after 24 h of dry storage, or following hydrothermal accelerated aging in boiling water for 16 h. The three-point bending test was used to evaluate the FS. The two-body wear test was performed on 50 disc-shaped specimens (n = 5/group). Surface gloss and translucency were measured for permanent VSC specimens (n = 5/group). SEM/EDS and statistical analyses were performed. The Form Cure device yielded the highest FS and lowest wear depth (p < 0.05). Hydrothermal aging significantly reduced FS. There were no statistical differences in FS and wear values between materials subjected to same post-printing conditions. VSC groups exhibited similar optical properties across different post-printing treatments. Post-printing treatment conditions had a significant impact on the FS and wear of the 3D-printed resin, while optical properties remained unaffected.

Assessing the Efficacy of Novel Fiber-Reinforced Dual-Cure Luting Resins.

Background: Dual-cure resin-based luting materials are increasingly favored in clinical applications due to their capacity to establish a strong bond with natural tooth structure and restorations. This study aimed to examine certain physical and handling characteristics of newly developed experimental dual-cure luting resins reinforced with short fibers (SFRCs) and compare them with commercially available dual-cure luting resins. Material and Methods: Seven dual-cure luting materials were tested (Relyx Ultimate, Duo-Link, eCEMENT, Variolink Esthetic, G-CEM LinkForce, experimental SFRC1, experimental SFRC2). Fourier transform infrared spectroscopy (FTIR) was utilized to determine the degree of monomer conversion (DC%) in the self and light-curing protocol. A rotating disk rheometer measured viscosity at room temperature (22°C) and simulated mouth temperature (35°C). Fracture toughness, flexural strength, and flexural modulus were evaluated using a 3-point bending test. Each luting resin was subjected to the examination of its surface microstructure using scanning electron microscopy (SEM). Analysis of variance (ANOVA) at a significance level of (p = 0.05) was conducted to analyze data. Results: It was revealed that DC% of the tested dual-cure resins was significantly (p< 0.05) affected by the curing mode, the dual-cure SFRC2 having the highest and Relyx having the lowest DC (64%, and 41% respectively). The viscosity of all tested materials decreased with increasing temperature. SFRC2 demonstrated the highest fracture toughness (2.3 MPa m1/2), while Relyx Ultimate, Duo-Link, and eCEMENT exhibited the lowest values (≈ 1 MPa m1/2)(p< 0.05). Both SFRCs and G-CEM link-force exhibited the highest flexural strength values, and SFRCs resulted in the highest flexural modulus values (p<0.05). Conclusions: The experimental fiber-reinforced dual-cure luting resins exhibited superior DC%, fracture toughness, and flexural properties, yet, SFRC2 showed the highest viscosity at elevated temperature. These results highlight the capability of short fiber reinforcement to enhance the mechanical properties of dual-cured resin-based luting materials without compromising handling characteristics. Key words:Dual-cure luting resin; short fibers; degree of conversion; viscosity; fracture toughness; flexural properties.

Load-bearing capacity and wear characteristics of short fiber-reinforced composite and glass ceramic fixed partial dentures.

The aim of this study was to evaluate load-bearing capacity and wear performance of experimental short fiber-reinforced composite (SFRC) and conventional lithium-disilicate CAD/CAM fabricated fixed partial dentures (FPDs). Two groups (n = 12/group) of three-unit CAD/CAM fabricated posterior FPDs were made. The first group used experimental SFRC blocks, and the second group fabricated from lithium-disilicate (IPS e.max CAD). All FPDs were luted on a zirconia testing jig with dual-curing resin cement. Half of FPDs per group were quasi-statically loaded until fracture. The other half experienced cyclic fatigue aging (100.000 cycles, Fmax = 500 N) before loading quasi-statically until fracture. Fracture mode was examined using SEM. Wear test was performed using 15,000 loading cycles. Both material type and aging had a significant effect on the load-bearing capacity of FPDs. Experimental SFRC CAD without fatigue aging had significantly the highest load-bearing capacity (2096 ± 149N). Cyclic fatigue aging decreased the load-bearing capacity of the SFRC group (1709 ± 188N) but increased it for the lithium-disilicate group (1546 ± 155N). Wear depth values of SFRC CAD (29.3µm) were significantly lower compared to lithium-disilicate (54.2µm). Experimental SFRC CAD demonstrated the highest load-bearing capacity before and after cyclic fatigue aging, and superior wear behavior compared to the control material.

Fracture behavior of discontinuous fiber-reinforced composite inlay-retained fixed partial denture before and after fatigue aging.

PURPOSE: To evaluate the fracture behavior of inlay-retained fixed partial dentures (IRFPDs) made of experimental short fiber-reinforced composite (SFRC) computer-aided design/computer-aided manufacturing (CAD/CAM) block before and after cyclic fatigue aging. METHODS: Five groups (n=20/group) of three-unit posterior IRFPDs were fabricated. The first and second groups were CAD/CAM fabricated from experimental SFRC blocks or lithium-disilicate (IPS e.max CAD, IVOCLAR) materials, the third group comprised a three-dimensional-printed composite (Temp PRINT, GC), and the fourth and fifth groups comprised conventional laboratory flowable composite (Gradia Plus, GC) and commercial flowable SFRC (everX Flow, GC), respectively. All IRFPDs were luted into a metal jig with adhesive dual-cure resin cement (RelyX Ultimate, 3M ESPE). Half the IRFPDs per group (n=10) were subjected to fatigue aging for 10,000 cycles. The remaining half were statically loaded until fracture without fatigue aging. The load was applied vertically between triangular ridges of the buccal and lingual cusps. The fracture mode was visually examined using optical and scanning electron microscopy (SEM). Data were statistically analyzed using a two-way analysis of variance (ANOVA) followed by Tukey's HSD test. RESULTS: ANOVA revealed that IRFPDs made of experimental SFRC CAD/CAM had the highest (P<0.05) load-bearing capacity before (2624±463 N) and after (2775±297 N) aging among all groups. Cyclic fatigue aging decreased the load-bearing capacity (P>0.05) of all tested prostheses, except for the experimental SFRC CAD/CAM and conventional laboratory composite IRFPDs (P>0.05). SEM images showed the ability of discontinuous short fibers in the experimental SFRC CAD/CAM composite to redirect and hinder crack propagation. CONCLUSIONS: CAD/CAM-fabricated IRFPDs made of experimental SFRC blocks showed promising performance in clinical testing in terms of fracture behavior.

Effect of Fiber Reinforcement Type on the Performance of Large Posterior Restorations: A Review of In Vitro Studies.

To reinforce extensively prepared cavities, different types of fiber reinforcement are utilized. Polyethylene and glass fibers are the most commonly used fibers in that purpose; each type has its own advantages over the other type. Therefore, the aim of this study is to review the literature to evaluate and compare the influence of different fiber reinforcement types on the performance of posterior large composite restorations. Two independent authors performed a comprehensive literature search using MEDLINE/PubMed, Google Scholar, and a manual search for cross references until July 2021. Authors selected only studies that contain comparisons between glass (continuous or short) and polyethylene (woven) fiber-reinforced composites (FRCs) in posterior cavities of human teeth, and that report the effect of fiber inclusion on fracture resistance, microleakage, and marginal adaptation of restorations. A number of 2711 potentially relevant articles were obtained from the electronic search. After extensive assessment, 2696 articles were ineligible to be included in the review, and only 15 articles met the inclusion criteria. Four out of nine studies, which tested the fracture resistance of FRC restorations, revealed similar performance of the glass and polyethylene fibers. The rest of the studies (n = 5) revealed statistically significant differences between the two types of fiber reinforcement, with the majority showed superior reinforcement of glass fiber. Moreover, the reviewed studies revealed that, using fibers within the composite restorations would reduce the microleakage and improve the marginal adaptation of the restoration regardless of the fiber type. FRCs tend to strengthen the restorations of structurally compromised teeth and improve their performance compared to plain composite restorations.

Shear-bond strength and optical properties of short fiber-reinforced CAD/CAM composite blocks.

The aim of this study was to assess the shear-bond strength (SBS) of resin-luting cement to experimental short fiber-reinforced CAD/CAM composite (SFRC) compared to conventional CAD/CAM (Cerasmart 270), 3D printed (GC TEMP PRINT, Pro3dure GR-17), and laboratory (Gradia Plus) composites. Moreover, translucency parameter values and light transmission were evaluated. For each of the five types of composites, discs were prepared (n = 16/group) and divided into subgroups (n = 8/group) according to surface treatment protocol (hydrofluoric acid or air-particle abrasion). SBS test was performed using universal testing machine until failure, and failure modes were visually analyzed. Translucency parameter and curing-light transmission values through 1, 2, and 3 mm thickness were quantified using spectrophotometry and the MARC resin calibrator, respectively. Scanning electron microscopy (SEM) was used to examine the CAD/CAM composites after surface treatment. Composite type and surface treatment had a significant effect on SBS. Laboratory composite showed the highest SBS value (22.4 MPa). Cerasmart 270 exhibited higher translucency parameter values (19.8, 11.0, 5.0) than SFRC (14.5, 5.2, 1.6) at the three composite thicknesses tested. Air-particle abrasion was more effective in enhancing SBS than acid etching. Experimental SFRC CAD/CAM composite showed higher SBS values than Cerasmart 270. For all composites, translucency parameter values and light transmission decreased as thickness increased.

Comparative evaluation between glass and polyethylene fiber reinforced composites: A review of the current literature.

BACKGROUND: Fiber reinforced composite (FRC) is a promising class of material that gives clinicians alternative treatment options. There are many FRC products available in the market based on either glass or polyethylene fiber type. The aim of this study was to present a comparison between glass and polyethylene fiber reinforced composites based on available literature review. MATERIAL AND METHODS: A thorough literature search, with no limitation, was done up to June 2017. The range of relevant publications was surveyed using PubMed and Google Scholar. From the search results, articles related to our search terms were only considered. An assessment of these articles was done by two individuals in order to include only articles directly compare between glass and polyethylene FRCs. The search terms used were "fiber reinforced dental composites" and "glass and polyethylene fibers in dentistry". RESULTS: The search provided 276 titles. Full-text analysis was performed for 29 articles that met the inclusion criteria. Most were laboratory-based research with various test specimen designs prepared according to ISO standard or with extracted teeth and only three articles were clinical studies. Most of studies (n=23) found superior characteristics of glass FRCs over polyethylene FRCs. CONCLUSIONS: Significant reinforcement differences between commercial glass and polyethylene fiber reinforced composites were found. Key words:Fiber reinforced composite, glass fiber, polyethylene fiber.

Short fiber reinforced composite: a new alternative for direct onlay restorations.

OBJECTIVES: To determine the static load-bearing capacity of direct composite onlay restorations made of novel filling composite resin system which combines short fiber-reinforced composite resin (FC) and conventional particulate filler composite resin (PFC). METHODS: Three groups of onlay restorations were fabricated (n = 8/group); Group A: made from conventional particulate filler composite resin (Z250, 3M-ESPE, USA, control), Group B: made from short fiber-reinforced composite resin (EverX posterior, StickTeck Ltd, member of GC group, Turku, Finland) as substructure with 1 mm surface layer of PFC, Group C: made from FC composite resin. The specimens were incrementally polymerized with a hand-light curing unit for 80 s before they were statically loaded with two different sizes (3 & 6 mm) of steel ball until fracture. Failure modes were visually examined. Data were analyzed using ANOVA (p = 0.05). RESULTS: ANOVA revealed that onlay restorations made from FC composite resin had statistically significantly higher load-bearing capacity (1733 N) ( p < 0.05) than the control PFC composite resin (1081 N). Onlays made of FC composite resin with a surface layer of PFC gave force values of 1405 N which was statistically higher than control group ( p < 0.05). No statistically significant difference was found in the load-bearing capacity between groups loaded by different ball sizes. SIGNIFICANCE: Onlay restorations combining base of short fiber reinforced composite resin as substructure and surface layer of conventional composite resin displayed promising performance in high load bearing areas.