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1.
Ukr Biokhim Zh (1999) ; 71(6): 108-10, 1999.
Artigo em Ucraniano | MEDLINE | ID: mdl-10820857

RESUMO

Data concerning the synthesis of bioactive lipid compound N-([1-14C]-palmitoyl)ethanolamine labeled by 14C fatty acid are reported. The method is based on the ability of ethanolamine and fatty acid to the direct chemical condensation at 180 degrees C with yielding of N-acylethanolamine. The purification of the end product by the double crystallization in ethanol allows to obtain chromatographically pure substance. The presented method of the labeled N-([1-14C]-palmitoyl)ethanolamine synthesis is simple and in extensive that's why it might be used in the area of biologically active compounds investigation.


Assuntos
Fosfatidiletanolaminas/síntese química , Radioisótopos de Carbono , Cromatografia Gasosa , Fosfatidiletanolaminas/química , Fosfatidiletanolaminas/isolamento & purificação
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