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1.
Sci Rep ; 10(1): 7481, 2020 May 04.
Artigo em Inglês | MEDLINE | ID: mdl-32366877

RESUMO

Process control in surface hardening depends greatly on the repeatability of the results. Induction heating facilities stand out in this aspect but challenges arise when it comes to the verification of the expected temperatures. In-situ temperature measurement of a workpiece may be made impossible due to it moving through an enclosed, automated induction facility that lacks built-in sensors. This paper uses transition patterns in the microstructure of the hardened region to reconstruct isothermal contour lines of the temperature field during austenitisation. It does so based on a continuous cooling transformation phase diagram and a time-temperature-austenitisation diagram of the considered steel. The presented method serves as a practical approach to validate simulations of the inductive austenitising process and supports simulations of the heat treatment of the work piece. Once these simulations have been iterated upon and validated thoroughly, they may then yield a reconstruction of the entire temperature field during the heat treatment process.

2.
Dent Mater ; 33(1): 99-109, 2017 01.
Artigo em Inglês | MEDLINE | ID: mdl-27884403

RESUMO

OBJECTIVE: Strength is one of the preferred parameters used in dentistry for determining clinical indication of dental restoratives. However, small dimensions of CAD/CAM blocks limit reliable measurements with standardized uniaxial bending tests. The objective of this study was to introduce the ball-on-three-ball (B3B) biaxial strength test for dental for small CAD/CAM block in the context of the size effect on strength predicted by the Weibull theory. METHODS: Eight representative chairside CAD/CAM materials ranging from polycrystalline zirconia (e.max ZirCAD, Ivoclar-Vivadent), reinforced glasses (Vitablocs Mark II, VITA; Empress CAD, Ivoclar-Vivadent) and glass-ceramics (e.max CAD, Ivoclar-Vivadent; Suprinity, VITA; Celtra Duo, Dentsply) to hybrid materials (Enamic, VITA; Lava Ultimate, 3M ESPE) have been selected. Specimens were prepared with highly polished surfaces in rectangular plate (12×12×1.2mm3) or round disc (Ø=12mm, thickness=1.2mm) geometries. Specimens were tested using the B3B assembly and the biaxial strength was determined using calculations derived from finite element analyses of the respective stress fields. Size effects on strength were determined based on results from 4-point-bending specimens. RESULTS: A good agreement was found between the biaxial strength results for the different geometries (plates vs. discs) using the B3B test. Strength values ranged from 110.9MPa (Vitablocs Mark II) to 1303.21MPa (e.max ZirCAD). The strength dependency on specimen size was demonstrated through the calculated effective volume/surface. SIGNIFICANCE: The B3B test has shown to be a reliable and simple method for determining the biaxial strength restorative materials supplied as small CAD/CAM blocks. A flexible solution was made available for the B3B test in the rectangular plate geometry.


Assuntos
Desenho Assistido por Computador , Porcelana Dentária , Materiais Dentários , Teste de Materiais
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