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1.
Polymers (Basel) ; 16(7)2024 Apr 03.
Artigo em Inglês | MEDLINE | ID: mdl-38611234

RESUMO

The objective of this paper is to investigate the debonding behavior of the interface between continuously and discontinuously fiber reinforced thermoplastics using the climbing drum peel test. The study emphasizes on the importance of considering different climatic boundary conditions on the properties of thermoplastics. Specimens with varying moisture contents, from 0m.% up to above 6m.% are prepared and tested. It is observed that an increase in moisture content from 0m.% to 2m.% results in an increase of the fracture surface energy from 1.07·103J/m2 to 2.40·103J/m2 required to separate the two materials, but a further increase in moisture to 6.35m.% conversely results in a subsequent decrease of the required energy to 1.91·103J/m2. The study presents an explanatory model of increasing plasticization of the polymer due to increased polymer chain mobility, which results in more deformation energy being required to propagate the crack, which is corroborated in SEM investigations of the fracture surface. A further increase in humidity leads to polymer degradation due to hydrolysis, which explains the subsequent reduction of the fracture energy. The experimental set up is modeled numerically for the first time with cohesive surfaces, which could successfully reproduce the effective force-displacement curve in the experiment by varying the interface parameters in the model over an influence length, allowing the conclusion of a process induced variation in the interface properties over a specific consolidation length.

2.
Materials (Basel) ; 14(23)2021 Nov 29.
Artigo em Inglês | MEDLINE | ID: mdl-34885467

RESUMO

The strain rate-dependent behavior of a unidirectional non-crimp fabric (UD-NCF) carbon fiber/snap-cure epoxy composite loaded along the transverse direction under quasi-static and dynamic conditions was characterized. Transverse tension and compression tests at quasi-static and intermediate strain rates were performed using hydraulic testing machines, while a split Hopkinson pressure bar (SHPB) apparatus was used for transverse compression tests at high strain rates. A pulse shaper was used on the SHPB apparatus to ensure dynamic equilibrium was achieved and that the test specimens deformed homogenously with a nearly constant strain rate. The transverse tensile strength at a strain rate of 16 s-1 increased by 16% when compared to that at quasi-static strain rates, while distinct localized fracture surface morphology was observed for specimens tested at different strain rates. The transverse compressive yield stress and strength at a strain rate of 325 s-1 increased by 94% and 96%, respectively, when compared to those at quasi-static strain rates. The initial fracture plane orientation for the transverse compression tests was captured with high-speed cameras and found to increase with increasing strain rate. The study provides an important data set for the strain rate-dependent response of a UD-NCF composite material, while the qualitative fracture surface observations provide a deeper understanding of the failure characteristics.

3.
J Mech Behav Biomed Mater ; 74: 371-382, 2017 10.
Artigo em Inglês | MEDLINE | ID: mdl-28675848

RESUMO

OBJECTIVE: Apply high-resolution benchtop micro-computed tomography (micro-CT) to gain greater understanding and knowledge of the formation of the micro-damage process zone formed during traverse fracture of cortical bone. METHODS: Bovine cortical bone was cut into single edge notch (bending) fracture testing specimens with the crack on the transverse plane and oriented to grow in the circumferential direction. We used a multi-specimen technique and deformed the specimens to various individual secant modulus loss levels (P-values) up to and including maximum load (Pmax). Next, the specimens were infiltrated with a BaSO4 precipitation stain and scanned at 3.57-µm isotropic voxel size using a benchtop high resolution-micro-CT. Measurements of the micro-damage process zone volume, width and height were made. These were compared with the simple Irwin's process zone model and with finite element models. Electron and confocal microscopy confirmed the formation of BaSO4 precipitate in micro-cracks and other porosity, and an interesting novel mechanism similar to tunneling. RESULTS: Measurable micro-damage was detected at low P values and the volume of the process zone increased according to a second order polynomial trend. Both width and height grew linearly up to Pmax, at which point the process zone cross-section (perpendicular to the plane of the crack) was almost circular on average with a radius of approximately 550µm (approximately one quarter of the unbroken ligament thickness) and corresponding to the shape expected for a biological composite under plane stress conditions. CONCLUSION: This study reports details of the micro-damage fracture process zone previously unreported for cortical bone. High-resolution micro-CT enables 3D visualization and measurement of the process zone and confirmation that the crack front edge and process zone are affected by microstructure. It is clear that the process zone for the specimens studied grows to be meaningfully large, confirming the need for the J-integral approach and it does not achieve steady state at Pmax in most specimens. With further development, this approach may become valuable towards better understanding the role of the process zone in cortical bone fracture and the effects of relevant modifications towards changes in fracture toughness in a cost effective way.


Assuntos
Osso Cortical/patologia , Fraturas Ósseas/diagnóstico por imagem , Microtomografia por Raio-X , Animais , Bovinos , Osso Cortical/diagnóstico por imagem , Porosidade
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