1.
J Chromatogr B Analyt Technol Biomed Life Sci
; 855(2): 242-8, 2007 Aug 15.
Artigo
em Inglês
| MEDLINE
| ID: mdl-17560179
RESUMO
A fast and sensitive method for the quantification of the mycotoxin ochratoxin A (OTA) in dry-cured meat products has been developed, which does not require a clean-up step, by HPLC with an alkaline mobile phase (pH 9.8). Validation procedures for specificity, trueness, ruggedness, stability, recovery and repeatability were performed. The decision limit (CC alpha) and the decision capability (CC beta) were calculated at 1.10 and 1.23 microg/kg, respectively. The procedure was applied to representative dehydration levels of dry-cured meat samples.
Assuntos
Cromatografia Líquida de Alta Pressão/métodos , Produtos da Carne/microbiologia , Micotoxinas/análise , Ocratoxinas/análise , Micotoxinas/isolamento & purificação , Ocratoxinas/isolamento & purificação , Reprodutibilidade dos Testes
2.
Angew Chem Int Ed Engl
; 44(32): 5126-30, 2005 Aug 12.
Artigo
em Inglês
| MEDLINE
| ID: mdl-16013071