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1.
Materials (Basel) ; 16(19)2023 Sep 28.
Artigo em Inglês | MEDLINE | ID: mdl-37834602

RESUMO

Ensuring adequate reliability of the production process of packaging closures has made it necessary to study the effect of annealing and varnishing variants on the strength and structural properties of the stock material. As a test material, EN AW-5052-H28 aluminium alloy sheets with a thickness of 0.21 mm were used. The surface treatment of the test material involved varnishing the sheet metal surface using various varnishes and soaking the sheet metal. The coefficient of friction and the abrasion resistance of the coatings were determined using the T-21 ball-and-disc tribotester. The tested sheets were subjected to tribological analysis by the T-05 roller-block tribotester using countersamples made of Caldie and Sverker 21 tool steels. The results of the tests showed differences in mechanical and structural properties depending on the method of sample preparation. Based on the test results, significant differences in the adhesion of anti-wear coatings were found. The results revealed that the most favourable friction conditions are provided by the CrN coating. The (AlTi)N interlayer in the (AlTi)N/(AlCr)N coating adheres to the substrate over the entire tested area and no detachment from its surface was observed, which proves good bonding at the substrate/coating interface. The tested AlTiN/TiAlSiXN coating is characterised by a more homogeneous, compact microstructure compared to the (AlTi)N/(AlCr)N coating.

2.
Materials (Basel) ; 15(21)2022 Oct 27.
Artigo em Inglês | MEDLINE | ID: mdl-36363135

RESUMO

The article presents the results of research on the influence of plastic deformation on the microstructure and tensile strength of Haynes 282 nickel superalloy produced by direct metal laser sintering (DMLS) and a conventional technique (casting). Samples were tested for dimensional accuracy using a 3D scanner. Then, the samples were subjected to plastic deformation by rolling. The microstructures of the DMLS and the as-cast samples were analysed using a scanning electron microscope. The strength properties of the samples were determined in a static tensile test. Microhardness measurements of the samples were also performed. Based on the analysis of the dimensional accuracy, it was found that the surface quality of the components produced by DMLS is dependent on the input parameters of the 3D printing process. Using the DMLS method, it is possible to produce Haynes 282 with a fine-crystalline microstructure containing dendrites. The fine-crystalline dendritic microstructure and low porosity showed very good tensile strength compared to the as-cast material. It was also found that the increase in the degree of plastic deformation of the as-cast Haynes 282 and the samples produced by the DMLS technique resulted in an increase in the strength of the tested samples, with reduced ductility.

3.
Materials (Basel) ; 14(12)2021 Jun 14.
Artigo em Inglês | MEDLINE | ID: mdl-34198565

RESUMO

Recent work indicates that the high-velocity oxy-fuel (HVOF) thermal spraying WC-Co coatings have been used to enhance the wear resistance of various engineering components in a variety of industrial environments. In the present work, WC-Co powder, containing Cr particles in an amount of 10%, was deposited on ductile cast iron with the HVOF thermal spray coating technique. An investigation was conducted to determine the role of Cr particles in the WC-Co coating produced with the HVOF technique on microstructure, mechanical, and wear properties in a system of type: WC-Co coating/ductile cast iron. The microstructure of the HVOF-sprayed WC-Co + Cr coating was characterised by light microscopy, X-ray diffraction (XRD), scanning electron microscope (SEM), transmission electron microscope (TEM), and energy-dispersive X-ray spectroscopy (EDS). The analysis of the microstructure showed the formation of a coating with low porosity, compact structure, and good adhesion to the substrate with a typical lamellar structure composed of fine molten Cr particles and finely fragmented WC grains embedded in a Co matrix, reaching the size of nanocrystalline. The scratch test was applied for the analysis of the adhesion of coatings to the substrate. The erosion behaviour and mechanism of material removal was studied and discussed based on microstructural examinations. Moreover, the results were discussed in relation to the bending strength test, including cracks and delamination in the system of the WC-Co + Cr/ductile cast iron, as microhardness and erosion resistance of the coating. It was found that the addition of Cr particles to the WC-Co powder, which causes hardening of the binder phase is a key influence on increased mechanical and wear properties in the studied system. Additionally, due to the construction of nanostructured coatings, suitable proportion of hard and soft phases, the technique sprayed HVOF coatings have advantageous properties such as high density and good slurry erosion resistance.

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