Chemical analysis on laser processed Ultrahydrophobic Ti-6Al-4V surface by high vacuum Process.

A technique has been developed for fabrication of ultrahydrophobic Ti-6Al-4V surface by vacuum process. This report has the data related to the article "Hybrid laser and vacuum process for rapid ultrahydrophobic Ti-6Al-4 V surface formation" on the fabrication of ultrahydrophobic Ti-6Al-4V by Vacuum process (Jagdheesh et al., 2019). The present data consist of X-ray photo electron spectroscopy spectrums recorded for the laser patterned ultrahydrophobic samples, droplet image and surface chemical composition of laser patterned Ti-6Al-4V samples before vacuum process(b. v. p.) and after vacuum process (a. v. p.) for 120 min. The presented data give a clear idea about the chemical modification evolved during the vacuum process.

On the fatigue behavior of medical Ti6Al4V roughened by grit blasting and abrasiveless waterjet peening.

Flat fatigue specimens of biomedical Ti6Al4V ELI alloy were surface-processed by high pressure waterjet peening (WJP) without abrasive particles using moderate to severe conditions that yield roughness values in the range of those obtained by commercial grit blasting (BL) with alumina particles. Fatigue behavior of WJP and BL specimens was characterized under cyclical uniaxial tension tests (R=0.1). The emphasis was put on a comparative analysis of the surface and subsurface induced effects and in their relevance on fatigue behavior. Within the experimental setup of this investigation it resulted that blasting with alumina particles was less harmful for fatigue resistance than abrasiveless WJP. BL specimens resulted in higher subsurface hardening and compressive residual stresses. Specimens treated with more severe WJP parameters presented much higher mass loss and lower compressive residual stresses. From the analysis performed in this work, it follows that, in addition to roughness, waviness emerges as another important topographic parameter to be taken into account to try to predict fatigue behavior. It is envisaged that optimization of WJP parameters with the aim of reducing waviness and mass loss should lead to an improvement of fatigue resistance.

Optical observation of shock waves and cavitation bubbles in high intensity laser-induced shock processes.

We report an experimental study of the temporal and spatial dynamics of shock waves, cavitation bubbles, and sound waves generated in water during laser shock processing by single Nd:YAG laser pulses of nanosecond duration. A fast ICCD camera (2 ns gate time) was employed to record false schlieren photographs, schlieren photographs, and Mach-Zehnder interferograms of the zone surrounding the laser spot site on the target, an aluminum alloy sample. We recorded hemispherical shock fronts, cylindrical shock fronts, plane shock fronts, cavitation bubbles, and phase disturbance tracks.

Optical characterization of extremely small volumes of liquid in sub-micro-holes by simultaneous reflectivity, ellipsometry and spectrometry.

We have fabricated and characterized a lattice of submicron cone-shaped holes on a SiO(2)/Si wafer. Reflectivity profiles as a function of angle of incidence and polarization, phase shift and spectrometry are obtained for several fluids with different refractive indexes filling the holes. The optical setup allows measuring in the center of a single hole and collecting all data simultaneously, which can be applied for measuring extremely low volumes of fluid (in the order of 0.1 femtolitres) and label-free immunoassays, as it works as a refractive index sensor. A three layer film stack model is defined to perform theoretical calculations.

Laser heat treatments driven by integrated beams: role of irradiation nonuniformities.

An analysis is given of how nonuniformities in the laser beam intensity translate into variations on the induced temperature distribution on an irradiated sample. The study involves materials with different thermal conductivities. By use of a reshaped irradiating beam obtained with a multifaceted integrating mirror, a three-dimensional numerical calculation allows us to establish both surface and in-depth temperature distributions. The results show that in the case of materials such as glass (i.e., with low thermal conductivity) large thermal gradients occur both on the surface and in depth during irradiation. However, the lateral heat flow is high enough to strongly reduce the surface gradients as soon as the laser irradiation ends. Conversely, in good thermal conductors such as nickel, the laser intensity nonuniformities induce a thermal peaking of the surface with lateral thermal gradients that are by no means negligible. Experimental evidence during laser glass polishing that confirms the numerical assessments are also provided.