Effect of gallic acid addition on some mechanical properties of self-adhesive resin cements.

Self-adhesive resin cements (RCs) activate matrix metalloproteinase (MMP) and cathepsin-related collagen degradation, and gallic acid (GA) inhibits the activity of both MMPs and cysteine cathepsins. The purpose of this study was to evaluate the setting time, biaxial flexural strength, and Vickers hardness of self-adhesive RCs after the addition of two different concentrations of GA. RelyX U200 (3M ESPE) and Panavia SA (Kuraray) were modified with 0.5 and 1 wt% GA. The setting time of five samples in each RC group was assessed using a thermocouple apparatus as described in the ISO 4049 test. Biaxial flexure strength was measured using a universal testing machine until failure. Vickers hardness was measured with three randomized indentations on the surface of each resin disc. RCs without GA were used as control. Data were analyzed using a one-way analysis of variance and Tukey's HSD test (α = 0.05). The setting times ranged from 2.4 to 4.6 min for RelyX and from 4.9 to 6.0 min for Panavia. The biaxial flexure strength ranged from 76.5 to 109.7 MPa for RelyX and from 73.3 to 108.2 MPa for Panavia. Vickers hardness values ranged from 41.6 to 58.6 for RelyX and 27.2 to 33.6 for Panavia. The addition of 0.5 and 1 wt% GA to improve durability of resin-dentin bonds had no adverse effects on setting time, whereas the biaxial flexure strength and Vickers hardness values for the tested materials were significantly reduced.

Surface treatment effects on bond strength of CAD/CAM fabricated posts to root canal dentin.

PURPOSE: To compare the effect of different surface treatments on the bond strength of CAD/CAM fabricated resin-based and prefabricated fiber posts to root canal dentin. METHODS: 160 single-rooted human teeth were selected and received endodontic treatment. The teeth were divided into four groups according to the post material used: (1) Prefabricated fiber-reinforced composite post (Snowpost), (2) CAD/CAM nanoceramic (Cerasmart), (3) CAD/CAM polymer infiltrated ceramic (Vita Enamic) and (4) CAD/CAM resin nanoceramic (Lava Ultimate). Then the posts were randomly assigned into four sub-groups according to the surface treatment method used: (1) Control (no treatment), (2) Laser (Er,Cr:YSGG laser device, Waterlase), (3) Hydrofluoric acid treatment [ 9.6% HF (Pulpdent) for 2 minutes], and (4) Sandblasting (50 µm Al2O3). Following post space preparation, posts were cemented with dual-cure resin cement (Panavia SA cement plus). From each root, five 1 mm-thick slices were obtained. The micropush-out bond strength test was performed for each slice. Data were analyzed by using two-way ANOVA and Tukey HSD tests. The fracture modes were evaluated under a stereomicroscope. Representative specimens were analyzed with SEM following surface treatments. RESULTS: Micropush-out bond strength of posts to dentin was significantly affected by the type of post material (P< 0.05), but not by the surface treatment (P= 0.397). CLINICAL SIGNIFICANCE: Posts manufactured by CAD/CAM could be suitable options for restoration of severely affected endodontically-treated teeth.

Effect of Combined Surface Treatments on Surface Roughness and Resin Bond Strength to Y-TZP Ceramic and Nickel-Chromium Metal Alloy.

Objective: This study compared the effects of different surface treatments on the surface roughness (Ra), and shear bond strength (SBS) of resin cement to yttria-stabilized tetragonal zirconia (Y-TZP) ceramic and nickel-chromium (Ni-Cr) base metal alloy, respectively. Materials and methods: Thirty disk-shaped specimens (3 mm height and 10 mm diameter) of each material (Y-TZP and Ni-Cr) were prepared. Both zirconia and metal specimens were randomly assigned to three equal groups, according to the surface treatments (n = 10): sandblasting, sandblasting + Er:YAG laser, and sandblasting + Nd:YAG laser. Resin cement cylinders (4 mm diameter and 3 mm thickness) were placed on each specimen. The SBS tests were performed at a 1 mm per minute crosshead speed through a knife-edge rod after 5000 thermal cycles. The Ra (µm) of the specimens was measured using a profilometer and evaluated topographically by atomic force microscopy and scanning electron microscopy. Analysis of variance, followed by Tukey's honestly significant difference, in addition to the Kruskal-Wallis test, followed by the Mann-Whitney U test, were used for statistical analysis (α = 0.05). Results: Combined sandblasting and laser treatment of the metal groups led to statistically higher Ra values than sandblasting alone (p < 0.05). For Y-TZP, there were no significant differences between the Ra values of the subgroups (p > 0.05). The SBS of the sandblasted metal group was significantly higher than the other two laser-irradiated groups, whereas the SBS of sandblasted zirconia was only significantly higher than the Nd:YAG laser-irradiated group (p < 0.05). Conclusions: Combined laser and sandblasting surface treatments resulted in rougher surfaces than sandblasting alone, especially for the metal specimens. Sandblasting, alone, improved the SBS of resin cement in both metal and zirconia, compared with the laser and sandblasting treatments, combined.

Effect of gallic acid addition on some mechanical properties of self-adhesive resin cements

Abstract Self-adhesive resin cements (RCs) activate matrix metalloproteinase (MMP) and cathepsin-related collagen degradation, and gallic acid (GA) inhibits the activity of both MMPs and cysteine cathepsins. The purpose of this study was to evaluate the setting time, biaxial flexural strength, and Vickers hardness of self-adhesive RCs after the addition of two different concentrations of GA. RelyX U200 (3M ESPE) and Panavia SA (Kuraray) were modified with 0.5 and 1 wt% GA. The setting time of five samples in each RC group was assessed using a thermocouple apparatus as described in the ISO 4049 test. Biaxial flexure strength was measured using a universal testing machine until failure. Vickers hardness was measured with three randomized indentations on the surface of each resin disc. RCs without GA were used as control. Data were analyzed using a one-way analysis of variance and Tukey's HSD test (α = 0.05). The setting times ranged from 2.4 to 4.6 min for RelyX and from 4.9 to 6.0 min for Panavia. The biaxial flexure strength ranged from 76.5 to 109.7 MPa for RelyX and from 73.3 to 108.2 MPa for Panavia. Vickers hardness values ranged from 41.6 to 58.6 for RelyX and 27.2 to 33.6 for Panavia. The addition of 0.5 and 1 wt% GA to improve durability of resin-dentin bonds had no adverse effects on setting time, whereas the biaxial flexure strength and Vickers hardness values for the tested materials were significantly reduced.

Fabrication of a screw-retained hybrid prosthesis following treatment of peri-implant defects: a case report.

The etiology of marginal bone loss around osseointegrated implants is primarily based on the biomechanical and/or microbial factors. If stresses and strains around dental implants under functional loading conditions are expected to exceed the physiologic tolerance thresholds of the alveolar bone, the fixed hybrid prosthesis might be a more reliable treatment of choice instead of fixed metal ceramic restorations. The purpose of this article is to report the 1-year follow-up of the periodontal and prosthetic rehabilitation of a patient who has presented with symptoms of peri-implantitis due to incorrectly planned implant supported fixed metal ceramic bridge which was later replaced with screw-retained hybrid prosthesis following the treatment of peri-implant defects. Treatment helped to maintain patient's self-confidence and comfort, as well as favorable masticatory function. Rehabilitation with screw retained hybrid prosthesis is an ideal treatment of choice for maxillomandibular skeletal discrepancies.