1.
Angew Chem Int Ed Engl
; 50(9): 2125-8, 2011 Feb 25.
Artigo
em Inglês
| MEDLINE
| ID: mdl-21344566
2.
Adv Exp Med Biol
; 611: 129-30, 2009.
Artigo
em Inglês
| MEDLINE
| ID: mdl-19400124
3.
Org Lett
; 8(20): 4465-8, 2006 Sep 28.
Artigo
em Inglês
| MEDLINE
| ID: mdl-16986926
RESUMO
A peptide carrying a mercaptomethylated proline derivative at the C-terminus was prepared by solid-phase peptide synthesis (SPPS) and converted to the thioester of 3-mercaptopropionic acid (MPA) by aqueous MPA under microwave irradiation conditions. This post-SPPS thioesterification reaction was successfully applied to the synthesis of a glycopeptide thioester composed of 25 amino acid (AA) residues, which was then used for the preparation of a 61-AA glycopeptide by the thioester condensation method.