1.
J AOAC Int
; 78(3): 841-5, 1995.
Artigo
em Inglês
| MEDLINE
| ID: mdl-7756899
RESUMO
A method is presented for rapid determination of bromide ion in commodities and blood by paired-ion liquid chromatography with electrochemical detection. The method involves extraction of samples with water and filtration. Blood is passed through a Sep-Pak C18 minicolumn. Recoveries are usually close to 100%, with satisfactory precision. The detection limit is 1 mg/kg. The method needs little labor and uses no noxious solvents or reagents.