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J Nanosci Nanotechnol ; 14(6): 4431-6, 2014 Jun.
Artigo em Inglês | MEDLINE | ID: mdl-24738408

RESUMO

We have studied the experimental conditions needed to produce LaNiO3 (LNO) nanostructures using a template-assisted method. In this route, a mesoporous anodic aluminum oxide template was filled with a chemical solution that had been prepared with polymeric precursors route. The precursor solutions and synthesized samples were characterized by X-ray diffraction (XRD), thermogravimetric analysis, infrared spectroscopy and high-resolution scanning electron microscopy (HRSEM). The XRD results for the samples that were heat-treated at 700 degrees C revealed that these samples crystallize in a perovskite-like LaNiO3 structure. HRSEM images revealed that the samples prepared with different deposition times (0.5, 1 and 2 h) promoted the formation of LaNiO3 nanotubes with different wall thicknesses.


Assuntos
Cristalização/métodos , Impressão Molecular/métodos , Nanotubos/química , Nanotubos/ultraestrutura , Óxidos/síntese química , Substâncias Macromoleculares/química , Conformação Molecular , Nióbio , Tamanho da Partícula , Propriedades de Superfície
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