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1.
Microsc Res Tech ; 82(7): 1191-1197, 2019 Jul.
Artigo em Inglês | MEDLINE | ID: mdl-30920097

RESUMO

This study compared the performance of a glass ionomer (GC Gold Label 1, GIC) as a fiber post cementation system for glass fiber posts with a self-adhesive resin cement (Relyx U200, RUC) and a conventional resin cement system (Scotchbond Muli-Purpose and Relyx ARC, RAC). Thirty endodontically treated canines were randomly divided in three groups (n = 10), according to the fiber post cementation system: (RAC)-Scotchbond Multi-Purpose and Relyx X ARC; (RUC)-Relyx U200 and (GIC)-GC Gold Label 1 Luting & Lining. Rhodamine was incorporated into the cementation system prior to the fiber post cementation. After glass fiber post cementation, roots were incubated in artificial saliva for 6 months. After that, specimens from the cervical, middle, and apical thirds of the post space were prepared and analyzed using a push-out bond strength test and confocal laser microscopy. ANOVA one way and Tukey tests showed that GIC and RUC demonstrated similar push-out bond strength values, independently of the post space third (p > .05); however, values were greater than those shown by RAC (p < .05). For dentin penetrability, GIC and RUC also had similar results (p > 0.05) and lower than RAC (p < 0.05). Inside the root canal, the cementation system using glass ionomer cement (GC Gold Label 1 Luting & Lining) has similar push-out bond strength to the self-adhesive resin cement (Relyx U200) and these were higher than the conventional resin (Relyx ARC), despite its higher dentin penetrability.


Assuntos
Cimentos Dentários/química , Cimentos Dentários/farmacologia , Cavidade Pulpar/efeitos dos fármacos , Dentina/efeitos dos fármacos , Cimentos de Ionômeros de Vidro/farmacologia , Cimentação , Resinas Compostas/química , Resinas Compostas/farmacologia , Dente Canino/efeitos dos fármacos , Colagem Dentária , Humanos , Teste de Materiais , Cimentos de Resina/farmacologia , Preparo de Canal Radicular
2.
Dent Mater ; 23(10): 1245-9, 2007 Oct.
Artigo em Inglês | MEDLINE | ID: mdl-17204320

RESUMO

OBJECTIVE: To identify and quantify the camphorquinone (CQ) used in different brands of composite resins as a function of the shade analyzed. MATERIALS AND METHODS: Filtek Z250 A3 (FZA3), Filtek Z-250 Incisal (FZI), Pyramid Enamel A1 (PEA1), Pyramid Enamel Translucent (PET), Filtek Supreme A3E (FSA3) and Filtek Supreme GT (FSGT) were used. Five hundred milligrams of each resin were weighed and then dissolved in 1.0 ml of methanol. The samples were centrifuged to accelerate the sedimentation of the inorganic particles. 0.8 ml of the supernatant solution was collected with a pipette and assessed under gas chromatography coupled to the mass spectrometer (GC-MS). The results were compared to pure CQ solutions, used as a standard. Student's t-test, (p=0.05) significant at the level of 5%, compared the results of each brand shade. RESULTS: A smaller amount of camphorquinone was found in Filtek Z-250 (FZI) resin incisal shade when compared to (FZA3) A3 shade. On the other hand, Filtek Supreme resin featured a statistically larger camphorquinone amount in the incisal shade. In Pyramid Enamel resin camphorquinone was found only in shade A1, while the photoinitiator used in the Translucent shade was not identified. SIGNIFICANCE: Based on the data obtained, it is possible to conclude that a single composite resin brand may feature differences in amount and type of photoinitiator used.


Assuntos
Resinas Acrílicas/química , Cor , Resinas Compostas/química , Poliuretanos/química , Terpenos/análise , Teste de Materiais
3.
Acta Odontol Latinoam ; 20(2): 103-7, 2007.
Artigo em Inglês | MEDLINE | ID: mdl-18590259

RESUMO

This study evaluated the effects of distinct surface treatments on the micro-tensile bonding strength (microTBS) of different ceramic materials. The occlusal surfaces of eighteen human maxillary molars were flattened perpendicularly to the long axis and divided in groups based on surface treatment (sandblasting: s; hydrofluoric acid: a; tribochemical silica coating: t): DP-s, DP-a, DP-t, IE-s, IE-a, IE-t, IC-s, IC-a, IC-t) and ceramic materials (Duceran Plus: DP, IPS Empress 2: IE, In-Ceram Alumina, IC). Panavia F luting resins were used according to the manufacturers' instructions to bond ceramic materials to the exposed dentin specimens under a load of 7.5 N. After 3-day storage, microTBS was tested at a cross-head speed of 1 mm/min. Data were analyzed with ANOVA and Tukey's test. ANOVA results showed that the microTBS of DP and IC were significantly different. The microTBS of DP-a was significantly higher than those of DP-s and DP-t. The microTBS of IC-t was significantly higher than those of IC-s and IC-a. Ceramic materials with different chemical formulations and applications yielded significantly different bond strengths to human dentin and must receive distinct surface treatments accordingly.


Assuntos
Colagem Dentária , Corrosão Dentária/métodos , Porcelana Dentária/química , Dentina/ultraestrutura , Condicionamento Ácido do Dente/métodos , Óxido de Alumínio/química , Silicatos de Alumínio/química , Humanos , Ácido Fluorídrico/química , Compostos de Lítio/química , Teste de Materiais , Compostos de Potássio/química , Cimentos de Resina/química , Silanos/química , Dióxido de Silício/química , Cloreto de Sódio/química , Estresse Mecânico , Propriedades de Superfície , Temperatura , Resistência à Tração , Fatores de Tempo
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