RESUMO
A method for isolation and identification of 21 glues from cadavers has been developed. Chromogenic reactions are proposed to be used for identification and conditions of chromatography in a thin layer of sorbent developed.
Assuntos
Adesivos/análise , Adesivos/intoxicação , Cadáver , Cromatografia em Camada Fina/métodos , Humanos , Estômago/química , Transtornos Relacionados ao Uso de Substâncias/metabolismoRESUMO
A method for detection and measurements in cadaveric material of some drugs used to induce abortions has been developed. The drugs were measured by spectrophotometry, photo-electro-colorimetry, and argentometry. Detection threshold by the said methods was 0.5 to 3 mg%.
Assuntos
Abortivos/análise , Ácido Ascórbico/análise , Cadáver , Cromatografia em Camada Fina/métodos , Colorimetria/métodos , Alcaloides de Claviceps/análise , Etacridina/análise , Feminino , Humanos , Iodo/análise , Fígado/química , Gravidez , Esparteína/análise , Espectrofotometria/métodosRESUMO
Method of detection, purification and determination of some antidiabetic agents (ADA)--bucarban, butamid, glybenclamid, glybutide, methformine, prediane, chlorpropamide, chlocyclamide, cyclamide in biological material was developed. Microcrystalline reaction with 10% alcoholic potassium iodide, colour reactions and investigation by TLC method both native substances and nitration products were developed to identify ADA. The assay is performed by spectrophotometry. Detection limit is 2-5 mg of each substance in 50 g of the material.