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1.
Materials (Basel) ; 16(3)2023 Feb 02.
Artigo em Inglês | MEDLINE | ID: mdl-36770279

RESUMO

Developing accurate and interpretable models to forecast concrete's self-healing behavior is of interest to material engineers, scientists, and civil engineering contractors. Machine learning (ML) and artificial intelligence are powerful tools that allow constructing high-precision predictions, yet often considered "black box" methods due to their complexity. Those approaches are commonly used for the modeling of mechanical properties of concrete with exceptional accuracy; however, there are few studies dealing with the application of ML for the self-healing of cementitious materials. This paper proposes a pioneering study on the utilization of ML for predicting post-fire self-healing of concrete. A large database is constructed based on the literature studies. Twelve input variables are analyzed: w/c, age of concrete, amount of cement, fine aggregate, coarse aggregate, peak loading temperature, duration of peak loading temperature, cooling regime, duration of cooling, curing regime, duration of curing, and specimen volume. The output of the model is the compressive strength recovery, being one of the self-healing efficiency indicators. Four ML methods are optimized and compared based on their performance error: Support Vector Machines (SVM), Regression Trees (RT), Artificial Neural Networks (ANN), and Ensemble of Regression Trees (ET). Monte Carlo analysis is conducted to verify the stability of the selected model. All ML approaches demonstrate satisfying precision, twice as good as linear regression. The ET model is found to be the most optimal with the highest prediction accuracy and sufficient robustness. Model interpretation is performed using Partial Dependence Plots and Individual Conditional Expectation Plots. Temperature, curing regime, and amounts of aggregates are identified as the most significant predictors.

2.
Materials (Basel) ; 15(22)2022 Nov 16.
Artigo em Inglês | MEDLINE | ID: mdl-36431612

RESUMO

The cement industry generates very large amounts of CO2 into the atmosphere. In recent years, there has been a search for alternative cementitious materials and micro-fillers that could partially or fully replace cement in cement composites without compromising their durability. This paper investigates the possibility of using brick powder (BP) and clay powder (CP) as a partial replacement for cement (up to 20% by weight) in cement paste. The raw materials were characterized, and the physical and mechanical properties of the modified cement pastes were studied, as well as their resistance to a short-term thermal shock at 250 °C. The study was supplemented by intelligent modelling of compressive strength using the support vector machine (SVM) algorithms. The results indicated a significant increase in tensile strength (up to 100%) and an increase in thermal resistance of cement pastes modified with BP and CP. The proposed SVM model had high accuracy (R2 = 0.90), indicating its suitability to predict the compressive strength of the modified cement matrix. This study complements the knowledge in the field of inter alia, the effect of a short-term thermal shock at elevated temperature on the properties of BP and CP modified cement paste, and the effect of BP, which, due to its grain size, plays more the role of a microfiller than a pozzolanic additive.

3.
Materials (Basel) ; 14(24)2021 Dec 07.
Artigo em Inglês | MEDLINE | ID: mdl-34947094

RESUMO

Recycled aggregate is a good option to be used in concrete production as a coarse aggregate that results in environmental benefits as well as sustainable development. However, recycled aggregate causes a reduction in the mechanical and durability performance of concrete. On the other hand, the removal of industrial waste would be considerably decreased if it could be incorporated into concrete production. One of these possibilities is the substitution of the cement by slag, which enhances the concrete poor properties of recycled aggregate concrete as well as provides a decrease in cement consumption, reducing carbon dioxide production, while resolving a waste management challenge. Furthermore, steel fiber was also added to enhance the tensile capacity of recycled aggregate concrete. The main goal of this study was to investigate the characteristics of concrete using ground granulated blast-furnace slag (GGBS) as a binding material on recycled aggregate fibers reinforced concrete (RAFRC). Mechanical performance was assessed through compressive strength and split tensile strength, while durability aspects were studied through water absorption, acid resistance, and dry shrinkage. The results detected from the different experiments depict that, at an optimum dose (40% RCA, 20%GGBS, and 2.0%), compressive and split tensile strength were 39% and 120% more than the reference concrete, respectively. Furthermore, acid resistance at the optimum dose was 36% more than the reference concrete. Furthermore, decreased water absorption and dry shrinkage cracks were observed with the substitution of GGBS into RAFRC.

4.
Materials (Basel) ; 14(21)2021 Oct 23.
Artigo em Inglês | MEDLINE | ID: mdl-34771857

RESUMO

The cement industry is responsible for 8% of global CO2 production. Therefore, a clear trend has been observed recently to replace to some extent the main binder of cement composites with environmentally friendly or recycled materials with a lower carbon footprint. This paper presents the effect of brick powder (BP) on the physico-chemical and mechanical properties of cement mortars. The effect of a short-term thermal shock on morphology and strength properties of green mortars was investigated. BP addition caused increase in porosity and decrease in compressive and flexural strength of mortars. The best results were obtained for samples with 5% wt. BP addition. Above this addition the strength decreased. The mechanical performance of the samples subjected to thermal loading increased compared to the reference samples, which is the result of a process called as the "internal autoclaving". The BP addition positively affects the linear shrinkage, leading to its reduction. The lowest linear shrinkage value was achieved by the mortar with the highest BP addition. An intelligent modeling approach for the prediction of strength characteristics, depending on the ultrasonic pulse velocity (UPV) is also presented. To solve the model problem, a supervised machine-learning algorithm in the form of an SVM (support vector machines) regression approach was implemented in this paper. The results indicate that BP can be used as a cement replacement in cement mortars in limited amounts. The amount of the additive should be moderate and tuned to the features that mortars should have.

5.
Materials (Basel) ; 14(15)2021 Jul 21.
Artigo em Inglês | MEDLINE | ID: mdl-34361256

RESUMO

Nanomaterials are potential candidates to improve the mechanical properties and durability of cementitious composites. SiC nanowhiskers (NWs) present exceptional mechanical properties and have already been successfully incorporated into different matrices. In this study, cementitious composites were produced with a superplasticizer (SP) and 0-1.0 wt % SiC NWs. Two different NWs were used: untreated (NT-NW) and thermally treated at 500 °C (500-NW). The rheological properties, cement hydration, mechanical properties, and microstructure were evaluated. The results showed that NWs incorporation statistically increased the yield stress of cement paste (by up to 10%) while it led to marginal effects in viscosity. NWs enhanced the early cement hydration, increasing the main heat flow peak. NWs incorporation increased the compressive strength, tensile strength, and thermal conductivity of composites by up to 56%, 66%, and 80%, respectively, while it did not statistically affect the water absorption. Scanning electron microscopy showed a good bond between NWs and cement matrix in addition to the bridging of cracks. Overall, the thermal treatment increased the specific surface area of NWs enhancing their effects on cement properties, while SP improved the NWs dispersion, increasing their beneficial effects on the hardened properties.

6.
Materials (Basel) ; 14(13)2021 Jun 25.
Artigo em Inglês | MEDLINE | ID: mdl-34202009

RESUMO

The urbanization process contributes to the growth of solid waste generation and causes an increase in environmental impacts and failures in the management of solid waste. The number of dumps is a concern due to the limited implementation and safe disposal of this waste. The interest in sustainable techniques has been growing in relation to waste management, which is largely absorbed by the civil construction sector. This work aimed to review plastic waste, especially polyethylene terephthalate (PET), that can be incorporated with construction materials, such as concrete, mortars, asphalt mixtures, and paving. The use of life-cycle assessment (LCA) is related, as a tool that allows the sustainability of products and processes to be enhanced in the long term. After analyzing the recent literature, it was identified that studies related to plastic wastes in construction materials concentrate sustainability around the alternative destination of waste. Since the plastic waste from different production chains are obtained, it was possible to affirm the need for a broader assessment, such as the LCA, providing greater quantification of data making the alternative processes and products more sustainable. The study contributes to enhance sustainability in alternative building materials through LCA.

7.
Materials (Basel) ; 13(23)2020 Nov 24.
Artigo em Inglês | MEDLINE | ID: mdl-33255219

RESUMO

Industrial waste from the production of metallic silicon and silicon-iron alloys, which includes silica fumes (microsilica), is subject to numerous applications aiming at its reuse in concrete and polymeric composites. Recycling solves the problem of their storage and adverse environmental impact. Six different formulas of epoxy resins were tested, differing in the type of polymer, the mixing process (sonication or not) and the presence of microsilica. The study showed that microsilica added to the epoxy resin changes its viscosity and free surface energy, and these are the parameters that determine the adhesion of the polymer to the concrete surface. Strength tests and SEM analysis have determined how microsilica molecules can penetrate the structure of polymer macromolecules by filling and forming temporary chemical bonds. Mixing the fillers with the adhesive was achieved by using a sonication process. The analysis of the obtained results showed that, depending on the initial composition of the polymer, the addition of microsilica can change the chemical, physical and mechanical properties of the hardened adhesive to varying degrees. In the case of adhesives used in the construction industry to strengthen and glue structural elements, these changes significantly affect the durability of the adhesive joints.

8.
Sensors (Basel) ; 20(14)2020 Jul 10.
Artigo em Inglês | MEDLINE | ID: mdl-32664357

RESUMO

The paper presents an original approach to the localization and analysis of the cracking patterns of cement composites. The lime cement matrix modified with microsilica was evaluated under a two-phase thermal load. For quantitative detection and analysis of thermal cracks, an image-processing method was applied. For this purpose, an original image double-segmentation method was developed using machine-learning algorithms. Among other things, the fractal analysis was used to describe the morphology and the thermal evolution of the cracking patterns. The basic mechanical characteristics were examined and the results indicated a very high correlation between tensile strength and all cracking patterns' parameters. This allows high-quality estimation of the mechanical properties of the lime cement matrix to be carried out on the basis of measurement and evaluation of morphology of the thermal cracking patterns. Knowledge in this field contributes to the development of non-destructive testing methods in cement composites technology, in terms of localization of and tracking the cracking patterns.

9.
Materials (Basel) ; 13(11)2020 May 29.
Artigo em Inglês | MEDLINE | ID: mdl-32486046

RESUMO

The structure and the development degree of a cracking pattern has a key impact on the durability of cement composites. This literature review focuses on the four most important aspects related to the evaluation of the surface cracking patterns, i.e., the process of formation, propagation and evolution of cracks into a branched system of cracks from the point of view of the fracture mechanics; the detection techniques of the cracking patterns on the surface of cement composites, where the tools of computer image analysis are the most used; parameters which can quantify the development degree and morphology of the cracks system; and also the influence of a cracking pattern on the functional features of cement composites. The studies described so far indicate the necessity of continuous development of this research area, because the knowledge of key relationships between the cracking patterns and functional properties of a cement composite is necessary to estimate the degree of material degradation. Researchers agree that the works carried out in the field of evaluation of the cracking patterns, to a large extent, contributes to the development of non-destructive testing methods in the field of cement composites technology.

10.
Materials (Basel) ; 12(18)2019 Sep 11.
Artigo em Inglês | MEDLINE | ID: mdl-31514365

RESUMO

The research presented in this paper presents a quantitative analysis of cracking patterns on the surface of cement paste, which has been modified by the addition of the multi-wall carbon nanotubes (MWCNTs). The cracking patterns analyzed were created as a result of increased temperature load. MWCNTs were used as an aqueous dispersion in the presence of a surfactant, sodium dodecyl sulfate (SDS). Four series of the cement paste were tested, and the samples differed in the water/cement (w/c) ratio, cement class, and the presence of MWCNTs. Image analysis tools were used to quantify the cracking patterns and it was proposed to measure parameters, such as the average cluster area, average cluster perimeter, average crack width, and crack density. In order to facilitate the image analysis process, the sample surface was subjected to preparation and using statistical analysis tools it was assessed whether the method of surface preparation affects the way the sample is cracked. The paper also presents the analysis of the relationships that occur between parameters describing the cracking patterns, and also with the physico-mechanical properties of the cement pastes. It was attempted to explain the dependencies using elements of fractal theory and the theory of dispersion systems.

11.
Materials (Basel) ; 12(9)2019 May 07.
Artigo em Inglês | MEDLINE | ID: mdl-31067658

RESUMO

The paper describes a new model of concrete production, which contains a glass cullet. A worn-out car side window have been used for the production of recycled glass aggregate (RGA) and its properties were examined. The RGA was used in concrete as a 50% and 100% mass substitute of the traditional aggregate. Basic tests of fresh concrete mix and hardened concrete were carried out. The consistency, the air content in the concrete mix, the density of hardened concrete, water absorption, water resistance, frost resistance, and the compressive strength (after 9, 28, and 90 days) were evaluated. Composite samples were also subjected to microscopic analysis. The results showed that the RGA can be recommended as an aggregate for concretes, and the features of the RGA concrete are more favorable than those of traditional concrete. The microscopic analyses allowed us to identify the reasons for improving the properties of the RGA composites.

12.
Materials (Basel) ; 11(10)2018 Oct 10.
Artigo em Inglês | MEDLINE | ID: mdl-30308995

RESUMO

The paper evaluates the cracking patterns created on the surface of a microsilica-modified cement matrix, which has been subjected to exposure at elevated temperatures. To do this, image analysis techniques were used, and the structure of the cracks was described by the stereological parameters. Four series of specimens were tested and in two of them, microsilica was used as a 10% replacement for the cement content. Using the theory of dispersion systems, the factors affecting the cracks' characteristics were identified. Additionally, the development process of cracking patterns due to the thermal interaction was schematically modeled. In addition, the analysis of the local microstructure of the cement matrix was performed by means of a scanning electron microscope and energy dispersive x-ray spectroscopy.

13.
Materials (Basel) ; 11(7)2018 Jul 14.
Artigo em Inglês | MEDLINE | ID: mdl-30011895

RESUMO

The paper presents an analysis of the possibility of using glass waste from worn out lighting materials as an aggregate for a polymer concrete. Glass waste was obtained from the company utilizing glass lighting elements, which was then subjected to crushing. The aggregate obtained was subjected to the tests of basic features, which were compared with aggregates that are traditionally applied to concretes. The next stage of the research program was the production of a polymer concrete that contained glass aggregate. Several types of mixtures were prepared in which glass waste was combined in various proportions with traditional sand⁻gravel aggregate. As a part of the research, the basic physical and mechanical characteristics of polymer concretes were determined. The microstructure of composites was also analyzed using a scanning electron microscope. The results of the research have shown that the aggregate obtained from glass waste can be successfully used for the production of a polymer concrete. The most beneficial physico-mechanical properties were obtained for a composite in which glass waste was used as a 50% substitute for traditional aggregate.

14.
Materials (Basel) ; 11(4)2018 Mar 29.
Artigo em Inglês | MEDLINE | ID: mdl-29596357

RESUMO

In the paper the cluster cracks of cement paste that has been modified with metakaolinite was analyzed. The samples were loaded with an elevated temperature based on a thermal shock. To describe the crack structure, three stereological parameters were proposed to measure: (i) the cluster average area ( A ¯ ); (ii) the cluster average perimeter ( L ¯ ); and (iii) the crack average width ( I ¯ ). The computer image analysis was implemented in the study, and 4 series of samples were subjected to the examination. In two series, metakaolinite was used as a substitute for 10% of a cement's mass. An assessment of the basic physico-mechanical characteristics of the cement matrix was also carried out. The structure of the cement paste was considered as a highly concentrated dispersion system, in which the interactions between the cement's grains at the initial stage of the structure self-assembly affect the crack characteristics. The study has been supplemented with microstructural investigations using a scanning electron microscope and an X-ray microanalyzer. The conducted research indicated the direction of changes in the geometrical characteristics of thermal cracks if the technological variables of the material are subjected to modification. It was also confirmed that the cluster structures have fractal character and can be analyzed and observed on many levels of a structural heterogeneity.

15.
Nanomaterials (Basel) ; 7(9)2017 Sep 11.
Artigo em Inglês | MEDLINE | ID: mdl-28891976

RESUMO

The article presents the results obtained in the course of a study on the use of carbon nanotubes (CNTs) for the modification of a cement matrix. Carbon nanotubes were introduced into a cement paste in the form of an aqueous dispersion in the presence of a surfactant (SDS-sodium dodecyl sulfate), which was sonicated. The selected physical and mechanical parameters were examined, and the correlations between these parameters were determined. An analysis of the local microstructure of the modified cement pastes has been carried out using scanning electron microscope (SEM) and X-ray microanalysis (EDS). In addition, the effect of carbon nanotubes on the change in characteristics of the cementitious material exposed to the sudden, short-term thermal load, was determined. The obtained material was characterized by a much lower density than a traditional cement matrix because the phenomenon of foaming occurred. The material was also characterized by reduced durability, higher shrinkage, and higher resistance to the effect of elevated temperature. Further research on the carbon nanotube reinforced cement paste, with SDS, may contribute to the development of a modified cement binder for the production of a lightweight or an aerated concrete.

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