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1.
Luminescence ; 39(1): e4616, 2024 Jan.
Artigo em Inglês | MEDLINE | ID: mdl-37953062

RESUMO

Cymbopogon citratus-mediated pure aluminium oxide (Al2 O3 ) and europium (Eu)-doped Al2 O3 with different amounts of metal ion were prepared using a green synthesis method. Synthesised nanoparticles were characterised by ultraviolet (UV)-visible spectroscopy, photoluminescence (PL), Fourier-transform infrared (FTIR) spectroscopy, X-ray diffraction (XRD) and scanning electron microscopy (SEM). Synthesis of nanoparticles is confirmed by using UV-visible spectroscopy showing maximum absorption at 411 and 345 nm for Al2 O3 and Eu-doped Al2 O3 , respectively. The antibacterial activity of prepared nanoparticles was evaluated against Pseudomonas aeruginosa, Streptococcus aureus, Escherichia coli and Klebsiella pneumoniae using a well-diffusion technique. The effect of pure Al2 O3 and Eu-doped nanoparticles shows excellent results against P. aeruginosa, S. aureus, E. coli and K. pneumoniae.


Assuntos
Cymbopogon , Nanopartículas Metálicas , Nanopartículas , Európio/química , Escherichia coli , Staphylococcus aureus , Antibacterianos/farmacologia , Antibacterianos/química , Espectroscopia de Infravermelho com Transformada de Fourier , Difração de Raios X , Nanopartículas Metálicas/química , Testes de Sensibilidade Microbiana
2.
Luminescence ; 38(11): 1912-1920, 2023 Nov.
Artigo em Inglês | MEDLINE | ID: mdl-37564001

RESUMO

In the present report, Aegle marmelos leaf powder was used to synthesize copper nanoparticles (CuNPs) using a simple and cost-effective method. A. marmelos leaves have various medicinal uses including for the treatment of diarrhoea, constipation, diabetes, cholera, skin diseases, earache, blood purification, heart problems, and so on. The plant biomolecules induce the reduction of Cu2+ ions to CuNPs and also act as a capping and stabilizing agent. The formation of CuNPs was confirmed using photoluminescence (PL) excitation and emission spectra on a Shimadzu RF-5301 PC spectrofluorophotometer and the absorbance spectra of a UV-visible spectrophotometer at different stages during the synthesis process. In addition, other properties of synthesized CuNPs were also investigated using X-ray diffraction, Fourier transform infrared spectroscopy, and transmission electron microscopy techniques. The average size of the synthesized CuNPs was in the range 20-40 nm. Furthermore, the synthesized NPs were also considered for an antimicrobial study against Gram-positive Staphylococcus aureus and Proteus, and Gram-negative Escherichia coli and Salmonella spp. using the agar well diffusion method. The zone of inhibition against the Gram-positive bacteria was greater than the zone of inhibition against the Gram-negative bacteria. These investigation results suggest that synthesized NPs are promising nanomaterials for use as antimicrobial agents.


Assuntos
Aegle , Anti-Infecciosos , Nanopartículas Metálicas , Cobre/química , Aegle/química , Extratos Vegetais/farmacologia , Extratos Vegetais/química , Nanopartículas Metálicas/química , Anti-Infecciosos/química , Folhas de Planta/química , Antibacterianos/análise , Espectroscopia de Infravermelho com Transformada de Fourier , Química Verde , Testes de Sensibilidade Microbiana
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