An apparatus for measuring nonlinear viscoelasticity of minerals at high temperature.

We describe a high-temperature, uniaxial creep apparatus designed to investigate nonlinear attenuation of materials over a wide range of temperatures (25-1300 °C) using forced oscillations combined with a bias stress. This apparatus is primarily designed for investigation of minerals and rocks with high melting temperatures. An oscillatory compressional stress is used to determine attenuation and Young's modulus at frequencies of 10-1-102 Hz and high stress amplitudes (>0.1 MPa). Large bias stresses are applied in addition to the oscillatory stresses such that attenuation tests are conducted simultaneously with the ongoing creep. The complex compliance of the apparatus was characterized by conducting calibration tests on orientated crystals of sapphire. The real part of the apparatus compliance exhibits a dependence on sample length and frequency, whereas the imaginary part is only dependent on frequency. The complex compliance is not dependent on the oscillation amplitude or the bias stress. We assess the accuracy and precision of this calibration by comparing measurements of the attenuation and Young's modulus of aluminum and acrylic to previously published values. We outline a set of criteria defining the conditions over which this apparatus can precisely determine the attenuation and Young's modulus of a sample based on the sample length and expected values of attenuation and Young's modulus.

Size effects resolve discrepancies in 40 years of work on low-temperature plasticity in olivine.

The strength of olivine at low temperatures and high stresses in Earth's lithospheric mantle exerts a critical control on many geodynamic processes, including lithospheric flexure and the formation of plate boundaries. Unfortunately, laboratory-derived values of the strength of olivine at lithospheric conditions are highly variable and significantly disagree with those inferred from geophysical observations. We demonstrate via nanoindentation that the strength of olivine depends on the length scale of deformation, with experiments on smaller volumes of material exhibiting larger yield stresses. This "size effect" resolves discrepancies among previous measurements of olivine strength using other techniques. It also corroborates the most recent flow law for olivine, which proposes a much weaker lithospheric mantle than previously estimated, thus bringing experimental measurements into closer alignment with geophysical constraints. Further implications include an increased difficulty of activating plasticity in cold, fine-grained shear zones and an impact on the evolution of fault surface roughness due to the size-dependent deformation of nanometer- to micrometer-sized asperities.