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1.
J Microsc ; 294(2): 177-190, 2024 May.
Artigo em Inglês | MEDLINE | ID: mdl-38400676

RESUMO

The fracture behaviour of concrete is studied in various micro- and macro-damage models. This is important for estimating serviceability and stability of concrete structures. However, a detailed understanding of the material behaviour under load is often not available. In order to better interpret the fracture behaviour and pattern, images of lightweight concrete were taken using a high-resolution computed tomography (µ-CT) scanner. The samples were loaded between the taken images and the load was kept constant during the measurement. This study describes the method used and how the data set was analysed to investigate displacements and cracks. It has been shown that displacements and damage to the concrete structure can be detected prior to failure, allowing conclusions to be drawn about the structural behaviour. In principle, the µ-CT measurement can be used to examine different kinds of concrete as well as other systems with inorganic binders and to compare the fracture behaviour of different systems.

2.
Materials (Basel) ; 16(3)2023 Feb 02.
Artigo em Inglês | MEDLINE | ID: mdl-36770278

RESUMO

Knowledge of the exact composition of building materials (aggregate, binder, air voids, etc.) is essential for the further development of more resistant and sustainable building materials. In numerous scientific studies, the material behavior of asphalt is tested using mechanical methods. Here, the overall material behavior is determined (bitumen, air voids, aggregate). With the advent of imaging techniques, it is becoming possible to determine the individual constituents separately and perform a more detailed analysis of their location, shape and composition. Three-dimensional and two-dimensional methods are available for this purpose. For this study, two different types of asphalt (porous asphalt and asphalt concrete) were analyzed using 3D X-ray computed tomography and asphalt petrology as 2D methods; the results of both investigations are compared. The objective of this study is to determine whether the 2D method provides suitable results for the microstructural analysis of asphalt samples and how the results differ from those studied by the 3D method. The comparison shows that both methods can be used to analyze voids in asphalt samples. The 2D method provides valuable insight into the distribution of voids in a sample. In addition to the distribution of voids within a 2D section, the 2D method can also be used to make some structural statements about the location and structure of the voids in the 2D plane. The X-ray computed tomography method allows more complex analyses of the pore structure because of the third direction (3D). In addition, the 3D method provides more data, so that the pore structure can be described even more precisely, and the pore size (length, width, height) can be mapped and analyzed with a high degree of accuracy.

3.
Materials (Basel) ; 14(24)2021 Dec 09.
Artigo em Inglês | MEDLINE | ID: mdl-34947154

RESUMO

The material behavior of asphalt depends on its composition of aggregate, bitumen, and air voids. Asphalt pavements consist of multiple layers, making the interaction of the materials at the layer boundary important so that any stresses that occur can be relieved. The material behavior at the layer boundary is not yet understood in detail, as further methods of analysis are lacking in addition to mechanical methods. For this reason, the layer boundary of asphalt structures was analyzed using imaging methods. The aim of this research was to find an imaging method that allows a detailed analysis of the bonding zone of asphalt layers. Two different imaging techniques were used for this purpose. One is a 2-D imaging technique (asphalt petrology) and the other is a 3-D imaging technique (high-resolution computed tomography). Image analysis is a widely used technique in materials science that allows to analyze the material behavior and their composition. In this research, attention was paid to the analysis of the position of the bitumen emulsion, because the contained bitumen is supposed to bond the layers together. It was found that the application of 2-D imaging (asphalt petrology) lacked the precision for a detailed analysis of the individual materials at the layer boundary. With high-resolution computed tomography, a detailed view is possible to visualize the individual materials at the layer boundary in 3D. However, it is difficult to differentiate the materials because there are no gradations in the gray values due to the identical densities. However, it is possible to differentiate between the bitumen from the asphalt and from the emulsion if a high-density tracer is added to the bitumen emulsion for the CT studies. The results of the investigations are presented in this article.

4.
Materials (Basel) ; 14(19)2021 Oct 05.
Artigo em Inglês | MEDLINE | ID: mdl-34640212

RESUMO

It is important to ensure the durability and safety of structures. In the case of newly developed materials that are outside the current rules, it is important to investigate all aspects of structural safety. The material studied in the following is a structural lightweight concrete with an ultra-high-performance matrix and expanded glass as a lightweight aggregate. The material, with a compressive strength of 60-100 MPa and a bulk density of 1.5-1.9 kg/dm3, showed high capillary porosities of 12 vol% (ultra-high-performance concretes (UHPC) < 5 vol%). Since the capillary porosity basically enables transport processes into the concrete, the material had to be examined more closely from the aspect of durability. Freeze-thaw resistance (68 g/m2) and chemical attack with sulfate at pH 3.5 for 12 weeks (16 g/m2) showed no increase in concrete corrosion. Targeted carbonation (0.53 mm/year0.5) and chloride penetration resistance (6.0 × 10-13 to 12.6 × 10-13 m2/s) also showed good results against reinforcement corrosion. The results show that most of the measured capillary pores resulted from the lightweight aggregate and were not all present as a pore system. Thus, the durability was only slightly affected and the concrete can be compared to an UHPC. Only the abrasion resistance showed an increased value (22,000 mm3/5000 mm2), which, however, only matters if the material is used as a screed.

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