Research on Hot Stamping-Carbon Partition-Intercritical Annealing Process of Medium Manganese Steel.

In order to improve the plasticity of hot stamping parts, this paper combines the heat treatment process with the plastic forming of sheet metal, and creatively proposes a new process of hot stamping-carbon partitioning-intercritical annealing. The mechanical properties and microstructure are characterized under the newly proposed process, the quenching-partition (QP) process, and the intercritical annealing (IA) process, respectively. The new process firstly undergoes incomplete austenitizing treatment at 610 °C, then carries out distribution treatment while stamping at 300 °C, and finally conducts annealing treatment in critical zone at 680 °C in two-phase zone. The results show that a multi-phase refined microstructure composed of lath martensite, retained austenite, fresh martensite, and carbides are obtained by the new process. Most of the retained austenite is shaped in the thin film due to martensitic shear, in which carbon and manganese elements diffuse from martensite to austenite by heat treatment, thus stabilizing the retained austenite. Retained austenite with a volume fraction of 33.7% is obtained in the new process. The retained austenite with higher content and better stability is completely consumed during the stretching process, which gives full play to discontinuous TRIP effects, thus delivering the elongation of 36.8% and the product of strength and elongation (PSE) reached as high as 43.6 GPa%.

A Comparison Study on the Strengthening and Toughening Mechanism between Cu-Bearing Age-Hardening Steel and NiCrMoV Steel.

Cu-bearing age-hardening steel has significant potential in shipbuilding applications due to its excellent weldability as compared to conventional NiCrMoV steel. Not much research has been carried out to analyze the differences in the mechanisms of strength and toughness between Cu-bearing age-hardening and NiCrMoV steel. Both steels were heat treated under the same conditions: they were austenized at 900 °C and then quenched to room temperature, followed by tempering at 630 °C for 2 h. The uniaxial tensile test reveals that the Cu-bearing age-hardening steel exhibits relatively lower strength but larger plasticity than NiCrMoV steel. The lower contents of Carbon and other alloying elements is one of possible reasons for these differences in mechanical properties. Transmission Electron Microscope observations show that two types of precipitates, Cr carbides and Cu-rich particles, exist in tempered Cu-bearing age-hardening steel. Cu-rich particles with sizes of 20-40 nm can inhibit the dislocation motion during deformation, which then results in dislocation pile ups and multiplication; this makes up the strength loss of Cu-bearing age-hardening steel and simultaneously improves its plasticity.

Compressive Properties and Energy Absorption Characteristics of Extruded Mg-Al-Ca-Mn Alloy at Various High Strain Rates.

This paper is focused on the mechanical properties and the energy absorption characteristics of the extruded Mg-Al-Ca-Mn alloy in different compression directions under high strain rate compression. Compressive characterization of the alloy was conducted from the high strain rate (HSR) test by using a Split Hopkinson Pressure Bar (SHPB). Results show that the investigated alloy exhibits a strong strain rate sensitivity. With the rise of strain rate, the compressive strength is increased significantly, and the deformation ability also improves. When compressed along the extrusion direction, as the strain rate increases, the total absorbed energy E, the crush force efficiency (CFE), and the specific energy absorption SEA of Mg-Al-Ca-Mn alloy are all greatly improved as compared with those obtained along other compression directions.

Simultaneous melting and solidification of a columnar dendritic microstructure in a temperature gradient: Numerical modeling and experiments⋆.

The microstructural evolution of a SCN-ACE alloy in a temperature gradient is studied by cellular automaton (CA) modeling and in situ experiments. The initially columnar dendrites gradually evolve to a completely solid region with a planar solid/liquid interface. The CA simulations and in situ observations present the migration of secondary dendrite arms and liquid pockets due to temperature gradient zone melting (TGZM), and the movement of the interface between a mushy zone and a fully liquid zone. The CA simulations show that the interface movement toward the lower temperature region is caused by the increasing concentration of the fully liquid region. Through updating the concentration in the fully liquid zone to the initial concentration in the CA simulation for mimicking the efficient stirring in liquid, the movement of the interface between the mushy zone and the fully liquid zone is hindered. The simulated liquid fractions and mean concentrations throughout the mushy zone decrease with time, which agree well with the analytical predictions. The simulated concentrations in the resolidified mushy zone are not higher than the temperature-dependent solidus concentrations, implying that no supersaturation remains after the mushy zone fully solidifies.

Histo-morphologic characteristics of intra-osseous implants of WE43 Mg alloys with and without heat treatment in an in vivo cranial bone sheep model.

WE43 Mg alloy, composed of Mg, Yttrium, Rare Earth elements, and Zirconium, has proved to be a suitable candidate for production of resorbable osteosynthesis implants in both clinical and experimental settings. In a previous study we tested biocompatibility and degradation properties of untreated (as-cast) and artificially aged (T-5) WE43 Mg-alloys as subperiosteal implants on a maxillofacial sheep model. Both the alloy compositions showed excellent biocompatibility, however, with respect to degradation rate, the as-cast form showed increased degradability compared with the T-5. In the present study, we tested the same alloy composition (i.e. as-cast and T-5) to assess their biological behavior and degradation pattern when implanted as endosteal implants on a calvarial bone sheep model. Six implants in form of cylindrical discs were tested in 6 sheep, one per composition of each disc was placed in two monocortical cranial defect created with high speed trephine bur in the parietal bone. After euthanasia at 6 weeks histomorphological analysis of the bone/implant specimens was performed. WE43-as cast showed higher degradation rate, increased bone remodeling, gas pockets formation and osteolysis compared with the T5 alloy. WE43-T5 showed greater bone/implant interface stability, and seemed to be more suitable for fabrication of endosteal bone screws.

Biocompatibility and degradation properties of WE43 Mg alloys with and without heat treatment: In vivo evaluation and comparison in a cranial bone sheep model.

PURPOSE: Orthopedic and maxillofacial bone fractures are routinely treated by titanium internal fixation, which may be prone to exposure, infection or intolerance. Magnesium (Mg) and its alloys represent promising alternatives to produce biodegradable osteosynthesis devices, with biocompatibility and, specifically, hydrogen gas production during the degradation process, being the main drawback. Aim of this study is to test and compare biocompatibility, degradation rate and physiscochemical properties of two Mg-alloys to identify which one possesses the most suitable characteristics to be used as resorbable hardware in load-bearing fracture sites. MATERIALS AND METHODS: As-cast (WE43) and T5 Mg-alloys were tested for biocompatibility, physical, mechanical and degradation properties. Microstructure was assessed by optical microscopy, scanning electron microscopy (SEM) and energy-dispersive spectroscopy (EDS); mechanical properties were tested utilizing quasi-static compression and failure analysis. Locoregional biocompatibility was tested by sub-periosteal implantation on the fronto-nasal region of large-animal model (sheep): regional immunoreaction and metal accumulation was analyzed by LA-ICP of tributary lymph-nodes, local reactions were analyzed through histological preparation including bone, implant and surrounding soft tissue. RESULTS: Mechanically, T5 alloy showed improvement in strength compared to the as-cast. Lymph-node Mg accumulation depicted no differences between control (no implant) and study animals. Both alloys showed good biocompatibility and osteogenesis-promoting properties. CONCLUSION: This study demonstrated excellent biocompatibility and osteogenesis-promoting capabilities of the tested alloys, providing a platform for further studies to test them in a maxillofacial fracture setting. T-5 alloy displayed more stability and decreased degradation rate than the as-cast.

Data characterizing compressive properties of Al/Al2O3 syntactic foam core metal matrix sandwich.

Microstructural observations and compressive property datasets of metal matrix syntactic foam core sandwich composite at quasi-static and high strain rate (HSR) conditions (525-845 s(-1)) are provided. The data supplied in this article includes sample preparation procedure prior to scanning electron and optical microscopy as well as the micrographs. The data used to construct the stress-strain curves and the derived compressive properties of all specimens in both quasi-static and HSR regions are included. Videos of quasi-static compressive failure and that obtained by a high speed image acquisition system during deformation and failure of HSR specimen are also included.

Data characterizing flexural properties of Al/Al2O3 syntactic foam core metal matrix sandwich.

Microstructural observations and flexural property datasets are provided for aluminum alloy matrix syntactic foam core sandwich composites. The tests are conducted in three-point bending configuration. The data supplied includes methods used for conducting microscopy and mechanical testing. Raw load-displacement data, which is used to plot stress-strain graphs, obtained during the flexural test is also included. Images from a DSLR camera are stitched together to form a detailed failure sequencing video. Failure of specimens is captured in sequential images using a digital camera. These images are stitched together to develop a video for visualization of failure mechanisms. Calculations are also included for a theoretical model that is used to estimate the flexural properties of the syntactic foam core sandwich.