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Appl Radiat Isot ; 68(9): 1855-8, 2010 Sep.
Artigo em Inglês | MEDLINE | ID: mdl-20434350

RESUMO

The effect of sample vial type and cocktail quantity on tritium measurement in liquid scintillation counting is studied in this paper. With both high and low level tritium samples, glass vials allow higher counting rates than plastic vials do. We also present detailed analysis of the way to obtain the optimal counting condition by dispensing different quantity of cocktail into sample vials. Results indicate that the optimal counting condition has little relationship with tritium concentration in the sample. The main factor which influences the counting is the quantity of cocktail added into samples. Figure of merit is employed to access the results, which increases as the quantity of cocktail increasing. But when the ratio of cocktail and sample reaches 2.0, increase of ratio makes little contribution to the counts, and the disintegrations per minute comes nearly to be a constant.


Assuntos
Artefatos , Contagem de Cintilação/instrumentação , Manejo de Espécimes/instrumentação , Trítio/análise , Desenho de Equipamento , Análise de Falha de Equipamento , Doses de Radiação , Reprodutibilidade dos Testes , Sensibilidade e Especificidade
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