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Org Biomol Chem ; 18(6): 1082-1086, 2020 02 14.
Artigo em Inglês | MEDLINE | ID: mdl-31971222

RESUMO

A novel cyclization of α-halogenoacetamides with 1-azadienes has been developed for the efficient preparation of monocyclic 1,4-diazepinones in one step under transition metal-free conditions. Various α-halogenoacetamides and 1-azadienes are well tolerated and give the desired products in good to excellent yields. This cyclization also demonstrates potential synthetic utility on a gram-scale and further transformation.

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