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1.
Molecules ; 29(11)2024 Jun 04.
Artigo em Inglês | MEDLINE | ID: mdl-38893519

RESUMO

Nitrite is one of the most common nitrogenous compounds, which is not only an important indicator of aquaculture water but also widely used as a food additive. Its potential toxicity poses a huge threat to aquatic products and human health. Therefore, it is important to develop a convenient and rapid sensor for the high-efficient onsite detection of nitrite. In this work, a novel electrochemical sensor was developed for the qualitative and quantitative analysis of nitrite. The developed nitrite electrochemical detection system is easily applied in onsite detection. The electrochemical working electrode was constructed based on the combination of Ag-CeO2 and conductive carbon paste (CPE) with excellent electrocatalysis activity and rapid electron transfer ability. By the application of the developed system and under the optimal conditions, the linear range was from 40.0 µM to 500.0 µM, and the detection limit was reduced to 4.3 µM. The recovery was between 92.1% and 108.1%, and the relative standard deviations (RSDs) were 0.49%~9.31%. The sensor exhibited superior reproducibility, high stability sensitivity, and anti-interference ability, confirming its effectiveness for nitrite analysis. Finally, the developed electrochemical sensor was successfully applied to detect nitrite in beverages and aquaculture water samples, indicating that this approach has great potential in onsite food testing and environmental monitoring.


Assuntos
Aquicultura , Bebidas , Cério , Técnicas Eletroquímicas , Nitritos , Nitritos/análise , Técnicas Eletroquímicas/métodos , Cério/química , Bebidas/análise , Prata/química , Limite de Detecção , Poluentes Químicos da Água/análise , Eletrodos , Reprodutibilidade dos Testes , Água/química , Água/análise
2.
Biosensors (Basel) ; 13(3)2023 Feb 27.
Artigo em Inglês | MEDLINE | ID: mdl-36979539

RESUMO

Antibiotics are considered a new type of organic pollutant. Antibiotic residues have become a global issue due to their harm to human health. As the use of antibiotics is increasing in human life, such as in medicine, crops, livestock, and even drinking water, the accurate analysis of antibiotics is very vital. In order to develop rapid and on-site approaches for the detection of antibiotics and the analysis of trace-level residual antibiotics, a high-sensitivity, simple, and portable solution is required. Meanwhile, the rapid nanotechnology development of a variety of nanomaterials has been achieved. In this review, nanomaterial-based techniques for antibiotic detection are discussed, and some reports that have employed combined nanomaterials with optical techniques or electrochemical techniques are highlighted.


Assuntos
Técnicas Biossensoriais , Nanoestruturas , Humanos , Antibacterianos/análise , Técnicas Biossensoriais/métodos , Nanoestruturas/química , Nanotecnologia/métodos , Técnicas Eletroquímicas/métodos
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