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Room temperature drop hammer impact and compression after impact (CAI) experiments were conducted on carbon fiber-epoxy resin (CF/EP) composites to investigate the variation in impact load and absorbed energy, as well as to determine the residual compressive strength of CF/EP composites following impact damage. Industrial CT scanning was employed to observe the damage morphology after both impact and compression, aiding in the study of impact-damage and compression-failure mechanisms. The results indicate that, under the impact load, the surface of a CF/EP composite exhibits evident cratering as the impact energy increases, while cracks form along the length direction on the back surface. The residual compressive strength exhibits an inverse relationship with the impact energy. Impact damage occurring at an energy lower than 45 J results in end crushing during the compression of CF/EP composites, whereas energy exceeding 45 J leads to the formation of long cracks spanning the entire width of the specimen, primarily distributed symmetrically along the center of the specimen.
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Low-heat Portland cement and ground granulated blast furnace slag are widely used for the preparation of hydraulic concrete. Nevertheless, the effect and mechanism of corrosion on low-heat Portland cement paste mixed with ground granulated blast furnace slag need to be further explored. This paper investigated the impact of ground granulated blast furnace slag on the calcium leaching of low-heat Portland cement paste by evaluating its mass loss, porosity, leaching depth, compressive strength, and Vickers hardness, and comparing it with the leaching performance of ordinary Portland cement paste. Furthermore, the phase composition and morphology of low-heat Portland cement paste containing ground granulated blast furnace slag were analyzed by X-ray diffraction, mercury intrusion porosimetry, and scanning electron microscopy. The results indicate that, after 180 days of soaking in ammonium chloride solution, the mass loss rate, growth rate of porosity, leaching depth, and compressive strength loss rate of low-heat Portland cement paste were 8.0%, 43.6%, 9.1 mm, and 27.7%, respectively, while those of ordinary Portland cement paste were 7.4%, 37.8%, 8.4 mm, and 30.1%, indicating that low-heat Portland cement paste is slightly more damaging than ordinary Portland cement. The addition of ground granulated blast furnace slag could significantly improve the leaching resistance of low-heat Portland cement. For instance, after adding 20% ground granulated blast furnace slag, the above test values were 2.4%, 28.5%, 5.6 mm, and 20.8%, respectively. The reason for this is that ground granulated blast furnace slag has the potential to reduce the porosity of low-heat Portland cement paste, and it can also undergo the secondary hydration reaction with its hydration product Ca(OH)2 to enhance the paste structure. Considering the cost performance, the suitable dosage of low-heat Portland cement paste for satisfactory leaching resistance is about 20%.
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Carbon fiber reinforced polymer (CFRP) tendons are composite materials that offer significant advantages in terms of tensile strength and lightweight properties. They are being increasingly utilized in the construction industry, particularly in bridge cables and building structures. However, due to their relatively poor transverse mechanical properties compared to steel cables, securing these tendons with anchors presents a challenge. This paper reviews the structure and force characteristics of three types of anchors for CFRP tendons-clamping anchorage, bonded anchorage, and composite anchorage-analyzes and summarizes the anchorage characteristics and damage mechanisms of each type of anchorage, and highlights that the optimization of the mechanical properties of the tendons is key to the design and research of anchoring systems. The new composite anchorage offers comprehensive advantages, such as minimal tendon damage at the anchorage section, more uniform stress distribution, and better anchorage performance, despite being more complex in design compared to single-type anchorages. However, there remain challenges and research gaps in testing and validating these anchoring systems under realistic loading and environmental conditions, including impacts, cyclic stresses, humidity, and high temperatures. Future efforts should focus on developing new testing techniques and models to simulate real-world conditions, enabling more accurate assessments of anchorage performance and longevity. By doing so, we can fully harness the mechanical properties of CFRP tendons and further enhance the safety and efficiency of our built environment.
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To investigate the influence of water content on the rockburst phenomena in tunnels with horizontal joints, experiments were conducted on simulated rock specimens exhibiting five distinct levels of water absorption. Real-time monitoring of the entire blasting process was facilitated through a high-speed camera system, while the microscopic structure of the rockburst debris was analyzed using scanning electron microscopy (SEM) and a particle size analyzer. The experimental findings revealed that under varying degrees of water absorption, the specimens experienced three stages: debris ejection; rockburst; and debris spalling. As water content increased gradually, the intensity of rockburst in the specimens was mitigated. This was substantiated by a decline in peak stress intensity, a decrease in elastic modulus, delayed manifestation of pre-peak stress drop, enhanced amplitude, diminished elastic potential energy, and augmented dissipation energy, resulting in an expanded angle of rockburst debris ejection. With increasing water content, the bond strength between micro-particles was attenuated, resulting in the disintegration of the bonding material. Deformation failure was defined by the expansion of minuscule pores, gradual propagation of micro-cracks, augmentation of fluffy fine particles, exacerbation of structural surface damage akin to a honeycomb structure, diminishment of particle diameter, and a notable increase in quantity. Furthermore, the augmentation of secondary cracks and shear cracks, coupled with the enlargement of spalling areas, signified the escalation of deformation failure. Simultaneously, the total mass of rockburst debris gradually diminished, accompanied by a corresponding decrease in the proportion of micro and fine particles within the debris.
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This study concerned the in situ investigation of the defect evolution and fracture mechanism of additively manufactured (AM) Ti-6Al-4V under uniaxial tensile tests. In order to achieve this, microstructure characterization was initially carried out in order to identify the defects within the matrix of the candidate material. In situ testing was then performed, focusing on the spherical defect to observe its evolution under tensile loading. It was found that, before the fracture stage, the geometric evolution of the spherical defect towards an ellipse shape was dominated by the load in the tensile direction. In addition, the slip band density was found to be aggravated near the spherical defect due to the geometric discontinuity-induced stress concentration. During the fracture process, the defect geometry evolved as an irregular shape, which was mainly attributed to the micro-void-induced localized multi-axial stress state. The fracture analysis indicated that defects play a key role in crack initiation, leading to the fracture of LPBF materials.
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In general, formed components are lightweight as well as highly economic and resource efficient. However, forming-induced ductile damage, which particularly affects the formation and growth of pores, has not been considered in the design of components so far. Therefore, an evaluation of forming-induced ductile damage would enable an improved design and take better advantage of the lightweight nature as it affects the static and dynamic mechanical material properties. To quantify the amount, morphology and distribution of the pores, advanced scanning electron microscopy (SEM) methods such as scanning transmission electron microscopy (STEM) and electron channeling contrast imaging (ECCI) were used. Image segmentation using a deep learning algorithm was applied to reproducibly separate the pores from inclusions such as manganese sulfide inclusions. This was achieved via layer-by-layer ablation of the case-hardened steel 16MnCrS5 (DIN 1.7139, AISI/SAE 5115) with a focused ion beam (FIB). The resulting images were reconstructed in a 3D model to gain a mechanism-based understanding beyond the previous 2D investigations.
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Mycotoxin contamination has become a major food safety issue and greatly threatens human and animal health. Patulin (PAT), a common mycotoxin in the environment, is exposed through the food chain and damages the gastrointestinal tract. However, its mechanism of enterotoxicity at the genetic and metabolic levels remains to be elucidated. Herein, the intestinal histopathological and biochemical indices, transcriptome, and metabolome of C57BL/6â¯J mice exposed to different doses of PAT were successively assessed, as well as the toxicokinetics of PAT in vivo. The results showed that acute PAT exposure induced damaged villi and crypts, reduced mucus secretion, decreased SOD and GSH-Px activities, and enhanced MPO activity in the small intestine and mild damage in the colon. At the transcriptional level, the genes affected by PAT were dose-dependently altered in the small intestine and fluctuated in the colon. PAT primarily affected inflammation-related signaling pathways and oxidative phosphorylation in the small intestine and immune responses in the colon. At the metabolic level, amino acids decreased, and extensive lipids accumulated in the small intestine and colon. Seven metabolic pathways were jointly affected by PAT in two intestinal sites. Moreover, changes in PAT products and GST activity were detected in the small intestinal tissue but not in the colonic tissue, explaining the different damage degrees of the two sites. Finally, the integrated results collectively explained the toxicological mechanism of PAT, which damaged the small intestine directly and the colon indirectly. These results paint a clear panorama of intestinal changes after PAT exposure and provide valuable information on the exposure risk and toxic mechanism of PAT.
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Metabolômica , Camundongos Endogâmicos C57BL , Patulina , Transcriptoma , Animais , Patulina/toxicidade , Camundongos , Transcriptoma/efeitos dos fármacos , Masculino , Intestino Delgado/efeitos dos fármacos , Intestino Delgado/patologia , Intestino Delgado/metabolismo , Mucosa Intestinal/efeitos dos fármacos , Mucosa Intestinal/metabolismo , Colo/efeitos dos fármacos , Colo/patologia , Intestinos/efeitos dos fármacos , Intestinos/patologiaRESUMO
Aluminum matrix composites (AMMCs) have demonstrated substantial potential in the realm of armor protection due to their favorable properties, including low density, high specific stiffness, and high specific strength. These composites are widely employed as structural components and frequently encounter high strain rate loading conditions, including explosions and penetrations during service. And it is crucial to note that under dynamic conditions, these composites exhibit distinct mechanical properties and failure mechanisms compared to static conditions. Therefore, a thorough investigation into the dynamic mechanical behavior of aluminum matrix composites and precise constitutive equations are imperative to advance their application in armor protection. This review aims to explore the mechanical properties, strengthening the mechanism and deformation damage mechanism of AMMCs under high strain rate. To facilitate a comprehensive understanding, various constitutive equations are explored, including phenomenological constitutive equations, those with physical significance, and those based on artificial neural networks. This article provides a critical review of the reported work in this field, aiming to analyze the main challenges and future development directions of aluminum matrix composites in the field of protection.
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To improve the efficiency of frozen soil excavation, the new shaft tunneling machine was developed. The new shaft tunneling machine exerts pressure on the frozen soil through the cutter under the joint action of its own gravity, the drum rotational force and the inertia force, and the frozen soil is damaged. By unique way of breaking frozen soil to improve the efficiency of frozen soil excavation, the drum rotation speed is one of the factors affecting the performance of frozen soil excavation. This article applies SolidWorks software to establish the model of cutter breaking frozen soil, takes advantage of Hyper Mesh finite element software coupled with LS-DYNA solver to acquire the regular pattern of change in the force change, frozen soil stress-strain and specific energy of cutter crushing frozen soil, etc., which analyzes the destruction of frozen soil when the drum of the new shaft tunneling machine is rotating at the speed of 25-40 rpm. Combine with field test to investigate the mechanism of cutter breaking frozen soil under the optimal drum rotation speed. The investigation results demonstrate that: when frozen soil's self-bearing capacity is lower than the force of cutter, it breaks up and detaches from the soil body, and frozen soil undergoes tensile, compressive and shear damages. For this research, it is instructive for practical engineering.
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Carbon/Carbon (C/C) composites exhibit excellent mechanical properties at high temperatures, making them widely used in aerospace, such as the leading edges of spaceplane wings and the nose cones of hypersonic aircraft. However, damage caused by rain erosion to C/C composites affects their mechanical properties and poses significant challenges during operational service periods. A jet impingement test platform was employed to conduct single and multiple water-jet erosion tests on three-dimensional orthogonal C/C composite materials and to investigate the residual mechanical properties of the specimens after jet impact. The damage was characterized using optical microscopy, scanning electron microscopy, and X-ray computed tomography. The results showed that the damage types of the C/C composite materials under water-jet impingement included fiber bundle fracturing, delamination, and debonding. The extent of erosion damage was positively correlated with the jet velocity and diameter. The changes in the multi-jet damage indicated a cumulative expansion process, and z-directional fiber bundles exhibited superior resistance to jet impact damage propagation. The results of the three-point bending tests showed that the greater the initial impact damage, the lower the residual mechanical properties of the materials, and the residual strength of the specimen suddenly decreased when damage occurred at the back of the specimen.
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The research object is diorite in the Lingbei TBM section of the Hanjiang-To-Weihe River Qinling tunnel, with a buried depth of over 1 km. Using MTS-2000 microcomputer-controlled electro-hydraulic servo universal testing machine and DS5-16b acoustic emission (AE) monitoring system, uniaxial compression and acoustic emission monitoring tests were carried out on rock samples, to study the uniaxial compression mechanical properties and acoustic emission characteristics of the deep diorite. The results of the study indicate that: (1) During uniaxial compression, diorite undergoes four stages: initial compaction, elasticity, yield and failure, in which the curve of the initial compaction stage is significantly smoother. The uniaxial compressive strength is 41.95 MPã102.42 MPa, with an average of 74.07 Mpa; The axial peak strain ranges from 1 % to 1.4 %, and the failure mode belongs to brittle ductile splitting failure. (2) The cumulative ringing count and energy showed a very slow increase trend during the calm period; After entering a surge period (with the appearance of Kaiser points), both show a significant transition state; During the slow increase period, the overall growth rate of the two slowed down and remained almost silent. (3) On the basis of the analysis of RA-AF values during the deformation and rupture process of diorite, it can be seen that the damage type of diorite is tensile damage by the significant low RA value and high AF value characteristics, which coincides with the actual damage fracture characteristics of the rocks in the sample. (4) During the compaction stage, there are few acoustic emission location points, which correspond to low energy and are mainly distributed at the higher and lower ends of the sample; After entering the elasticity stage, the number of positioning points significantly increases and gradually expands towards the middle; Near Kaiser point, the number of location points and corresponding energy are both in a sharp increase state, and this trend is in good agreement with the changes in the ringing count-time and energy-time curves. (5) The damage time mainly starts at the end of the calm period, and the pattern of change in the damage curve coincides with the localization point and energy evolution. The results of the research can be used as a referential basis for the development of the excavation, protection and other construction plans for the Lingbei TBM section of the Hanjiang-To-Weihe River Qinling tunnel or similar surrounding rock tunnels, as well as for further conducting triaxial unloading tests on diorite.
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To study the fatigue failure and microstructure evolution behavior of SS304, low-cycle fatigue tests are conducted at room temperature (RT), 300 °C, and 650 °C. The results indicate that, because of the influence of the dislocation walls, carbon-containing precipitates, and deformation twins, the cyclic hardening behavior is presented at RT. However, different from the cyclic hardening behavior at RT, the cyclic softening behavior of SS304 can be observed due to the dynamic recovery and recrystallization containing dislocation rearrangement and annihilation at 300 °C and 650 °C. In addition, two fatigue crack initiation modes are observed. At RT, the single fatigue crack initiation mode is observed. At high temperatures, multiple crack initiation modes are presented, resulting from the degradation of material properties. Furthermore, a new fatigue life prediction model considering the temperature is conducted as a reference for industrial applications.
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Lead halide perovskites (LHPs) are outstanding candidates for next-generation optoelectronic materials, with considerable prospects of use and commercial value. However, knowledge about their toxicity is scarce, which may limit their commercialization. Here, for the first time, we studied the cardiotoxicity and molecular mechanisms of representative CsPbBr3 nanoparticles in LHPs. After their intranasal administration to Institute of Cancer Research (ICR) mice, using advanced synchrotron radiation, mass spectrometry, and ultrasound imaging, we revealed that CsPbBr3 nanoparticles can severely affect cardiac systolic function by accumulating in the myocardial tissue. RNA sequencing and Western blotting demonstrated that CsPbBr3 nanoparticles induced excessive oxidative stress in cardiomyocytes, thereby provoking endoplasmic reticulum stress, disturbing calcium homeostasis, and ultimately leading to apoptosis. Our findings highlight the cardiotoxic effects of LHPs and provide crucial toxicological data for the product.
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Compostos de Cálcio , Nanopartículas , Animais , Camundongos , Compostos de Cálcio/toxicidade , Miocárdio , Óxidos/toxicidade , Nanopartículas/toxicidadeRESUMO
Root damage from urban street trees represents a substantial concern arising from the conflict between root growth and limited growth spaces. Nonetheless, the phenomenon of root damage, which threatens the safety of urban facilities, appears to have received little scholarly attention. Moreover, the effectiveness of some proposed measures for root damage prevention and control has not yet received consistent evaluation. Accordingly, this review aims to examine root damage, including its causes and available prevention and control measures. Urban trees are found to have a high potential to exert root damage on infrastructures when the following factors exist. These include large and mature tree, fast-growing trees, trees planted in limited soil volumes, shallow-rooted tree with buttress roots, trees whose diameter at breast height exceeds 10 cm, old and cracked road paving, high soil surface moisture content, short distances between trees and sidewalks (<2 to 3 m), and underground pipes that are already broken and made of metals or stones. The phenotypic traits of trees may be the primary factor causing root damage when there is a mismatch between the root-soil requirements of urban street trees and the actual soil environment. The poor effectiveness of root damage prevention and control measures may be attributed to the lack of connection between the development of control measures and the mechanism of root damage.
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Solo , Árvores , Solo/químicaRESUMO
Designing bio-composites for structural applications requires a thorough understanding of their mechanical behavior. In this study, we examined the differences in the tensile strength and drop-weight impact response between polypropylene reinforced with flax fibers and that reinforced with pinewood short fibers, as both fibers differ in composition (cellulose, hemicellulose, and lignin) and length-to-diameter ratio. We found that flax fibers, which have higher cellulose content and are twice as long as pine fibers, increased the stiffness and shock resistance of bio-composite materials. However, pine fibers, which contain more lignin, showed increased material ductility and energy absorption. Impulse excitation, acoustic emission and micro-CT techniques were used to evaluate the post-impact mechanical properties and the contribution of each damage mechanism to the final material failure (tearing). The experimental results were used to validate a model based on finite elements. Our results revealed that the experimental and finite-element analyses were in good agreement.
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The composite fretting-corrosion damage due to combinations of radial, tangential, rotational, and other fretting causes local adverse tissue reactions and failure of artificial joints. Previous studies have mainly focused on the single fretting mode, while ignoring the coupled effects of multimode fretting. The fretting-corrosion mechanisms between the components are not yet fully understood. In this study, the tangential-radial composite fretting was realized by applying a normal alternating load to the tangential fretting. The composite fretting corrosion behavior of zirconia toughened alumina ceramic/Ti6Al4V alloy used for the head-neck interface of an artificial hip joint under simulated body fluid was investigated. The effects of displacement and alternating load amplitude were considered. The alternating load amplitude was given by the maximum normal load and minimum normal load ratio R. The results showed that the composite fretting damage mechanisms of this pair were mainly abrasion and tribocorrosion. Cracking also existed under large displacement. The effect of alternating load on fretting corrosion was found to be mainly caused by changes in the contact area and instantaneous contact state. In addition, the alternating load during the composite fretting promoted the formation of the three-body layer in the contact area. A decrease in load ratio caused fretting to change from gross to partial slip. In the case of small displacement, the load ratio had little effect on the friction work or wear scar profile. The corrosion rate of materials and the concentration of metal ions released into the solution increased as load ratio decreased. In cases of large and medium displacement, load ratio reduction increased the friction work and expanded the wear scar. The reduction in load ratio also caused the corrosion rate of the material to increase and then decrease, and the metal ion concentration decreased.
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Líquidos Corporais , Cicatriz , Humanos , Corrosão , Ligas , Óxido de AlumínioRESUMO
To improve their interfacial properties, 3D orthogonal woven fabrics with basalt filament yarns were modified with functionalized carboxylated carbon nanotubes (KH570-MWCNTs) and polydopamine (PDA). Fourier infrared spectroscopy (FT-IR) analysis and scanning electron microscopy (SEM) testing were used. It was demonstrated that both methods could successfully modify basalt fiber (BF) 3D woven fabrics. The 3D orthogonal woven composites (3DOWC) were produced with epoxy resin and 3D orthogonal woven fabrics as raw material by the VARTM molding process. The bending properties of the 3DOWC were tested and analyzed by experimental and finite element analysis methods. The results showed that the bending properties of the 3DOWC modified by KH570-MWCNTs and PDA were significantly improved, and the maximum bending loads were increased by 31.5% and 31.0%. The findings of the finite element simulation and the experiment results were in good agreement, and the simulation error value was 3.37%. The correctness of the finite element simulation results and the model's validity further reveal the material's damage situation and damage mechanism in the bending process.
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The anti-ESD characteristic of the electronic system is paid more and more attention. Moreover, the on-chip electrostatic discharge (ESD) is necessary for integrated circuits to prevent ESD failures. In this paper, the mixed TCAD model of the ESD protection circuit is built and simulated, and the negative transmission line pulse (TLP) injection damage experiment is carried out on the CD4069UBC chip. The circuit model consists of three-dimensional shallow trench isolation (STI) diode TCAD models and a three-dimensional multi-gate Complementary Metal-Oxide-Semiconductor (CMOS) inverter TCAD model. Moreover, the TCAD modeling is based on a 0.25 µm technology node. Through the transient simulation of the electrothermal coupling, the electrical signal of the input and output nodes of the circuit and the distribution of the electrothermal parameters in the device are obtained. Moreover, by analyzing the simulation results, the physical phenomena and the mechanisms of interference and damage mechanism during TLP injection are explained. The location and type of diode damage in the TLP injection simulation results of the circuit model are consistent with the TLP experiment damage results. The proposed ESD protection circuit model and analysis method are beneficial to ESD robustness prediction and ESD soft damage analysis of IC.
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Rough surfaces have been widely considered as negative factors affecting cavitation erosion resistance. However, this study presented the opposite result. Here, 316L stainless steel substrates and the arc-sprayed 316L stainless steel coatings were subjected to a specific grinding process that introduced scratches on the surfaces. The surface hardness values of these ground specimens were measured to evaluate the influence of the grinding-induced strain hardening. The cavitation erosion performance of the specimens was evaluated. The results showed that rough surfaces with scratches could enhance the cavitation erosion resistance, particularly at the early stage of cavitation erosion. The scratches had a greater effect on the cavitation erosion resistance of the coatings than on the substrates. Moreover, rough surfaces with initial surface scratches could extend the incubation period of the 316L stainless steel substrates due to the inhibition of the plastic deformation. The SEM observation showed that the scratch structure of the coating surface inhibited the growth of cracks and the propagation of cavitation pits. This study could also serve as a reference for investigating the cavitation erosion behaviors of materials with a particular surface feature.
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OBJECTIVES: To compare the impact-sliding wear of different CAD/CAM resin-ceramic materials and tooth enamel, and explore the corresponding wear damage mechanism. METHODS: Human tooth enamel (EN), Vita ENAMIC (Vita, VE), Lava Ultimate (3 M, LU), and GC CERASMART (GC, CS) were used in this study. The hardness, elastic modulus, and roughness values of the samples were measured. Further, impact-sliding wear tests were performed in a ball-on-flat configuration with spherical zirconia antagonists and the coefficients of friction (CoF) were recorded simultaneously. Additionally, a white light interferometer was used to determine the volume losses and scanning electron microscopy was used to observe the wear morphology of the wear scars and the damage feature in the vertical sections to clarify the damage mechanism during the impact-sliding wear test. RESULTS: EN exhibited the highest elastic modulus and CoF, followed by VE, LU, and CS. The hardness and roughness of EN and VE were similar and were higher than those of LU and CS. Throughout the wear tests, VE exhibited the highest volume loss, whereas CS exhibited the lowest. The wear damage characteristics of VE were similar to those of EN, displaying brittle fractures of inorganic substances and plastic deformation of organic substances in the impact part, exhibiting plough marks in the sliding parts. In the case of LU and CS, the entire wear areas displayed plastic deformation of the resin matrix, exfoliation of the filler particles, and plough marks. SIGNIFICANCE: Enamel and polymer-infiltrated ceramic network materials exhibit similar wear damage modes. Additionally, the high-density nanocomposite resin material is the most resistant to impact-sliding wear from a tribological perspective.